Showing 26 results for Microstructure
M. Shamanian, A. Saatchi, M. Salehi and T. H North,
Volume 21, Issue 2 (1-2003)
Abstract
The metallurgical and mechanical properties of Ti6Al4V/(WC-Co) friction welds have ben investigated. The microstructure close to the bondline comprised a mixture of acicular and equiaxed α plus β phases. The diffusion of elements in the welded specimens has been detected. The fracture strengths of Ti6Al4V/(WC-Co) friction welds markedly improved when the cobalt content in the (WC-Co) carbide substrate increased.
During the three-point bend testing of Ti6Al4V/WC-6wt.%Co welds, the crack initiated at the bondline region at the periphery of the weld and then propagated into the brittle (WC-6wt.%Co) substrate, while with the Ti6Al4V/WC-11 wt.%Co and Ti6Al4V/WC-24wt.%Co welds, the crack initiated and propagated at the bondline region.
Keywords: Friction welding, Ti6Al4V alloy, Cemented tungsten carbide, Microstructure, Fracture strength
H. Moslemi Naeini, M. Maerefat and M. Soltanpour,
Volume 22, Issue 1 (7-2003)
Abstract
In hot forming process, the workpiece undergoes plastic deformation at high temperature and the microstructure of the workpiece changes according to the plastic deformation. These changes affect the mechanical properties of workpiece. In order to optimize this process, both the plastic deformation of workpiece and its microstructural changes should be taken into consideration. Since material behaviors at elevated temperatures are usually rate-sensitive, the analysis of the hot forming processes requires a thermo-viscoplastic model. In this paper, by coupling the flow stress prediction model developed with finite element analysis of thermo-viscoplastic of the hot upsetting process, temperature, strain rate, flow stress distributions and geometry of the workpiece at each time step can be calculated. At each time step, the strain rate and temperature at each element are obtained. From these values and the history of deformation, the changes in microstructure and flow stress can be determined.
Keywords: Hot forming, Process, Finite element analysis, Flow stress, Microstructure, Hot upsetting process
A.r. Kiani Rashid and M. A. Golozar,
Volume 22, Issue 2 (1-2004)
Abstract
M. Shamanian and A. Saidi,
Volume 24, Issue 1 (7-2005)
Abstract
The 25Cr-35Ni heat resistant steel has been widely used when resistance to oxidation and creep rapture at elevated temperatures is required. In this paper, the microstructural effect on the weldability of this alloy is investigated. The results of this study indicate that this steel has a perfect weldability in the as cast condition but does not possess good weldability in the aged condition. The as cast microstructure of 25Cr-35Ni steel consists of austenite matrix and a network of primary carbides, while the aged condition consists of austenite matrix and y primary and secondary carbides. The morphological change of primary
carbides and the secondary carbides precipitate formation, reducing the elongation and ductility of aged steel, should have enhanced the steel susceptibility to cracking, particularly in the area of the eutectic carbides, and hence, the reduced weldability of the steel. The cracking observed was of the intergranular type and spread along the eutectic carbides. It was found that the carbides in the as cast steel consisted of NbC and M23C6, whereas that of the aged steel also exhibited Ni16Nb6Si7 and M23C6 carbides
E. Ganjeh, H. Khorsand,
Volume 31, Issue 1 (6-2012)
Abstract
The fracture surfaces of PM Cr-Mo steels intensively depends on pores structure, densification, diffusion of alloying elements, contact area between particles (sinter necks), microstructural homogeneity, and type of applied load. Also, knowing about element distribution in PM parts to evaluate what places are good for crack growth, nucleation and coalescenc is important. In this investigation, fracture surfaces and crack growth mechanism for element distribution environments of cracks were studied under the three point bending (TPB) test. In this work, crack growth mechanism in Cr-Mo PM parts with three different densities (6.7, 7 and 7.2 g/cm3), were evaluated accurately. Crack walk occurred in some places that had more alloying elements, particularity molybdenum. In addition, crack route was obtained from among the sharpened porosities and martensite/bainite structures.
