Showing 19 results for Process
M. Oliazadeh, M. Noaparast and R. Dehghan Simakani,
Volume 21, Issue 2 (1-2003)
Abstract
Application of gravity and magnetic separation methods to upgrade low grade Manganese ores from Venaj Mine has been reported elsewhere. This paper discusses the results of flotation tests, as well as combination of flotation and magnetic method to concentrate fine particles (less than 150 microns) of manganese ore. Results obtained from various direct and reverse flotation tests, using different types of reagents, indicated that manganese fines cannot easily be concentrated by flotation.
In this investigation, combination of direct flotation and magnetic separation for fine particles (finer than 150 microns) with 8.36% Mn, 34.11% SiO2, 23.05% Fe2O3 yielded a manganese concentrate with 26.78% Mn, 11.64% SiO2, 20.37% Fe2O3 and 56% recovery. Desliming 10-15 micron particles prior to flotation tests improved product quality and the recovery.
Keywords: Mineral Processing, Flotation, Manganese, Vanarj Mine
F. Torkamani Azar and M. Zanjani,
Volume 22, Issue 1 (7-2003)
Abstract
Recently, image processing technique and robotic vision are widely applied in fault detection of industrial products as well as document reading. In order to compare the captured images from the target, it is necessary to prepare a perfect image, then matching should be applied. A preprocessing must therefore, be done to correct the samples’ and or camera’s movement which can occur during the capturing of images. The Radon Transform technique is applied in this study which is inherently invariant to any movement, such as dislocation and rotation which leads to scale changing. According to this technique, simple methods are proposed to determine the degree of movement. Results of computer simulation show the priority of the proposed
method to other techniques. The accuracy of the proposed algorithm is less than 0.1 degree and is applicable to different segments such as texts, tables, drawings, …, which are prepared in different writing languages by different devices such as digital camera, scanner, fax, and printer.
Keywords: Image processing, Image matching, Radon Transform, Skew detection documents, Computer application in industry.
H. Moslemi Naeini, M. Maerefat and M. Soltanpour,
Volume 22, Issue 1 (7-2003)
Abstract
In hot forming process, the workpiece undergoes plastic deformation at high temperature and the microstructure of the workpiece changes according to the plastic deformation. These changes affect the mechanical properties of workpiece. In order to optimize this process, both the plastic deformation of workpiece and its microstructural changes should be taken into consideration. Since material behaviors at elevated temperatures are usually rate-sensitive, the analysis of the hot forming processes requires a thermo-viscoplastic model. In this paper, by coupling the flow stress prediction model developed with finite element analysis of thermo-viscoplastic of the hot upsetting process, temperature, strain rate, flow stress distributions and geometry of the workpiece at each time step can be calculated. At each time step, the strain rate and temperature at each element are obtained. From these values and the history of deformation, the changes in microstructure and flow stress can be determined.
Keywords: Hot forming, Process, Finite element analysis, Flow stress, Microstructure, Hot upsetting process
R. Mozaffarinia, F. Ashrafizadeh, M. A. Golozar,
Volume 22, Issue 2 (1-2004)
Abstract
The purpose of this work was to production of ceramic thin films by using of Sol-Gel process. For this purpose deposition of SiO2 on substrates of soda-lime glasses has been carried out. Coating treatments on prepared specimen were conducted in a Sol solution by means of dipping at various times. After drying and performing appropriate heat treatment on each sample, the thickness of coated layer was measured by means of roughness method. Some of the specimens were also exposed to heat and chemical environment to evaluate the coating resistance in such media. SEM examination and EDAX and XRD analysis of coating layers was also conducted on some samples.
The results indicated that by Sol-Gel method, it is easily possible to achieve thin layers in the scale of one hundredth micron meter. Any change of the thickness layer on the surface is negligible and the quality of the coating is excellent. Also, experiments indicated that deposited coatings by Sol-Gel process, are stable and give enough durability in various environments.
K. Farmanesh and A. Najafi-Zadeh,
Volume 23, Issue 1 (7-2004)
Abstract
Among the titanium alloys, Ti-6Al-4V is the most widely used. In the present work, the uniaxial hot compressive behavior of Ti-6Al-4V has been investigated under constant strain rates. A series of dilatometery experiments were carried out to determine the transformation temperatures at different cooling rates. Specimens were homogenized at 1050 °C for 10 minutes followed by fast cooling to different straining temperatures from 1050 to 850°C. The cooling rate was chosen fast enough to prevent high temperature transformation during cooling. A series of isothermal compression tests were conducted at different temperatures of 850, 900, 950, 1000, 1050°C at constant true strain rates of 0.1, 0.01 and 0.001 s-1, respectively. Samples were uniaxialy compressed to a true strain of 0.55 followed by water quenching to room temperature. The apparent activation energy for compression in two phase regions was calculated at 840 KJmol-1. The partial globularization of a-phase was observed in the specimens deformed at low strain rates and at temperatures near the transformation zone followed by annealing.
