Showing 7 results for Microhardness
B. Bakhit, A. Akbari,
Volume 31, Issue 2 (12-2012)
Abstract
Composite and nanocomposite Ni-Co/SiC coatings were synthesized by electro-codeposition of micro and nano-sized SiC particles with average diameter of 10m and 20nm using horizontal electrodes. Surface morphology, chemical composition, phase composition, hardness and corrosion resistance of the deposited coatings were studied using SEM observations and EDX, XRD, microhardness and polarization measurements as a function of the electrodeposition current density. The results indicated that the nanocomposite coatings exhibit higher hardness and corrosion resistance compared with the composite coatings containing micro-sized SiC particles despite their lower percentage of the SiC content. The maximum hardness values of 615HV and 490HV were obtained for nanocomposite and composite coatings deposited at current density of 3A/dm2. The observed properties were discussed based on the structural details.
S. Tavassoli, M. Abbasi, R. Tahavvori,
Volume 35, Issue 2 (9-2016)
Abstract
The purpose of this article is to study the formation of intermetallic compounds (IMCs) at the interface of Al/Cu bimetal produced by compound casting of molten Al in solid copper tubes. The mechanism of the intermetallic compounds formations at the interface, the effects of molten aluminum pouring temperature and solid copper tubes preheating tempreture, were investigated on the IMCs type and thickness and Al/Cu interface microstructures were characterized by optical microscope (OM) and electron probe micro-analyzer (EPMA). Results show that the interface consists of three main layers, where Layer (I) is α-Al/Al2Cu eutectic structure, layer (II) is intermetal of Al2Cu and layer (III) constituites several intermetallic compounds such as AlCu, Al3Cu4, Al2Cu3 and Al4Cu9. Considering the components of hypereutectic melt at the interface, initially layer (II) was formed by θ phase nucleation and growth mechanism, then layer (I) was formed by Al and Cu dissolving and solidification. Finally layer (III) was formed by solid-state phase diffusion. Raising molten Al temperature and preheating solid Cu leads to increase of the intermetallic compounds thickness at interface which consequently increases the specific electrical resistance and decreases the Al/Cu bond strength. From experimental results it seems that the bond strength is affected by the thicknesses of layer II and III.
S. Safi, Dr G. H. Akbari,
Volume 36, Issue 1 (6-2017)
Abstract
Strengthening of copper matrix by dispersion of metallic oxides particles as an efficient way to increase strength without losing thermal and electrical conductivities has been recognized for many years. Such a composite can withstand high temperatures and keep its properties. Such copper alloys have many applications especially in high temperature including resistance welding electrodes, electrical motors and switches. In the present work, at first, the Cu-1%Al solid solution was prepared by the mechanical alloying process via 48 hours of milling. Subsequently, 0.66 gr of copper oxide was added to Cu-1%Al solid solution and mechanically milled for different milling times of 0,16, 32, 48 hours. The milled powder mixtures were investigated by X-Ray Diffraction and scanning electron microscopy techniques. The lattice parameter of Cu increased at first, but then decreased at longer milling times. The internal strain increased and the average Cu crystal size decreased during milling process.The particle size decreased during the whole process. With increasing annealing temprature from 450°C to 750°C, the microhardness values of samples decreased at the beginning but then increased. From these results, it can be concluded that nanosize aluminaparticles are formed in the copper matrix.
Kh. Farjam Hajiagha, A. R. Akbari, R. Mohammadzadeh,
Volume 36, Issue 2 (9-2017)
Abstract
In this study, the kinetics of austenite layer growth on the surface of Fe-23Cr-2.4Mo ferritic stainless steel during solution nitriding and the effects of nitrogen adding on microstructure and hardness of the steel have been investigated. Steel plates of 2 mm thick were solution-nitrided at 1200˚C under nitrogen pressure of 0.25 MPa for 2, 3, 6, 9, 12 hours. Microstructure, the thickness of austenite layer and the hardnes of the nitrided samples, were investigated by using optical microscope, X-ray Diffraction (XRD) and microhardness measurements. The results showed that during solution nitriding, nitrogen diffuses through the lattice and grain boundaries and transforms ferrite to austenite phase, with average nitrogen diffusion coefficient of 6.54×10-5 mm2s-1. The thickness of the austenite layer formed on the samples surfaces increased proportional to the square root of the nitriding time, so that after 12 hours niriding, the whole thickness of the ferritic sample with hardness of 262 HV0.1 transformed to austenite with hardness of 420 HV0.1.