S.s. Sayyedain, H.r. Salimijazi, M.r. Toroghinejad, F. Karimzadeh.,
Volume 33, Issue 1 (7-2014)
Abstract
Due to their superior properties such as high specific strength, high creep resistance and high strength at elevated temperatures, aluminum composites reinforced with alumina nano particles are widely used for advanced purposes such as aerospace and auto industries. Lack of an appropriate welding process limits their applications. Transient liquid phase (TLP) bonding is one of the state-of-the-art joining processes. It is used for welding composites and advanced materials. Microstructure and mechanical properties of TLP bonding depend on the bonding time and temperature. In the current study, the effect of bonding time on the microstructure and bonding strength of the TLP diffusion bonded of Al2O3p/Al nanocomposite was investigated. A thin layer of copper deposited by electroplating was used as an interlayer. The bonding times of 20 and 40 min were not sufficient for completing the isothermal solidification, and the bonding strengths were not satisfactory. By increasing the bonding time to 60 min at constant bonding temperature of 580 ºC, the isothermal solidification was completed and the final joint microstructure consisted of soft α-Al phase with dispersed CuAl2 precipitated particles. Decreasing the amount of brittle eutectic structures in the joint seam by increasing the bonding time was the main reason for improvement of the joint shear strength. The maximum joint shear strength was achieved at 580 ºC for 60 min which was about 85% of the shear strength of the base material.
M. Haerifar, M. Zandrahimi,
Volume 34, Issue 1 (5-2015)
Abstract
In the present study, 304 stainless steel (SS) was electrochemically plated with nanocrystalline Mn-Cu alloy coatings from a bath containing ammonium sulfate. The effects of current density on the microstructure, crystallographic structure, and chemical composition of the deposits were studied. The results showed that at low current densities, discontinuous coatings with a large amount of Cu can be obtained. Further increase in current density resulted in amorphous, compact and heterogeneous coatings with a small amount of Cu. The presence of Cu at low contents in precipitated coatings delayed the phase transformation of as-deposited ductile g-Mn to the brittle and hard a-Mn. However, the results did not show any specific changes in the grain size of the coatings with variation of current densities.
M.r. Dehnavi, B. Niroumand, F. Ashrafizadeh,
Volume 34, Issue 1 (5-2015)
Abstract
Effects of discontinuous ultrasonic treatment on the microstructure, nanoparticle distribution, and mechanical properties of cast Al413-SiCnp nanocomposites were studied. The results showed that discontinuous ultrasonic treatment was more effective in improving the mechanical properties of the cast nanocomposites than the equally timed continuous treatment. The yield and ultimate tensile strengths of Al413-2%SiCnp nanocomposites discontinuously treated for two 20 minute periods increased by about 126% and 100% compared to those of the monolithic sample, respectively. These improvements were about 107% and 94% for the nanocomposites continuously treated for a single 40 minute period. The improvement in the mechanical properties was associated with severe refinement of the microstructure, removal of the remaining gas layers on the particles surfaces, more effective fragmentation of the remaining agglomerates as well as improved wettability and distribution of the reinforcing particles during the first stage of solidification.
A. Samadi, M. Ghayebloo ,
Volume 34, Issue 2 (7-2015)
Abstract
To evaluate the effect of inoculant addition on functionally graded microstructure of centrifugally cast Al-Mg2Si composites, two cylinders of Al-13.8 wt.% Mg2Si with and without the addition of 1 wt.% Al-5Ti-B inoculant were cast in a vertical centrifugal casting machine. The chemical composition, microstructures and microstructural phases of the different radial sections of the cast cylinders were studied using induction coupled plasma (ICP) method, optical/scanning electron microscopes, and X-ray diffractometry, respectively. The results showed that in the inoculant content cylinder, owing to the prevailing thermal regime as well as the specific mode of eutectic solidification in this composite, the titanium and boron compounds were segregated towards the middle layer of the cylinder and caused the formation of primary Mg2Si particles and non-eutectic Al () in this layer. In addition, due to the effect of centrifugal force during solidification, a higher volume fraction of the light primary Mg2Si particles, according to Stocks law, was segregated towards the inner layer of the cast cylinders.