Seyyed Jalal Hemmati, M.a. Niazi, M. Maarefat, and R. Naghdabadi,
Volume 24, Issue 2 (1-2006)
Abstract
Flame bending process is one of the forming processes of steel plates. During this process, plate is formed with heating by gas torch flame followed by controlled cooling along specified paths. Considering simple tools used in the process, it is a popular and economical forming method. At present, this process is manually done on the basis of skilled technician’s
experience. Experimental and non-automated procedures decrease productivity of the process. In this paper, a method is proposed for simulation of material deformation. Regarding the physics of the process, large deformation thermoelastic-plastic analysis has been applied. In the simulations, a new analytical solution is used for thermal analysis of plate. The analytical solution along with finite element analysis of the deformation in ANSYS program is able to interpret experimental observations. The simulations show reasonable results, compared with the analytical results by other researchers and with experimental data. The method and simulation results can be used to study the process automation
H.r. Khazaki, A. Shahandeh, and S.r. Hejazi,
Volume 27, Issue 2 (1-2009)
Abstract
This research proposes a vigorous methodology based on the fuzzy set theory to improve the facility layout process. Using natural language, the fuzzy set theory is an appropriate tool for controlling complex systems such as facility planning. The closeness rating between departments in a plant depends on qualitative and quantitative factors. Some of these factors may have a greater effect on the closeness rating. Thus, analytical hierarchy process (AHP) is used to find the weight of these factors. In this paper, a computer program, called FDARC, is developed to generate quantitative activity relationship charts. These charts are used by FLAYOUT to develop the layouts. The procedure is compared with two other recent methods. Computational results are used to demonstrate the effectiveness and efficiency of the method proposed.
L. Akbarshahi, H. Sarpoolaki, H. Ghassai,
Volume 33, Issue 1 (7-2014)
Abstract
In this research according to unique properties of fused silica and Its numerous applications fused silica parts with 77% by weight solid loading formed by gel casting. Rheological behavior of the slurry and sintering conditions were optimized. Sample sintered at optimum conditions has bulk density of 1.71 g/cm3, open porosity of 18.13%, water absorption of 10.60%, linear shrinkage after firing of 3.5%, closed porosity of 1.09% and relative density of 78.80%. Its thermal expansion coefficient in range of room temperature to 1000 ◦C has been measured 0.4432×10-6 1/ . Results showed that With increasing temperature and time In addition to the increased vscous flow, Crystallization also extend. Finally sintered at high temperature and short time for an instance with the lowest overall high crystallinity and density, were found suitable
B. Hassani, F. Karimzadeh, M. Enayati, M. Borouni,
Volume 35, Issue 1 (6-2016)
Abstract
In this study, TIG welding was used to clad and repair the surface of cast AZ91C magnesium alloy. Then, friction stir processing and T6 heat treatment wrer applied on the welded region. Microhardness results showed an improvement in the mean hardness of welded zone and also FSPed zone. Increase in the mean microhardness of the welded zone after T6 heat treatment to the maximum value was also concluded. The results of wear test showed that the wear resistance of the welded area was improved. Further improvement in wear properties was obtained after friction stir processing and T6 heat treatment.
M. H. Tahmasebi, K. Raeissi, M. A. Golozar, A. Vicenzo, M. Bestetti,
Volume 35, Issue 3 (12-2016)
Abstract
In the present investigation, Mn-Ni binary nano-oxide was deposited by potentiodynamic method on stainless steel at room temperature and the effect of annealing process (at 200 oC for 6 h) on microstructure and electrochemical performance of the synthesized pseudocapacitor was studied. The results showed the significant effect of annealing process on increasing the capacitance and decreasing the charge transfer resistance of the electrode. Field Emission Scanning Electron Miscroscopy (FESEM) images depicted interconnected and random nano-flakes in the oxide film microstructure. Moreover, a partially crystallized structure consisting disorder hexagonal birnessite type phase was formed upon annealing in the deposited oxide film with about 10 %at Ni in composition. Based on the galvanostatic charge-discharge plots, the highest specific capacitance (384 F g-1) and specific energy (53 Wh kg-1) were found at specific current of 0.1 A g-1 for the annealed oxide electrode. Finally, cycle life test results at specific current of 10 A g-1 showed an excellent cyclability and an increase of about 23% in specific capacitance of synthesized pseudocapacitor after 5000 charge-discharge cycles in 1 M Na2SO4.
