The present research has examined the effect of adding Si3N4 on the mechanical and structural properties of NiCrAlY alloy. The structural and mechanical properties of the manufactured samples were characterized by SEM, XRD,  micro-hardness evaluation and pin on disk wear test. Various concentrations of Si3N4 powder (1, 3, and 5 wt.%) were mixed with NiCrAlY powder using a mechanical ball mill. Next, the mixtures were sintered at 1100 ^°C using the spark plasma sintering (SPS) technique. The XRD patterns indicated that the samples were composed of two phases of solid solution γ-Ni(Cr) and intermetallic compounds β-NiAl. The results of micro-hardness measurements showed that adding 1% Si₃N₄ to NiCrAlY enhanced the hardness from 418 to 614 HV. However, with an increase in the Si₃N₄ content from 1 to 5 wt%, the hardness diminished from 614 to 543 HV, and by Adding Si3N4 to the NiCrAlY, its tribological properties were significantly improved.