A. Shirali, A. Honarbakhsh Raouf , S. Bazzaz Bonabi,
Volume 34, Issue 2 (7-2015)
Abstract
Certain amount of retained austenite can increase ductility of steels because of the TRIP phenomenon during plastic deformation. One method for achieving this is partitioning of carbon into austenite to stabilize it at room temperature. The quenching and partitioning (Q&P) heat treatment leads to a microstructure consisting of martensite and stabilized retained austenite between martensite plates, which provides a better combination of strength and ductility. In this study, the effect of parameters of Q&P process (quenching temperature, partitioning temperature and partitioning time) on the microstructure and retained austenite volume fraction of a low alloy medium carbon steel was investigated. The results showed that the high increase in partitioning time causes the disappearance of martensite blades and reduction of austenite volume fraction. However, increasing
of partitioning temperature made the retained austenite films become thicker and its volume fraction increase. On the other hand, by increasing the quenching temperature, carbon content of retained austenite increased sharply.
M. Jafarian, M. Paidar, M. Jafarian,
Volume 35, Issue 1 (6-2016)
Abstract
In this study, microstructure and mechanical properties of diffusion joints between 5754, 6061 and 7039 aluminum alloys and AZ31 magnesium alloy were investigated. Diffusion joints were done between the alloys at 440 °C, for duration of 60minutes, at 29 MPa pressure and under 1×10-4 torr vacuum. The interface of joints was studied using optical (OM) and scanning electron microscopy (SEM) equipped with EDS analysis and the line scan. According to the results of EDS analysis, the presence of intermetallic compounds including Al12Mg17, Al3Mg2 and their mixture was observed at the diffusion zone. Also, according to the results of the line scan, the hardness value of aluminum alloys has a considerable effect on diffusion of the magnesium atoms toward aluminum alloy and the greatest diffusion of magnesium was observed when 6061 aluminum alloy was used. More diffusion resulted in a stronger bond between atoms of magnesium and aluminum, and maximum strength of approximately 42 MPa was obtained when 6061 aluminum alloy was used.
S. Riahi, B. Niroumand,
Volume 35, Issue 2 (9-2016)
Abstract
Preliminary results of a research on the effects of microstructure and surface roughness of a hypoeutectic cast iron on its wetting angle are presented in this article. For this purpose, molten cast iron was solidified at different cooling rates to produce two samples of the same composition, i.e. a gray cast iron with A type flake graphite and a white cast iron. Two samples were then prepared in polished, electroetched (four different stages) and mechanically abraded (four different stages) conditions and their wetting angles were measured after evaluating their roughness profile. Maximum and minimum wetting angles were observed on white cast iron surfaces roughened with 80 and 800 sand papers which were equal to 42 and 13 degrees, respectively.Wetting angles of electroetched white cast iron surfaces varied between 25 and 31 degrees by varying surface roughness. Maximum and minimum wetting angles on the surface of gray cast iron were obtained in stage one (40 degree) and stage three (25 degree) of electroetching, respectively. Wetting angles on mechanically abraded surfaces of this sample varied between 27 and 31 degrees. Then, the surface roughness factor and the solid fraction in contact with water were calculated using Wenzel equation and Cassie Baxter equation, respectively, and Wenzel and Cassie-Baxter wetting angles of the surfaces were calculated and were compared with their corresponding measured wetting angles. The results indicated that the surface microstructure and the type of constituents present at the surface, surface-roughening method and surface-roughness value influence the cast iron surface wettability, and it is possible to modify metal wetting angle by modification of its structure, surface-roughness method and surface-roughness value. It was also shown that in gray cast iron, the wetting behavior of the electroetched surfaces followed Cassie-Baxter equation in the first and second stages of electroetching and followed Wenzel equation at higher surface roughness (third and fourth stages of electroetching). In all stages of mechanically abrading, the surface of this sample followed Wenzel equation. The wetting behavior of the white cast iron followed Wenzel equation in all electroetching stages. In mechanically abraded conditions, the white cast iron wettability was variable and depended on the surface roughness.