M. Soltani, B. Niroumand, M. Shamanian,
Volume 36, Issue 2 (9-2017)
Abstract
In this paper, the optimization of the surface composite of Mg AZ31B-carbon nanotub(CNT) via friction stir processing was investigated. Then, the most effective process parameters such as transverse speed, rotational speed, CNT weight percent and welding passes were studied by Response Surface Methodology (RSM) design of experiment. The specimens were also characterized by micro-hardness, tensile, shear punch and pin on disk dry sliding wear tests. The optimization results of hardness and weight reduction responses showed that the best conditions would be achievable with a transverse speed of 24 mm/min, rotational speed of 660 rpm, 4wt.% CNT and 3 welding passes. Moreover, fracture analysis of the surfaces proved a uniform distribution of CNTs in the matrix resulted in higher tensile and shear strength.
M. Zadali Mohammad Kotiyani, Khalil Ranjbar,
Volume 38, Issue 1 (6-2019)
Abstract
In this research, an in-situ hybrid composite reinforced by Al3Zr and Al3Ti aluminide particles was fabricated by friction stir processing (FSP). The base metal was in the form of a rolled Al 3003-H14 alloy sheet, and zirconium and titanium metal powders were used as the reinforcements. Six passes of FSP were applied. Tensile strength and hardness of the base metal, as well as FSPed samples before and after applying heat treatment, were determined. Microstructural examinations were performed using optical and scanning electron microcopy (SEM), and phase formation was identified by X-Ray diffraction. Microstructural examination revealed that by applying FSP, the prior large and elongated grains of the base metal were converted to the fine and equiaxed grains. It was also observed that chemical reactions occurred at the interface between the aluminum matrix and the metallic powders, forming in-situ aluminides of Al3Zr and Al3Ti. The post annealing heat treatment activated these solid state chemical reactions and more aluminides were formed. It was also found that the heat treated hybrid composite possessed the highest tensile strength and hardness values. The tensile strength in such samples reached 195 MPa, as compared to 110 MPa of the base metal.
M. H. Musazadeh, R. Vafaei, E. Mohammad Sharifi, Kh. Farmanesh,
Volume 38, Issue 3 (12-2019)
Abstract
Finite element (FE) simulations in conjunction with experimental analysis were carried out to characterize the deformation behavior of an AISI 321 austenitic stainless steel (ASS) during cold pilgering process. The effect of process parameters including feed rate (4 and 8 mm) and turn angle (15, 30 and 60°) on damage build-up were also evaluated. The Johnson-cook model was used to simulate the flow behavior of material. By considering compressive stresses, a new revised Latham-Cockcraft damage was calculated and used to determine the optimum process parameters. It was found that the radial and hoop strains in all friction conditions were compressive, while the axial strains were observed to be tensile. The amount of strain (whether it is compressive or tensile strain) was also higher on the outside of the tube compared to its inside. By considering fatigue cycles of a tube element during the process, the feed rate of 8mm, turn angle of 60° and the lowest coefficient of friction were determined as optimum parameters.
G. R. Faghani, A. R. Khajeh-Amiri,
Volume 38, Issue 4 (1-2020)
Abstract
Due to special properties such as low density, high strength and high corrosion resistance Ti-6Al-4V alloy has been used extensively in various industries, especially in the aerospace aspects. However the major problem of this alloy is its poor tribological properties under relatively high loads. In the present study, in order to improve the tribological properties of mentioned alloy, chromium particles were added to Ti-6Al-4V layers in the nitrogen-containing atmosphere during the Tungsten Inert Gas (TIG) welding process. Microstructural investigations using optical microscopy, X-ray diffraction analysis and scanning electron microscopy, proved the formation of TiN, TiCr2 and Cr2N particles in the matrix of hard titanium phase. The hardness of TIG alloyed layer increased to 1000 HV0.3 which was 4 times higher than that of the base alloy. Moreover, the wear rate of TIG alloyed samples with chromium and nitrogen under 30N load and distance of 1000 m was 5.9 times lower than that of the bare Ti-6Al-4V alloy.
S. Arjmand, M. Tavoosi,
Volume 39, Issue 3 (12-2020)
Abstract
The present work aims to modify surface properties of pure Ti by development of Ti-Al-N intermetallic composite coatings. In this regard, tungsten inert gas (TIG) cladding process was carried out using Al 1100 as filler rod with Ar and Ar+N2 as shielding gases. Phase and structure of the samples were investigated by X-ray diffraction (XRD) technique, optical microscopy (OM) and scanning electron microscopy (SEM). Hardness values and corrosion behavior of the obtained coatings were also compared using Vickers microhardness tester and potentiostat, respectively. The results showed that composite structure containing Al3Ti, Ti3Al2N2 and Ti3Al intermetallic compounds could be formed on the surface of pure Ti. Amounts of brittle phases and welding defects at the titanium-coating interface were least by welding under pure Ar shielding. Despite the increasing amount of structural defects such as porosity and non-uniformity under Ar+N2 shielding, the prepared coatings had higher hardness (more than 100 HV) and corrosion resistance (more than twice) compared with those obtained under Ar shielding.
