Showing 34 results for Steel
M. H. Fathi, Gh. Feizi, Sb. Moosavi, Gh. Gahanshahi, M. Salehi, A. Saatchi and V. Mortazavi,
Volume 20, Issue 1 (7-2001)
Abstract
Hydroxyapatite coatings have been used on metallic substrates in a variety of applications, including modifying the surface of human implants, bone osseointegration and biological fixation. In this paper, the effects of various kinds of metallic substrate on clinical and pathological results of in vivo tests are presented. Four kinds of endodontic implants i.e, stainless steel, cobalt base alloy, plasma sprayed hydroxyapatite coated stainless steel, plasma sprayed hydroxyapatite coated cobalt base alloy were prapared and implanted in mandibular canine of
cats. After a healing period of 4 months, investigation by SEM and histopathological interpretation and evaluation showed significant differences in tissue response and osseointegration between coated and non-coated metallic implants. It was concluded that the results were affected by the kind of metallic substrate .
Keywords: Hydroxyapatite coating, Dental endodontic implant, Osseointegration, Corrosion, Stainless steel,
Cobalt base alloy
A. Nasr-Esfahany and M.heydarzadeh Sohi,
Volume 23, Issue 2 (1-2005)
Abstract
Zinc-Nickel electrodeposits have been widely adopted for surface treatment of automobile steel sheet for high corrosion resistance. In this work the effect of pulse parameters on the Zn-Ni alloy electrodeposits was investigated. The hardness, thickness, corrosion resistance and composition of deposits thus produced were investigated. The surface topography of the deposits was also observed in SEM and results are reported. It has been shown that the thickness of the pulse electrodeposits
was almost even. The hardness in the pulse electrodeposits increased by increasing the on-time period and by decreasing the current density. It was also noticed that increasing the on-time period increases the nickel content of the deposit. Pulse electrodposits had fine structure and the structure become finer by reducung the on-time period and pulse frequency. The corrosion dehaviors of the deposits were then investigated. The results showed that the corrosion resistance of the DC electrodeposits improves in their nickel content increases. Pulse electodeposits show the same behavior, but deposits with about 13% nickel show maximum corrosion resistance.
M. Shamanian and A. Saidi,
Volume 24, Issue 1 (7-2005)
Abstract
The 25Cr-35Ni heat resistant steel has been widely used when resistance to oxidation and creep rapture at elevated temperatures is required. In this paper, the microstructural effect on the weldability of this alloy is investigated. The results of this study indicate that this steel has a perfect weldability in the as cast condition but does not possess good weldability in the aged condition. The as cast microstructure of 25Cr-35Ni steel consists of austenite matrix and a network of primary carbides, while the aged condition consists of austenite matrix and y primary and secondary carbides. The morphological change of primary
carbides and the secondary carbides precipitate formation, reducing the elongation and ductility of aged steel, should have enhanced the steel susceptibility to cracking, particularly in the area of the eutectic carbides, and hence, the reduced weldability of the steel. The cracking observed was of the intergranular type and spread along the eutectic carbides. It was found that the carbides in the as cast steel consisted of NbC and M23C6, whereas that of the aged steel also exhibited Ni16Nb6Si7 and M23C6 carbides
F. Nateghi, and A. S. Ghods,
Volume 25, Issue 2 (1-2007)
Abstract
An effective approach for strengthening masonry buildings is to apply shotcrete reinforced with mesh on the surface of the wall. It is not possible to assess the behaviour of coated walls solely using analytical approaches based on simple equations of theory of elasticity without the use of numerical methods. Unreinforcced masonry wall is modelled in this study using the finite element software “ANSYS” to assess the behavior of walls strengthened with reinforced jacket. The accuracy of the model is ensured by calibrating the model against results obtained from laboratory tests. Then the calibrated model is
generilized to model the strengthed wall and, finally, the analytical results obtained from masonry walls and strengthed walls are compared and evaluated.
