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Showing 2 results for M. Kalantar

M. Kalantar and G. Fantozzi,
Volume 22, Issue 1 (7-2003)
Abstract

Dense Silicon nitride was investigated to determine the effect of its microstructural parameters and densification on thermo-mechanical properties and thermal stress resistance to fracture initiation during a hot or cold mechanical and thermal shock testing. The different materials and microstructures were obtained by changing the parameters such as the type of the powder, additive, forming process and sintering condition. Maximum crack growth and thermal shock resistance of dense Si3N4 are achieved after complete conversion of the aàB transformation, and after the change in grain morphology towards elongated grain and the relative crystallization of the second phases have been obtained. The characteristics are obtained by a high a phase content of the starting powder, high Y2O3, and sintering condition of higher temperature (2000ْC), longer soaking times (1h) and load application at the beginning of the thermal cycle. Keywords: Silicon nitride, Thermo- mechanical properties, Thermal shock resistance, Crack propagation resistance
P. Zarrabian, M. Kalantar, M. Mosallaeepour, A. Mashreghi,
Volume 33, Issue 3 (Journal of Advanced Materials- winter 2015)
Abstract

Nickel ferrite based cermets and their relevant composites have been widely used as inert anodes for aluminum electrolysis due to their good combination of chemical resistance, thermal stability and mechanical properties. In this study, various NiO/NiFe2O4 composites consisting of 5, 10 and 15% NiO in conjunction with Cu/NiFe2O4 cermets containing 0.5, 10 and 15% Cu were prepared by powder metallurgy method. The degradation resistance of the developed inert composites was examined under hot corrosion condition by plunging samples in to the molten electrolyte at 1000ºC. The strength, toughness, hardness, relative density, microstructural observation, phase analysis and electrical resistivity were evaluated by 3-points bending tests, Vickers method, Archimedes method, scanning electron microscope, x-ray diffraction and conventional direct current four-probe techniques, respectively. The experimental results for NiO/NiFe2O4 composites showed that a significant improvement of toughness and degradation resistance continuously occurred with a moderate decrease in strength by increasing NiO content, while the relative density was increased only up to 5%NiO content. By increasing the Cu content in the cermet samples, all the properties such as strength, toughness and electrical conductivity were improved considerably but the degradation resistance decreased.

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