S. Arjmand, G. H. Akbari, G. R. Khayati,
Volume 39, Issue 4 (2-2021)
Abstract
The purpose of the present work is to investigate the influence of the number of weld-passes on microstructure, hardness and residual stresses of composite coatings composed of Ti-Al-Si intermetallic compounds. In this regard, surface coating of pure Ti was carried out using one and two passes of tungsten inert gas (TIG) welding with an Al filler alloy (grade 4043). Phase and structural evaluations of the coatings were investigated by X-ray diffraction, optical and scanning electron microscopies. microhardness and residual stress values of the coatings were measured using ASTM E384-HV device and the Sin2ψ method, respectively. The results showed that as the number of welding passes increased or the dilution ratio decreased, the volume fraction of Ti5Si3-Al3Ti intermetallic phases within the fusion zone increased and the volume fraction of martensite phase in the heat affected zone decreased. As a result, the average hardness value of the coating increased to be about 130 % compared to that of the pure Ti substrate. The tensile residual stresses at the center line of fusion zone were 165 ± 30 and 210 ± 35 MPa for the coatings prepared in one and two welding passes, respectively.
R. Amirarsalani, M. Morakabati, R. Mahdavi,
Volume 40, Issue 1 (5-2021)
Abstract
In this research, the hot deformation behavior of W360 tool steel was investigated using hot compression test at 1000-1200°C and strain rates of 0.001, 0.01, 0.1, and 1 s-1. According to the results, dynamic recrystallization was found the most important restoration factor of this alloy during hot deformation. Recrystallization was enhanced with an increase in temperature and strain rate. Also, the hot working process was optimized by drawing the processing map of this steel. Microstructural images obtained from the hot compression test showed that recrystallization started at 1000°C and the strain rate of 0.01 s-1 and developed with increasing temperature and strain rate due to an increase in the stored energy and suitable regions for nucleation. The results of drawing the processing map showed that the best hot deformation region was the temperature range of 1050-1150°C and strain rates of 0.1-1 s-1.
M. Salehi, M. Eskandari, M. Yeganeh,
Volume 40, Issue 2 (9-2021)
Abstract
In this study, microstructural changes in the thermomechanical processing and its effect on the corrosion behavior of 321 austenitic stainless steel were investigated. EDS analysis and optical microscopy were used to identify precipitates and microstructure, respectively. To evaluate the corrosion properties, potentiodynamic polarization test and electrochemical impedance spectroscopy were performed. First, the as-received sample was subjected to cold rolling with a 90% thickness reduction at liquid nitrogen temperature, and then annealing was performed at temperatures of 750, 850, and 1050 °C for 10 min. The results showed that severe cold rolling slightly improved the corrosion properties and in annealed samples, the corrosion resistance increased with more uniform microstructure, more reversion of martensite phase to austenite, and reduction of grain size. Annealed samples at 850 °C and 1050 °C with polarization resistance values of 8.200 kΩ.cm2 and 3.800 kΩ.cm2 depicted the highest and lowest corrosion resistance compared to other samples, respectively.
A. Mehdikhani, H. Fallah-Arani, F. Dabir, A. Ghanbari,
Volume 41, Issue 2 (11-2022)
Abstract
In this research, the effect of hydrogen peroxide (H2O2) and benzoyl peroxide (BPO) on the structural properties, porosity, active pores, and surface area of the MOF-5 (Zn4O(BDC)3) metal-organic framework was studied. For this purpose, the metal-organic framework was synthesized by direct mixing and the molar ratios of the precursors to the ligand were modified to minimize the stoichiometric calculation error as well as the washing process to improve the properties of the synthesized MOF-5. In order to characterize the synthesized compounds and to investigate the effect of peroxides and washing process on the properties of the samples, X-ray diffraction (XRD), fourier Transform infrared spectroscopy (FTIR), and thermogravimetric/Differential scanning calorimetry (TG-DSC) analysis were performed. Structure, pore volume (1.212 cm3/g), and specific surface area (2307 m2/g) were compared to the sample synthesized with H2O2. DM-P-03 was selected as the optimal sample and prepared for thermal stability. According to TG-DSC analysis, the remaining zinc compounds in the sample were checked and the thermal stability of MOF-5 structure was confirmed up to 470°C.
