Volume 38, Issue 4 (Journal of Advanced Materials-Winter 2020)
2020, 38(4): 33-42 |
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Loghman Estarki M R, Ghalibaf Tousi H, Mohammad Sharifi E, Sheikh H, Alhaji A. Effect of Chelating Agent on Morphology and Phase Evolution of Spinel Nanoparticles Synthesized via Sol-Gel Method. Journal of Advanced Materials in Engineering (Esteghlal) 2020; 38 (4) :33-42
URL: http://jame.iut.ac.ir/article-1-1027-en.html
URL: http://jame.iut.ac.ir/article-1-1027-en.html
Department of Materials Engineering, Malek Ashtar University of Technology, P.O. Box 83145/115, Iran. , loghman57@gmail.com
Abstract: (4198 Views)
The purpose of this study was to evaluate the effect of glycyrol (tri-dentate, GLY) and ethylenediamine (double- dentate clay, en) chelating agents on phase and morphology changes of spinel nanoparticles synthesized by sol-gel method. Characterization of samples was performed by X-ray diffraction (XRD) and field-emission scanning electron microscope (FESEM) equipped with energy dispersive X-ray spectrometer (EDX). The results showed that both samples synthesized with GLY and en contain cubic spinel phase. The sample synthesized with ethylenediamine has a pyramidal morphology with particle size in the range of 20-25 nm whereas the specimen prepared with glycerol is spherical with particle size in the range of 20-25 nm. Finally, suggested mechanism for morphological changes of spniel nanoparticles was discussed.
Type of Study: Research |
Subject:
Advanced Synthesis and production processes
Received: 2019/03/16 | Accepted: 2019/12/9 | Published: 2020/02/10
Received: 2019/03/16 | Accepted: 2019/12/9 | Published: 2020/02/10
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