K. Zangeneh Madar and S. M. Monir Vaghefi,
Volume 23, Issue 2 (1-2005)
Abstract
In the present stady, thermochemical treatment in H2/NH3 atmosphere was used as a post-treatment for electroless Ni-P coatings on the AISI 4140 steel substrates. High phosphorus (9%) coatings with thicknesses of 2, 24 and 48 m were applied and the effects of the thermochemical treatment on the morphology, structural changes, roughness, hardness
and wear resistance of coatings were studied by SEM, EDS, XRD, profilometry, and microhardness tester. Wear test was used to evaluate wear characteristics of coatings. The wear behaviour of the thermochemical treated/Ni-P coated samples was assessed by comparison with thermochemical treated/uncoated (nitrided) samples. The results showed that effect of thermochemical treatment varies with the coating thickness. In addition, it was shown that a multicomponent coating containing phosphide, nitride and intermetallic phases as well as diffusion region can be developed in the thin (2 m) electroless Ni-P coated steel by thermochemical treatment. This sample showed better wear resistance than 24 m Ni-P coated steel under higher load. This behavior was ascribedto nitride phases formed at the surface as well as a nitrogen diffusion zone at the subsurface of thin Ni-P coated steel
M. Barjesteh, K. Zangeneh Madar, S. M. Abbasi, K. Shirvani,
Volume 38, Issue 2 (Journal of Advanced Materials-Summer 2019)
Abstract
In this study, the effect of platinum-aluminide coating parameters on surface roughness of nickel-based superalloy Rene®80 was evaluated. For this purpose, different thicknesses of Pt-layer (2, 4, 6 and 8µm) were plated on the Samples. Then diffusion aluminide coating in two types, high tempeature-low activity and low temperature-high activity was performed. The results of structural investigations by scanning electron microscope and X-Ray diffraction indicated a three-zone structure of coating in all thicknesses of platinum layer, as well as in the two methods of aluminizing. Surface roughness of coatings was measured in three steps: 1-after Pt plating, 2-after Pt diffusion, and 3-after aluminizing and final aging. The results showed that the thickness of Pt and the final thickness of the coating directly affected the surface roughness. The minimum surface roughness was created by high temperature low activity with 2µ of Pt-layer (2.6μm) and the maximum of surface roughness was obtained in low-temperature high activity with 8µ of the Pt-layer (8.8 μm).