D. Mostofinejad and M. Noormohamadi,
Volume 27, Issue 2 (1-2009)
Abstract
Although studies on RC beams under shear have a history record of more than 100 years, many important
issues in this context still remain that have evaded attention. The aim of the current study is to study a number of these less investigated aspects of the behavior of RC beams under shear. For this purpose, and based on the modified compression field theory, a computer program has been written to study the effects of transverse and longitudinal steel reinforcement and shear span, a/d, on the behavior of RC beams under shear. The results show that the shear capacity of the beam cannot be increased beyond an optimum amount of transverse steel ratio. This paper will try to provide a precise definition of this optimum transverse steel ratio. Another finding of the present study is that increasing tensile longitudinal steel ratio increases the amount of the optimum transverse steel ratio, while increasing a/d decreases the optimum transverse steel ratio.
J. Aghazadh Mohandesi, A. Nazari,
Volume 29, Issue 2 (12-2010)
Abstract
Charpy impact energy of functionally graded steels in the form of crack arrester configuration was investigated. Functionally graded steels which contain layers of ferrite, austenite, bainite and/or martensite could be produced by electroslag remelting. The results showed that notch tip position and the distances of notch with respect to the bainite and martensite layers significantly affect the impact energy of the specimens. Generally, the plastic deformation zone ahead of a crack in a functionally graded material depends on the position of the notch tip where according to the direction of gradient slope may increase or decrease. The closer the notch tips to the brittle phase, the smaller the impact energy of the specimen and vice versa. The effect of plastic zone size on impact energy of functionally graded steels was notionally investigated.
H. Ebrahimifar , M. Zandrahimi,
Volume 29, Issue 2 (12-2010)
Abstract
In order to increase the efficiency and working life of mettalic interconnects used in solid oxide fuel cells, protective coatings with high electrical conductivity are used. In this study, AISI 430 ferritic stainless steel was coated in a cobalt-base pack mixture by pack cementation. The effect of oxide thickness on the area specific resistance (ASR) was investigated by applying isothermal oxidation at 800 °C and non-isothermal oxidation at a temperature range of 400 – 900 ºC. Results showed that the formation of MnCo2O4 and CoCr2O4 Spinels during oxidation improved electrical conductivity. The increase of isothermal oxidation time and temperature increases the oxide thickness, and consequently the ASR increased.
M. Eshraghi Kakhki, A. Kermanpur, M. A. Golozar,
Volume 30, Issue 1 (6-2011)
Abstract
In this work, a 3D thermo-microstructural model was developed to simulate the continuous cooling of steel. The model was employed for simulation of cooling process of the gears made from a plain carbon steel (AISI 1045) and a low alloy steel (AISI 4140). Temperature-dependent heat transfer coefficients for two different quenching media were evaluated by experimental and computational methods. The effects of latent heat releases during phase transformations, temperature and phase fractions on the variation of thermo-physical properties were investigated. The present model was validated against cooling curve measurements, metallographic analysis, and hardness tests, and good agreement was found between the experimental and simulation results. This model was used to simulate the continuous cooling process and to predict the final distribution of microstructures and hardness in steel gears.
A. Fattah-Alhosseini, A. Saatchi, M.a. Golozar, K. Raeissi, B. Bavarian,
Volume 32, Issue 2 (12-2013)
Abstract
In this study, effect of potential on composition and depth profiles of passive films formed on 316L stainless steel in 0.05 M sulfuric acid has been examined using X-ray photoelectron spectroscopy (XPS). For passive film formation within the passive region, four potentials -0.2, 0.2, 0.5, and 0.8 VSCE were chosen and films were gown at each potential for 60 min. XPS analysis results showed that atomic concentration of Cr and Fe initially increase (E < 0.5 VSCE) and then decrease with potential. This decrease is due to surface dissolution of the Fe and Cr oxides. For both alloying elements, Ni and Mo, no obvious change in atomic concentration was showed. Results indicated that at higher potentials, before entering transpassive region, oxidation of Cr3+ to Cr6+ is happened.