S. S. Seyyed Afghahi, M. Jafarian, M. Salehi,
Volume 35, Issue 3 (12-2016)
Abstract
In this research, investigation of the microstructure and magnetic properties of doped barium hexaferrite with cobalt, chromium and tin with BaCoxCrxSnxFe12-3xO19 (x=0.3,0.5) formula, was performed using solid state method. Phase and structural investigation by X-ray Diffraction (XRD) and Fourier Transform Infrared (FTIR) Spectroscopy respectively, confirmed the formation of barium hexaferrites single phase without the presence of non-magnetic secondary phase after heat treatment for 5 h at temperature of 1000 °C. Also, according to scanning electron microscopy (SEM) images, morphology of particles was perfectly hexagonal with average particle size 200-250 nm. Based on magnetic parameters measured by Vibrating Sample Magnetometer (VSM), both samples were soft magnetic and the highest saturation magnetization was obtained for the sample with composition of BaCo0.3Cr0.3Sn0.3Fe11.1O19. The values of saturation magnetization (Ms) and the coercivity (Hc) were 42.21 emu/g and 656 Oe respectively for this compound.
Seyed M. Ahl Sarmadi, M. Shamanian, H. Edris, M. Atapoor, A. Behjat, M. Mohtadi Bonab, J. Szpunar,
Volume 36, Issue 1 (6-2017)
Abstract
Super duplex stainless steel is a kind of duplex stainless steel that has pitting resistant equivalent number over than 40. Unified Numbering System (UNS) S32750 is a common super duplex stainless stee, that is mostly applied in oil and gas refinery industries, because of its proper corrosion-resistant properties . Therefore, joining of these steels by welding is very important, but the greatest problem in this regard is the corrosion and decrease in mechanical properties after welding.. In this research, UNS S32750has been joined by friction stir welding method. The tool being used in this research was a WC with 16mm shoulder diameter, 5 mm pin diameter, and 1.9 mm height. X-ray diffraction showed that harmful phases, such as sigma or chi have not been formed. Microstructure study indicated that grain size in the stir zone has decreased. Vickers Hardness Test Method has been applied on welded samples. Moderate microhardness of base metal was 285 Vickers but, the microhardness increased in the stir zone to 360 Vickers, because of decreasing the grain size. The cyclic polarization determined that potential and corrosion current of joint metal by friction stir welding method was similar to base metal. Also, it was revealed that ferrite percentage in the stir zone doesn't decrease very much because the friction stir welding heat input is very low and the colding rate is very high.
S. E. Mousavi, M. Meratian, A. Rezaeian,
Volume 36, Issue 4 (3-2018)
Abstract
Equal Channel Angular Pressing (ECAP) is currently one of the most popular methods for fabricating Ultra-Fine Grained (UFG) materials. In this study, mechanical properties of the 60-40 two phase brass processed were evaluated by ECAP. The samples were repeatedly ECAP-ed to strains as high as 2 at a temperature of 350 ◦C using route C. The microstructure of the samples showed that small grains were formed in the boundaries which indicates the occurrence of recrystallization in different passes. Observation of slip trace in the microstructure of the samples showed that even in such alloy with a low-stacking fault energy, dislocations slip trigger the deformation. Investigation of mechanical properties showed that with increasing the number of passes, tensile strength, microhardness and ducility improved at the same time.
M. Rajabi, M. Shahmiri, M. Ghanbari,
Volume 37, Issue 4 (3-2019)
Abstract
In this study, the effects of boron (B) and zirconium (Zr) on the microstructure and mechanical properties of Fe3Al-based alloys were investigated. Cylindrical samples were produced using a vacuum induction melting furnace (VIM); consequently, the melt was cast into a metallic mold. The microstructure, phase identification, tensile and compressive mechanical properties and fractography of the samples were investigated. Upon microstructural observation, it was found that the alloys microstucture was denderitic and the precipitated phases were mostly present between interdendritic regions. Addition of B and Zr to the alloys resulted in the formation of boride precipitates and Laves phases. The results, therefore, showed that Zr had the most pronounced effect on the mechanical properties because of the formation of Laves phases. Fractographic studies of alloys also revealed that the brittle fracture was dominant between the samples.
