Volume 34, Issue 2 (Journal of Advanced Materials- Summer 2015)                   2015, 34(2): 61-69 | Back to browse issues page

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Amiri H, Mirkazemi S M, Beitollahi A. Synthesizing CoFe2O4 by Glass-Ceramic Method and Characterizing its Magnetic Properties in Na2O-Fe2O3-CoO-B2O3-SiO2 System. Journal of Advanced Materials in Engineering (Esteghlal) 2015; 34 (2) :61-69
URL: http://jame.iut.ac.ir/article-1-669-en.html
Synthesizing CoFe2O4 by Glass-Ceramic Method and Characterizing its Magnetic Properties in Na2O-Fe2O3-CoO-B2O3-SiO2 System
H. Amiri , S. M. Mirkazemi * , A. Beitollahi
Iran University of Science and Technology, Tehran, Iran , mirkazemi@iust.ac.ir
Abstract:   (10862 Views)
In this investigation, the effect of heat treatment on magnetic properties of glass and nano-structured cobalt-ferrite glass-ceramic was studied. The glass was synthesized in the system of Na2O-Fe2O3-CoO-B2O3-SiO2. Based on DTA results, heat treatment was done at different times and temperatures. X-ray diffraction pattern of glass-ceramic showed the crystallization of CoFe2O4 and some nonmagnetic phases. The highest magnetization of 11.8 emu/g was obtained for the sample heat-treated for 2 hr at 670C in graphite bed. Average crystallite size of CoFe2O4 in this sample was 50 nm. Scanning Electron Microscopy (SEM) confirmed the formation of cobalt ferrite nanoparticles in the glass matrix.
Keywords: Heat treatment, Cobalt-Ferrite, Glass-Ceramic, Nano-structured
Full-Text [PDF 639 kb]   (4464 Downloads)    
Type of Study: Research | Subject: Surface engineering and coatings
Received: 2015/09/2 | Accepted: 2015/09/2 | Published: 2015/09/2
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