Reza Eshghi, S.m.hadavi, V.varmazyar,
Volume 33, Issue 3 (3-2015)
Abstract
In this research, Ti-6Al-4V alloy was brazed with 410 stainless steel by three different filler metals as silver-base,
nickel-base, and titanium-base alloys. In order to obtain optimum clearance, brazing was done in three different clearances
of 0.02, 0.04 and 0.06 mm. Also, the strength and hardness of the brazing zone were investigated. The results of shear strength
showed that the brazed samples with titanium-base alloy at the clearance of 0.02 mm had the maximum strength among the
different samples which was 149.5 MPa.
H. Tavakoli, M. Soltanieh, H. Aghajani, M. Jafarpour,
Volume 34, Issue 1 (5-2015)
Abstract
This study was intended to investigate the effect of injection of aluminium into the crystallizator on type, composition and activity of inclusions in low carbon steel grade USD7. The steel is made in Zob-e-Ahan Isfahan factory and its porosities and inclusions results in the problem of rupturing during rolling process. To improve the quality of this steel, 2.4 mm diameter pure aluminum wires were injected in to the crystallizator at the rate of 2, 4, 6 or 8 m/min in certain periods and then sampling was done. The results indicated that much of the added aluminum changed to aluminum oxide slag, and the remaining part altered the chemical composition of the inclusions. Increased aluminum caused an increase in the activity of alumina and reduction in the activity of other oxides in the slag and existing inclusions in the melt. By increasing Al2O3 activity from 0.313 to 0.649, the Al2O3 formation and oxygen exclusion probability increased in the system. Scanning electron microscopy showed that without aluminium injection, most of inclusions were FeO-MnO type placed around existing porosities in the ingot. The optimum rate of aluminum injection was found to be 4 m/min.
A.h. Khosrovaninezhad, M. Shamanian, A. Rezaeian , M. Atapour,
Volume 34, Issue 2 (7-2015)
Abstract
This paper reports on the mechanical properties of the dissimilar joints between AISI 316 austenitic stainless steel and St 37 low carbon steel achieved using friction stir welding technique. The welding was carried out by means of rotational speed of 800 rpm and linear speeds of 50,100,150 mm/min. EDS and XRD techniques were employed in order to determine possible phase transformations. Tensile test, shear punch test and microhardness measurements were conducted to evaluate the mechanical properties of the joints. The results of phase investigations showed that no carbide and brittle phase were detected at the joint boundary. Also, tensile test results demonstrated that failure occurred in the St 37 base metal. According to the shear punch test, the highest ultimate shear strength and yield shear strength was achieved for the sample welded at rotational speed of 800 rpm and linear speed of 150 mm/min, while this sample showed the least elongation. In addition, the highest microhardness was measured in the stir zone of austenitic stainless steel sample welded in the above mentioned welding condition, which can be attributed to the decrease in grain size caused by recrystallization process.
M. Atapour, M.m. Dana, F. Ashrafizadeh,
Volume 34, Issue 4 (3-2016)
Abstract
In this investigation, the effect of grain size on the corrosion behavior of 304L stainless steel has been studied. Samples with grain sizes of 0.5, 3 and 12 micrometers were fabricated through formation of strain-induced martensite by 80% cold rolling of the stainless steel sheets at -15 °C and its reversion to austenite during annealing at 900 °C for 1, 5 and 180 min. The corrosion behavior of samples with different grain sizes was investigated by cyclic polarization experiments and immersion tests in 0.1 M hydrochloric acid (HCl). The polarisation tests showed no differences in uniform corrosion rates of the samples. The results of the cyclic polarisation and immersion tests showed that decreasing the grain size improved the pitting corrosion resistance from 290 mVAg/Agcl for grain size of 12 micrometers to 420 mVAg/Agcl for grain size of 0.5 micrometers.