B. Pourbahari, H. Mirzadeh, M. Emamy,
Volume 37, Issue 4 (3-2019)
Abstract
Microstructural evolutions during the high-temperature annealing of Mg alloys containing Al and Gd and after the extrusion process were evaluated and compared to those of the AZ61 alloy. It was revealed that during exposure at the elevated temperatures, the presence of (Mg,Al)3Gd phase, in the form of fine and dispersed particles in the matrix after the extrusion process, could be favorable for the inhibition of grain growth. It was also found that the Al2Gd particles could not effectively retard the coarsening of grains. On the other hand, the grain growth of AZ61 alloy was found to be problematic, which was related to the dissolution of the Mg17Al12 intermetallic phase at temperatures higher than 300°C. In the Mg alloys containing both Al and Gd elements, the increased thermal stability was observed, which was ascribed to the rise of the melting temperature. Finally, some abnormal grain growth was observed in the presence of Al2Gd phase, which was attributed to the nonuniform pinning of grain boundaries by this intermetallic compound.
M. Barjesteh, K. Zangeneh Madar, S. M. Abbasi, K. Shirvani,
Volume 38, Issue 2 (9-2019)
Abstract
In this study, the effect of platinum-aluminide coating parameters on surface roughness of nickel-based superalloy Rene®80 was evaluated. For this purpose, different thicknesses of Pt-layer (2, 4, 6 and 8µm) were plated on the Samples. Then diffusion aluminide coating in two types, high tempeature-low activity and low temperature-high activity was performed. The results of structural investigations by scanning electron microscope and X-Ray diffraction indicated a three-zone structure of coating in all thicknesses of platinum layer, as well as in the two methods of aluminizing. Surface roughness of coatings was measured in three steps: 1-after Pt plating, 2-after Pt diffusion, and 3-after aluminizing and final aging. The results showed that the thickness of Pt and the final thickness of the coating directly affected the surface roughness. The minimum surface roughness was created by high temperature low activity with 2µ of Pt-layer (2.6μm) and the maximum of surface roughness was obtained in low-temperature high activity with 8µ of the Pt-layer (8.8 μm).
G. R. Faghani, A. R. Khajeh-Amiri,
Volume 38, Issue 4 (1-2020)
Abstract
Due to special properties such as low density, high strength and high corrosion resistance Ti-6Al-4V alloy has been used extensively in various industries, especially in the aerospace aspects. However the major problem of this alloy is its poor tribological properties under relatively high loads. In the present study, in order to improve the tribological properties of mentioned alloy, chromium particles were added to Ti-6Al-4V layers in the nitrogen-containing atmosphere during the Tungsten Inert Gas (TIG) welding process. Microstructural investigations using optical microscopy, X-ray diffraction analysis and scanning electron microscopy, proved the formation of TiN, TiCr2 and Cr2N particles in the matrix of hard titanium phase. The hardness of TIG alloyed layer increased to 1000 HV0.3 which was 4 times higher than that of the base alloy. Moreover, the wear rate of TIG alloyed samples with chromium and nitrogen under 30N load and distance of 1000 m was 5.9 times lower than that of the bare Ti-6Al-4V alloy.
F. Shahriari Nogorani, M. Afari, M. A. Taghipoor, A. Atefi,
Volume 39, Issue 1 (5-2020)
Abstract
Practical applications of thermal barrier coatings with aluminide bond-coats are limited due to oxide scale spallation of the aluminide coating under applied thermal stresses. Considering the positive effects of oxygen-active elements or their oxides on the high temperature oxidation behavior, in this research zirconia was introduced into an aluminide coating. For this purpose, a Watts type bath was used to electroplate a layer of Ni-ZrO2 composite on a Ni-based substrate. Aluminizing was performed using the conventional two-step process at 760 and 1080 °C. Microstructural characterization of coatings in the as-coated conditions and after cyclic oxidation via 5-hour cycles at 1050 °C was performed using electron microscopy, energy dispersive spectroscopy and X-ray diffractometry. The results showed that the general three-zone microstructure of the simple high activity aluminide coatings develops below the pre-deposited nickel-zirconia layer and latter converts to a nearly un-alloyed porous NiAl. In spite of its porous surface layer, the zirconia modified coating has a higher oxidation resistance than the unmodified aluminide coating.
