Volume 32, Issue 1 (Jun 2013)
2013, 32(1): 91-99 |
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A. M. Molavi, S. M. Mirkazemi, A. Beitollahi. The Effects of Heat Treatment and Atmosphere on Magnetic Properties of Nano-Structured Nickel Ferrite Glass-Ceramic. Journal of Advanced Materials in Engineering (Esteghlal) 2013; 32 (1) :91-99
URL: http://jame.iut.ac.ir/article-1-554-en.html
URL: http://jame.iut.ac.ir/article-1-554-en.html
School of Material Science and Engineering, Iran University of Science and Technology , mahdi.molavi@gmail.com
Abstract: (7577 Views)
The effects of temperature, time and atmosphere on microstructure and magnetic properties of NiFe2O4 glassceramic were investigated utilizing differential thermal analysis, X-ray diffraction, vibrating sample magnetometer and scanning electron microscope techniques. Various compositions were studied in the Na2O-NiO-Fe2O3-B2O3-SiO2 system to obtain amorphous phase. The sample heat-treated in graphite bed at 510°C for 1 hr showed higher magnetization than the one heattreated in the air under the same condition. XRD analysis showed the presence of nickel ferrite and some non-magnetic phases such as sodium borate and silicate phases in the heat treated samples. The maximum magnetization of samples reduced by increasing the holding time from 1hr to 3 hr at 510°C. Increment of temperature to 700°C increased the amount of NiFe2O4 and maximum magnetization.
Type of Study: Research |
Subject:
General
Received: 2015/02/9 | Accepted: 2015/05/6 | Published: 2015/05/6
Received: 2015/02/9 | Accepted: 2015/05/6 | Published: 2015/05/6
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