H. Shokrvash, A. Vajd, M. Shaban Ghazani,
Volume 34, Issue 4 (3-2016)
Abstract
In the present research, an effective thermo-mechanical processing route in the temperature range of metastable austenite region (Ae3<T< Ar3) was employed to achieve ultra-fine grain size in a plain low carbon steel during integrated extrusion equal channel angular pressing. At first, the effect of preheating temperature on the strain and temperature distributions inside the deformed samples were investigated using 3D finite element simulation. According to the result of FEM simulation, the preheating temperature of 930 ˚C was selected as an appropriate temperature for fabrication of ultra-fine ferrite structure. Severe plastic deformation was then imposed on samples with the predicted preheating temperature and the results showed a great consistency with FEM simulation predictions. Optical micrographs taken from the center point of the samples showed that the ferrite grains could be refined from 32 μm to 1-3 μm by different mechanisms.
Seyed M. Ahl Sarmadi, M. Shamanian, H. Edris, M. Atapoor, A. Behjat, M. Mohtadi Bonab, J. Szpunar,
Volume 36, Issue 1 (6-2017)
Abstract
Super duplex stainless steel is a kind of duplex stainless steel that has pitting resistant equivalent number over than 40. Unified Numbering System (UNS) S32750 is a common super duplex stainless stee, that is mostly applied in oil and gas refinery industries, because of its proper corrosion-resistant properties . Therefore, joining of these steels by welding is very important, but the greatest problem in this regard is the corrosion and decrease in mechanical properties after welding.. In this research, UNS S32750has been joined by friction stir welding method. The tool being used in this research was a WC with 16mm shoulder diameter, 5 mm pin diameter, and 1.9 mm height. X-ray diffraction showed that harmful phases, such as sigma or chi have not been formed. Microstructure study indicated that grain size in the stir zone has decreased. Vickers Hardness Test Method has been applied on welded samples. Moderate microhardness of base metal was 285 Vickers but, the microhardness increased in the stir zone to 360 Vickers, because of decreasing the grain size. The cyclic polarization determined that potential and corrosion current of joint metal by friction stir welding method was similar to base metal. Also, it was revealed that ferrite percentage in the stir zone doesn't decrease very much because the friction stir welding heat input is very low and the colding rate is very high.
Kh. Farjam Hajiagha, A. R. Akbari, R. Mohammadzadeh,
Volume 36, Issue 2 (9-2017)
Abstract
In this study, the kinetics of austenite layer growth on the surface of Fe-23Cr-2.4Mo ferritic stainless steel during solution nitriding and the effects of nitrogen adding on microstructure and hardness of the steel have been investigated. Steel plates of 2 mm thick were solution-nitrided at 1200˚C under nitrogen pressure of 0.25 MPa for 2, 3, 6, 9, 12 hours. Microstructure, the thickness of austenite layer and the hardnes of the nitrided samples, were investigated by using optical microscope, X-ray Diffraction (XRD) and microhardness measurements. The results showed that during solution nitriding, nitrogen diffuses through the lattice and grain boundaries and transforms ferrite to austenite phase, with average nitrogen diffusion coefficient of 6.54×10-5 mm2s-1. The thickness of the austenite layer formed on the samples surfaces increased proportional to the square root of the nitriding time, so that after 12 hours niriding, the whole thickness of the ferritic sample with hardness of 262 HV0.1 transformed to austenite with hardness of 420 HV0.1.
Mr S. A. Razavi, Mr S. F. Ashrafizadeh,
Volume 36, Issue 2 (9-2017)
Abstract
Age hardening processes cause a wide range of changes in 17-4 PH stainless steel properties. Aging at 480ºC for 1 hour (A480-1) and aging at 620ºC for 4 hours (A620-4) are two most applicable heat treatment processes for this alloy. Not only the studies on fatigue behavior of this alloy in these two heat treatment conditions are few, but also the methods of fatigue test were mostly axial. In this study, after microstructure studies, hardness and tension tests, fatigue behavior at A480-1 and A620-4 conditions were evaluated by using a rotational bending fatigue test machine. Tension results showed that yield strength and ultimate tensile strength of A480-1 specimens were 40 percent more than A620-4 specimens. However, elongation of A620-4 specimens was 30 percent more than A480-1 specimens. Fatigue results revealed the endurance limit of aged specimens is 50 MPa more than overaged specimens. Overall results showed that A480-1 condition specimens are more resistant to fatigue than A620-4 condition specimens.
