Showing 10 results for Plasma
A. Sadough - Vanini,
Volume 22, Issue 1 (7-2003)
Abstract
An analysis of the demands of ULSI and GSI technologies shows the necessity of multi-layer devices to reduction of signal transmission delay time. This reduction is realized by using a better conductor metal, such as Cu and a surrounding insulator with low capacity than actually used, such as Dow Cyclotene 3022. In this paper, the results of evaporated and sputtered Cu to Dow Cyclotene 3022 were studied. After presentation of interfacial reaction that causes adherence, the methods of enhanced adherence as surface modification of polymer by nitrogen plasma have been investigated.
Keywords: Metalization, Cyclotene, Adherence, Plasma, Multi-layer
E. Sadri, F. Ashrafizadeh, M. Ramazani,
Volume 32, Issue 2 (12-2013)
Abstract
In plasma sprayed nanostructured composite coatings with ceramic matrix, the feedstock must consist of nanoparticles of appropriate specifications. In this research, the procedure for production of Cr2O3-Ag agglomerated nanostructured composite powder to produce comosite coatings has been investigated. Nanopowders of Cr2O3 with 0, 2, 5, and 10 volume percentages of silver were dispersed to obtain a homogeneous aqueous dispersion appropriate for spray drying process. In the second stage, Cr2O3-Ag composite powders were produced by agglomeration process. The nanostructured composite powders were, then, used in the atmospheric plasma spray (APS) process to deposit a series of composite coatings for evaluation. The composite powders, with a granulated morphology, had uniform distribution of silver in a ceramic matrix and the coatings were composed of nanoparticles and particles of nano-sized crystallites. Experimental results indicated that presence of nanoparticle zones within the microstructure led to non-uniform porosities formed between splats and these zones. Furthermore, use of nanopowders in the feedstock caused a reduction in lamellae thickness of plasma sprayed coatings.
S. Bassaki, F. Golestani Fard, R. Naghizadeh, M. Rashidzadeh,
Volume 34, Issue 3 (12-2015)
Abstract
Titanium dioxide-nickel oxide porous coatings were synthesized by Plasma Electrolytic Oxidation (PEO)/ ElectroPhoretic Deposition (EPD) in one step and within a short time. The main purpose of this research was to increase photocatalytic activity of titanium oxide by increasing surface area and coupling of titanium oxide with nickel oxide. Applied voltage effects on phase structure, surface morphology and photocatalytic efficiency of coatings were studied. Phase structure and surface morphology of the synthesized catalysts were investigated by XRD and SEM, respectively. Photocatalytic efficiency of the samples was studied through measuring the decomposition rate of 4-chlorophenol. The results showed that the coatings mainly consisted of anatase and nickel oxide phases whose amounts in coatings increased with the voltage. There was an enhancement of the photocatalytic efficiency in TiO2/NiO composite coatings compared with TiO2 coatings. Besides, there was an optimum amount of NiO to reach maximum photocatalytic efficiently.
M. Rezazadeh, R. Emadi, A. Saatchi, A. Ghasemi, M. Rezaeinia,
Volume 35, Issue 3 (12-2016)
Abstract
Simultaneous application of mechanical pressure and electrical charge on powder samples in spark plasma sintering process, has resulted in a sample with a density close to the theory. In the present study, a thermal-electrical-mechanical coupled finite element model of spark plasma sintering system using multi-objective optimization algorithm is proposed to optimize the mold variable. The simulation performed for Si3N4-SiO2 (1:1 mol) specimen has good agreement with the experimental results. Multi-objective genetic algorithms was used for optimization of mold design in order to maximize the temperature of sample core and minimize the mises stress in the mold. The results show that the optimized dimensions cause 8% increase in sample temperature and about 18% decrease in temperature difference between mold surface and sample core. This leads to better uniformity in the porosity distribution of final sample.
G. Kafili, B. Movahedi, M. Milani,
Volume 36, Issue 3 (11-2017)
Abstract
In this study, Spark Plasma Sintering (SPS) of both slip casted and powder specimens of alumina/ yttria core-shell nanocomposite were utilized for fabricating transparent Yttrium Aluminum Garnet (YAG) ceramics. Phase evolution, optical transmittance and the microstructure of sintered samples were compared. In slip casting process, Dolapix CE64 was used as a dispersant for preparing the stable aqueous slurry of this nanocomposite powder. The effect of Dolapix concentration and pH value on the stability of the suspension was described, and the viscosity diagrams were investigated at different pH value and different weight percents of Dolapix. The rheological behavior of the nanocomposite powder slipped at 60-70 wt% solid loading was studied by measuring their viscosity and shear stress as a function of shear rate of the slurry. The results showed that, the suspension has a minimum viscosity at pH of 10 by addition of 2.5 wt% Dolapix. Also, the slurry with solid loading of 60 wt% showed the Newtonian behavior and this rheological behavior was preserved even above this solid loading values. Slip casting technique caused the uniform size and pores distribution as well as eliminating large pores in the green body. Consequently, transparent YAG ceramic with 60% optical transmittance was achieved after SPS process of slip casted green body which was much higher than that of nanocomposite powder, i.e. about 30% at the same sintering conditions.