M.r. Khanzadeh Gharah Shiran, H. Bakhtiari, M. Mohammad Javadi,
Volume 36, Issue 3 (11-2017)
Abstract
In this research, the effect of standoff distance and explosive material thickness on metallurgical features of explosive welding connection of copper to 304 stainless steel has been investigated. Experimental analysis were performed using optical microscopy, scanning electron microscopy, microhardness test and tensile shear strength test. The results indicated that due to severe plastic deformation in welding, both grain elongation and refinement occurred near the connection. Also, increasing of welding parameters led to an increase in the locally melted zones. The results showed that chemical composition of the melted zone consisted of elements of both flyer and base plates. By decreasing the explosive material thickness and standoff distance, the hardness of copper interface zone decreased from 103.4 HV to 99.8 HV. Moreover, increasing the temperature in stainless steel connection led to decreased hardness. As such, the maximum tensile shear strength of 244 MPa was observed in the sample with 79 mm explosive thickness and 3 mm standoff and the minimum tensile shear strength of about 208 MPa in the sample with 46 mm explosive thickness and 3 mm standoff. By decreasing explosive thickness and standoff, the bond strength decreased, too.
M. Alizadeh, A. Cheshmpish,
Volume 37, Issue 2 (9-2018)
Abstract
In this research, Ni-Mo-Al2O3 composite coatings were electro-deposited on the mild carbon steel in a citrate bath containing micro- sized Al2O3 particles. Afterward, the effect of the particle concentration in the electrolyte bath (ranging from 0 g/L to 30 g/L) on the microstructure, microhardness, and corrosion performance was evaluated. To investigate the microstructural changes and the surface morphology of the coatings, as well as the particle distribution in the deposits, optical and scanning electron microscopy coupled with the energy dispersive X-ray spectroscopy was utilized. The corrosion behavior of the prepared coatings was investigated in a 3.5 wt. % NaCl solution. The results showed that the presence of the Al2O3 particles in the Ni-Mo coatings changed the microstructure and also, increased the microhardness and corrosion resistance of them. It was also found that the desirable structure of the protruding crystallite morphology with no detectable pores could be achieved at the medium concentrations of reinforcement (e.g. 20 g/L). Further the optimum concentration of the particles in the electrolyte bath to attain the composite coating with the desirable microstructure and consequently, the desirable corrosion resistance was found to be 20 g/L.
A. Mohammadi, B. Niroumand, A. Saboori,
Volume 40, Issue 4 (3-2022)
Abstract
Electron beam melting (EBM) is among the modern additive manufacturing processes whereby metal powders are selectively melted to produce very complicated components with superior mechanical properties. In this study, microstructure, hardness, and surface roughness of EBM fabricated Ti6Al4V samples were characterized. The results showed that the microstructure consisted of epitaxially-grown primary columnar β phase transformed to basketweave and Widmanstatten-type α phase during the subsequent rapid cooling. Martensitic needle-type α phase was also observed on the surfaces of the specimens. It was shown that higher parts of the sample had finer microstructures than the lower parts reaching to less than 340 nm in average thickness of the α layers due to distancing from the hot build platform rendering less opportunity for diffusional β → α+β transformation. The porosity content of the samples was lower than that of some other additive manufacturing processes. Vickers micro-hardness of the samples was measured to be around 337 HV which was higher than those reported for other additive manufacturing processes of the alloy.