M. Poorkabirian, H. Mostaan, M. Rafiei,
Volume 36, Issue 2 (9-2017)
Abstract
In this research, dissimilar welding between 4130 low alloy steel and austenitic stainless steel 316L has been investigated using Gas Tungsten Arc Welding (GTAW). Two types of filler metals, including ERNiCr-3 and ER309L, were used for this purpose. Moreover, the joint microstructures including the weld metals, heat affected zones and interfaces were characterized by optical and Scanning Electron Microscopy (SEM). The mechanical behavior of the joint was tested by impact and tension tests. Observations by SEM showed that in impact test, the fracture is soft. In the tensile test, the welded sample by ER309L filler metal was fractured from 316L base metal, but welded specimen with ERNiCr-3 was fractured from welded zone. Also, the results showed a dendritic structure in the nickel-based weld metal. No crack was found in the cellular-dendritic microstructure of ER309L weld metal due to the existance of delta ferrite between them.
H. Chavilian, K. Farmanesh, A. Soltanipour, E. Maghsoudi,
Volume 36, Issue 3 (11-2017)
Abstract
In this research, industrial hot deformation processes was simulated for 321 austenitic stainless steel using hot compression test with the aim of acquiring technical knowledge and indigenization of stainless steel production. The obtained stress-strain curves showed the common retrieval dynamic behaviour. By microscopic studies, the main restoration mechanism during hot deformation in this steel was diagnosed as dynamic recrystallization, that due to low stacking fault energy of 321 stainless steel, this phenomenon was justified. Then, using diagrams related to real stress, real strain and strain rate, the onset point of dynamic recrystallization was determined under different conditions. Also, using the constitutive equations and Zener-Holloman parameter, hot deformation behaviour of 321 stainless steel was studied and the activation energy of hot deformation for this steel was determined as 422 (Kj/mol).
Sh. Tavakoli Dehaghi, S. Darvishi, Sh. Nemati, M. Kharaziha,
Volume 37, Issue 3 (12-2018)
Abstract
Abstract: With the advances in the development of biomaterials for tissue replacement, the attention of scientists has been focused on the improvement of clinical implant properties. In this regard, despite the appropriate properties of the stainless steel, the application of stainless steel as implants has been limited due to the weak corrosion resistivity. The purpose of this paper was preparation and characterization of hydrophobic polydimethylsiloxane (PDMS)-SiO2-CuO nanocomposite coating on the 316L stainless steel surface. The 316L stainless steel was coated by SiO2 nanoparticles (20 wt. %), CuO nanoparticles (0.5, 1 and 2 wt. %) and biocompatible PDMS. In this research, x-ray diffraction (XRD) and scanning electron microscopy (SEM) were applied to characterize the coating. Moreover, the roughness and water contact angle of the coatings consisting of various amounts of CuO nanopowder were estimated. Finally, the effects of various amounts of the CuO nanopowder on the corrosion resistivity of nanocomposite coatings were investigated. XRD patterns confirmed the presence of crystalline CuO nanoparticles on the substrate. Due to the non-crystalline nature of silica nanoparticles and the semi-crystalline PDMS polymer, no peak confirming the presence of these phases was detected on the XRD pattern of the nanocomposite coating. SEM images showed the formation of a lotus leaf-like layer on the surface of the nanocomposite coating containing 1 and 2 wt. % CuO. Moreover, water contact angle evolution revealed that while contact angle was 81 degree without CuO nanoparticles, it was enhanced to 146 degree in the presence of 1 wt. % CuO. Moreover, the corrosion study showed the nanocomposite containing 2 wt.% CuO had the best corrosion resistance, the corrosion current density of 2.1E-7 A.cm-2, and the corrosion potential of 0.22 V.