A. Habibi, S.m. Mousavi Khoie, F. Mahboubi,
Volume 37, Issue 2 (9-2018)
Abstract
By using cathodic plasma electrolysis, a thin film of diamond-like carbon and carbyne was produced on the nickel surface. The ethanolic solution at different concentrations of 15, 30 and 50 vol% was used as the electrolyte; the produced carbon film was studied by using glow discharge optical emission spectroscopy, scanning electron microscopy, optical profilometer, and surface enhanced Raman scattering. The results proved the coating formation of 40-60 nm thick carbon materials on the nickel surface. The intensity ratio of carbyne band to the amorphous carbon structure band in the Raman spectroscopy was decreased from 1.o4 to 0.32 by an increase in ethanol concentration; this was related to the reduction at the carbyne and the increase of the diamond-like carbon content in the produced film. Also, the study of the samples surface showed an increase in the surface roughness from 520 to 750 nm by enhancing the ethanol concentration.
M. Toorani Farani,
Volume 39, Issue 1 (5-2020)
Abstract
In this study, Plasma Electrolytic Oxidation (PEO) at three frequencies of 500, 1000 and 3000 Hz was applied on Mg surface and the effect of PEO surface preparation on protective behavior of three types of epoxy, fusion bond epoxy (FBE) and polyurethane coatings was investigated. The microstructural and protective properties of PEO coatings were studied by SEM, potentiodynamic polarization and electrochemical impedance spectroscopy (EIS). The results showed that the coating formed at frequency of 3000 Hz had smaller pore size and better protection properties. EIS test in 3.5 Wt.% NaCl solution was also used to investigate the protective behavior of the two-layered coatings. The results showed that PEO process had a favorable effect on the protective behavior of the polymer layers. Moreover, the best protection behavior was related to the PEO/FBE coating system.
S. Masoomi Ganjgah , M. Abbasi,
Volume 39, Issue 4 (2-2021)
Abstract
This study aims at investigating changes in microstructure and strength of W alloy and Cu bimetals with varying spark plasma sintering (SPS) temperature and percentage of copper in W-Cu-Ni alloy. After SPS of W (12 wt%)-Cu (14 wt%)-Ni (3 wt%) alloy powder into consolidated discs at 1350 ° C, they were spark plasma sintered to copper discs at various temperatures. Assessment of the interface microstructure and shear strength was performed by field emission scanning electron microscpe (FESEM) and shear strength test, respectively. Results indicated SPS is successful in forming a perfect metallic bond with monolithic interface and high shear strength of about 45 MPa in Cu/W-12Cu-3Ni bimetal that is extra high quality and not reported in previous investigations.
S. Shahzamani, M. R. Toroghinejad, A. Asharfi,
Volume 40, Issue 2 (9-2021)
Abstract
In this study, Al/Al2O3 composite was produced by accumulative roll bonding (ARB) process coupled with the plasma electrolytic oxidation (PEO) process. The alumina was grown on Al sheets by electrolyte technique with three different thicknesses (10, 20, and 40 µm). The results showed that incorporation of alumina up to 3.22 vol.% in aluminum matrix enhanced the yield and tensile strength of the composite, whereas increasing the amount of alumina up to 6.25 vol.% deteriorated the tensile properties. In the last part, a serial sectioning process was employed to develop a three-dimensional (3D) representation of the microstructure of Al2O3 particles reinforced Al composite for visualization and finite-element modeling (FEM).
R. Zarei, E. Mohammadsharifi, M. R. Loghman, M. Ramazani, Kh. Zamani,
Volume 41, Issue 1 (8-2022)
Abstract
The present research has examined the effect of adding Si3N4 on the mechanical and structural properties of NiCrAlY alloy. The structural and mechanical properties of the manufactured samples were characterized by SEM, XRD, micro-hardness evaluation and pin on disk wear test. Various concentrations of Si3N4 powder (1, 3, and 5 wt.%) were mixed with NiCrAlY powder using a mechanical ball mill. Next, the mixtures were sintered at 1100 °C using the spark plasma sintering (SPS) technique. The XRD patterns indicated that the samples were composed of two phases of solid solution γ-Ni(Cr) and intermetallic compounds β-NiAl. The results of micro-hardness measurements showed that adding 1% Si3N4 to NiCrAlY enhanced the hardness from 418 to 614 HV. However, with an increase in the Si3N4 content from 1 to 5 wt%, the hardness diminished from 614 to 543 HV, and by Adding Si3N4 to the NiCrAlY, its tribological properties were significantly improved.
