Showing 8 results for F. Ashrafizadeh
M. Shamanian, M. Salehi and F. Ashrafizadeh,
Volume 16, Issue 2 (1-1998)
Abstract
The use of Fe-Al intermetallic compound coatings has been investigated in order to improve the tribological behaviour of carbon tool steel. The coatings were formed by a pack cementation process and subsequently diffusion annealing at 900˚C in an argon controlled atmosphere. The optimum diffusion time was selected on the basis of optimum thickness and tribological behaviour.
The microstructure and the phases developed on the surface were identified by metallography, microhardness, X-ray diffraction (XRD), microanalysis (EDX) and glow discharge optical spectroscopy (GDOS) techniques. Experimental results indicate that a three layer coating is formed on the surface of the aluminized specimens, the outermost layer being identified as Fe2Al5 and the underlying layers as FeAl and Fe3Al. A two layer coating was formed on the surface of the aluminized and subsequently diffusion annealed specimen at the optimum time. The FeAl and Fe3Al have been formed on and below the surface, respectively.
The results from wear testing indicate that these coatings improve the wear and frictional behaviour of carbon steel significantly. The predominant wear mechanisms of diffusion annealed specimens were identified as delamination and oxidative wear.
F. Ashrafizadeh, M. R. Toroghinezhad,
Volume 17, Issue 1 (7-1998)
Abstract
In this study carburizing and boronizing processes were applied to powder metallurgy steel specimens and the mechanical and tribological properties of the substrate and coatings were evaluated under various process conditions.
The specimens, made from industrial test pieces, were carburized in a powder pack for a duration of 2-5 hrs at 850-950 ˚C. Similar specimens were pack boronized for 4 hrs at 950 ˚C. The effect of austenitization-quench treatment was also investigated on some specimens. The wear tests were carried out by means of a pin-on-disc tribotester against ball bearing steel.
The results indicate that by appropriate selection of process parameters it is possible to obtain high wear resistance together with moderate toughness. Boride layers with hardness values of 1700HV are properly formed on PM samples. The wear resistance, therefore, is significantly increased with practically no reduction in impact resistance. It is concluded that boronizing treatment can be more suitable for some PM parts under tribological conditions.
S. R. Bakhsi, M. Salehi, F. Ashrafizadeh,
Volume 17, Issue 2 (4-1998)
Abstract
A study for optimizing of siliconizing and borosiliconizing processes on carbon steels has been carried out. The process parameters, i.e, time and powder mixture, were considered for optimization of the case depth, surface quality and the hardness profile.
Time and temperature of the processes were 4 hr and 950˚C, respectively. Powder mixture in siliconizing process was 2.5% ferrosilicon, 2.5% NH4Cl and Al2O3, while the optimum simultaneous borosiliconizing process was obtained in a mixture of 90% boronizing powder and 10% siliconizing powder. These powders had already been optimized, individually. This is a depth of layer of about 150μm and maximum hardness value of 600HV0.1 in siliconized steels, and a depth of layer of about 100μm and a hardness value of greater than 3000 HV0.1 in borosiliconized steels. Microscopical tests by light microscopes, XRD and EDAX analyses indicated Fe3Si and Fe5Si3 phases within the surface layers of siliconized steel, and B(FeSi)3, Fe4.9Si2B, FeSi, FeB and Fe2B phases within the surface layers of borosiliconized steels.
R. Mozaffarinia, F. Ashrafizadeh, M. A. Golozar,
Volume 22, Issue 2 (1-2004)
Abstract
The purpose of this work was to production of ceramic thin films by using of Sol-Gel process. For this purpose deposition of SiO2 on substrates of soda-lime glasses has been carried out. Coating treatments on prepared specimen were conducted in a Sol solution by means of dipping at various times. After drying and performing appropriate heat treatment on each sample, the thickness of coated layer was measured by means of roughness method. Some of the specimens were also exposed to heat and chemical environment to evaluate the coating resistance in such media. SEM examination and EDAX and XRD analysis of coating layers was also conducted on some samples.
The results indicated that by Sol-Gel method, it is easily possible to achieve thin layers in the scale of one hundredth micron meter. Any change of the thickness layer on the surface is negligible and the quality of the coating is excellent. Also, experiments indicated that deposited coatings by Sol-Gel process, are stable and give enough durability in various environments.
S. Vahabzadeh, M. A. Golozar, F. Ashrafizadeh and A. Ghasemi,
Volume 27, Issue 2 (1-2009)
Abstract
A. Azimi Dastgerdi, F. Ashrafizadeh, M. R. Toroghinejad, F. Shahriari , H. Zahraei,
Volume 30, Issue 2 (Dec 2011)
Abstract
In this paper, bare spot defects in hot-dip galvanized sheets were studied in terms of the microstructure and their influence on the corrosion and mechanical properties. Surface characteristics and microstructural features were examined by scanning electron microscopy equipped with energy dispersive spectroscopy microanalysis system. The results showed that the major cause of the bare spots was the lack of wetability of the sheet surface due to contamination, improper heat treatment or chemical composition. Corrosion resistance was evaluated by standard salt spray test. Mechanical properties were examined by tensile testing. The time to red rust was much shorter on the bare spots as compared to other regions, but it appeared that bare spot defects had no significant effect on the mechanical properties of the galvanized steel sheets.
F. Shahriari, F. Ashrafizadeh, A. Saatchi,
Volume 31, Issue 2 (Dec 2012)
Abstract
Although titanium has been recognized for its excellent bio-compatibility with human tissues and good corrosion resistance in some specific environments, little attention has been paid to the surface enrichment of the components by titanium. In this paper, titanium diffusion coating was formed on the surface of Ni-based alloy B-1900 via pack cementation technique and the microstructure of the coatings obtained was studied. Diffusion titanizing was carried out via pack cementation technique at 850 and 950 C for 3 hours in a mixture of commercially pure titanium, Al2O3 and NH4Cl powder. Microstructure, phase composition and concentration profile of the coatings were examined using optical and electron metallography, X-ray diffraction, and glow discharge optical spectroscopy. The results showed that Ti2Ni and AlNi2Ti were the main constituents of the coating. The formation mechanism of the coatings was also evaluated.
E. Sadri, F. Ashrafizadeh, M. Ramazani,
Volume 32, Issue 2 (Dec 2013)
Abstract
In plasma sprayed nanostructured composite coatings with ceramic matrix, the feedstock must consist of nanoparticles of appropriate specifications. In this research, the procedure for production of Cr2O3-Ag agglomerated nanostructured composite powder to produce comosite coatings has been investigated. Nanopowders of Cr2O3 with 0, 2, 5, and 10 volume percentages of silver were dispersed to obtain a homogeneous aqueous dispersion appropriate for spray drying process. In the second stage, Cr2O3-Ag composite powders were produced by agglomeration process. The nanostructured composite powders were, then, used in the atmospheric plasma spray (APS) process to deposit a series of composite coatings for evaluation. The composite powders, with a granulated morphology, had uniform distribution of silver in a ceramic matrix and the coatings were composed of nanoparticles and particles of nano-sized crystallites. Experimental results indicated that presence of nanoparticle zones within the microstructure led to non-uniform porosities formed between splats and these zones. Furthermore, use of nanopowders in the feedstock caused a reduction in lamellae thickness of plasma sprayed coatings.
