Showing 154 results for Subject: Special
M.h. Nourmohammadi, M. Movahedi, A.h. Kokabi, M. Tamizi,
Volume 9, Issue 1 (5-2023)
Abstract
The miniaturization and compaction trends in electronic equipment and the removal of lead (Pb) element from solder alloys due to environmental considerations have created a great challenge in the field of designing and developing of new solder alloys. Therefore, researchers have recently focused on composite solder alloys using reinforcing particles to improve the reliability of lead-free solders. In this research, SAC0307 solder alloys (99 wt.% Sn, 0.3 wt.% Ag, and 0.7 wt.% Cu) with different percentages of cobalt microparticles were made by the Accumulative Roll Bonding (ARB) method. Then, the effect of the particles on wettability, microstructures and mechanical characteristics of solder alloys was investigated. The lowest contact angle was 23◦in 0.2 wt.% cobalt sample. By adding cobalt to the solder matrix, the size of intermetallic compounds (IMCs), Cu6Sn5 and Ag3Sn, decreased and the percentage of eutectic phases increased. The shape of the interfacial intermetallic compounds changed from scallop to layer shape by adding cobalt, and their average thickness increased about 13-71% in composite samples. The shear strength of solders increased up to 38% by enhancement of cobalt microparticles in the solder alloy containing 0.4 wt.% cobalt; however, shear strength was decreased in the composite solder containing 1 wt.% cobalt due to the agglomeration of microparticles. The shear fracture surfaces showed that the nature of the fracture changed from ductile fracture in the form of elongated dimples to brittle fracture in the form of cleavage with the increase in the percentage of cobalt microparticles. The composite solder alloys containing 0.2-0.4 wt.% Co have the best wettability behavior and tensile shear strength.
Gh. Khalaj, A. Fadaei,
Volume 9, Issue 1 (5-2023)
Abstract
In this research, the effect of post weld heat treatment on the microstructure and mechanical properties of the three-layer explosion welding joint of austenitic steel 321-aluminum 1050-aluminum 5083 was investigated. The welded samples were heat treated at 250 and 350°C for 10000 seconds. The structure and properties were investigated using optical microscope, scanning electron microscope, microhardness measurement and shear-compressive strength. The results showed that in all conditions, the interface of aluminum 5083-aluminum 1050 was smooth and with complete continuity; However, the interface between stainless steel 321 and aluminum 1050 had a reaction layer with variable and discontinuous thickness. During the heat treatment, the thickness of the interface layer increases according to the diffusion kinetics and reaches 18.6 microns in the maximum value. With the increase of heat treatment temperature, the average concentration of aluminum in the reaction layer of the interface increased from 85% to more than 90%, but the concentration of iron decreased from 10% to less than 5%. Also, shear-compressive strength decreases from 94.6 to 56.7 MPa.
L. Gadami Domabi, S. M. Rafiaei, S. Jahanbazi Gojani,
Volume 9, Issue 1 (5-2023)
Abstract
In this paper the production of chitosan and polylactic acid polymer scaffolds containing zinc oxide particles was carried out through the 3D printer method. Zinc oxide particles were processed through combustion synthesis method. According to the XRD results, the produced oxide has a high phase purity, and the evaporation of volatile impurities and the increase of crystallinity happened via performing the calcination process. In the X-ray diffraction pattern of PLA/ZnO/Chitosan, the broad peak in the range of 10-25 degrees indicates the amorphousness of the background polymer, and with the addition of ZnO, sharp and powerful peaks have appeared in the graph. The SEM images of zinc oxide synthesized by combustion method also showed that the size of ZnO nanoparticles is approximately 50 nm, while after the calcination heat treatment, the size of the particles increased greatly and reached an average size of 130-160 nm. Finally, the microscopic images obtained from the surface of scaffolds possessing 10% zinc oxide, 5% chitosan and polylactic acid showed that by optimizing the 3D printer, ZnO particles are uniformly dispersed in PLA/Chitosan polymer field.
Ali Adelian, Khalil Ranjbar, Mohammadreza Tavakoli Shoushtari,
Volume 9, Issue 2 (8-2024)
Abstract
This research studied the effect of two-stage over aging treatmenton the pitting corrosion behavior and microstructure of the weld metals in the 17-4 precipitation hardening stainless steel. For this purpose, this steel was subjected to solution annealing heat treatment at 1035°C for one hour before welding. Then gas tungsten arc welding (GTAW) was performed using ER630 similar filler metal. Subsequently, a section of the weldment was subjected to two-stage over aging treatment. The microstructure and corrosion resistance of the weld zone after the two-stage over aging treatment were investigated and compared with the weld zone behavior in the as-weld condition. Microstructural studies showed that the two-stage over aging treatment of the weld zone led to the tempering of the martensitic, the formation of more reversed austenite, and the formation of α-ferrite. The volume fraction of austenite in the as-weld condition was approximately 7% and increased to about 30% after two-stage over aging treatment, a four-fold increase. The pitting potential (EPit) of weld metal was -18.15 mv in the as-weld condition and reached 122.54 mv after two-stage over aging treatment, which also signifies an improvement in pitting resistance. The two-stage over aging treatment also reduced the potential differences between the different parts of welding zones reducing the galvanic corrosion occurrence. The assessment of mechanical properties through impact test revealed that impact resistance after two-stage over aging treatment can be increased by about 66 % compared to as-weld condition.
Ali Khorram, Hassan Habibi, Alireza Yazdipour,
Volume 9, Issue 2 (8-2024)
Abstract
This study aimed to investigate the effect of diffusion welding parameters on the microstructural characteristics and mechanical properties of the dissimilar joint between 418 steel and Inconel 738 superalloy using Ni interlayer with a thickness of 50 µm. The experiments were performed in a vacuum furnace at three temperatures of 1000, 1050 and 1150 °C for 45, 60, 75 and 90 min under the pressure of 5 MPa.The results show that voids and non-bonded areas are seen in the samples that were bonded at a lower temperature (1000 °C). By increasing the joining temperature from 1000 °C to 1050 °C, all micro discontinuities have disappeared, which shows that the microplastic deformation of roughness has improved. Then, by increasing the temperature to 1150 °C, non-bonded areas are observed in the joint due to the reduction of pressure on the contact surfaces. When pure nickel is used as an interlayer, intermetallic compounds of γ' [Ni3(Al, Ti)] are formed in the γ matrix phase on the side of Inconel 738 superalloy while compounds of FeNi3 and γ (γFe, Ni) are formed on the side of 418 steel. According to the results of line scan analysis, the slope and penetration of elements in Inconel 738 superalloy is lower than 418 steel, which indicates less penetration in Inconel 738 superalloy. In the sample welded at the temperature of 1050 °C and the time of 90 Min, the penetration value of the nickel interlayer in 418 steel and Inconel 738 superalloy was 40 µm and 35 µm, respectively. By comparing the maximum hardness, it can be concluded that the joint at the temperature of 1050 °C and the time of 90 Min has a lower maximum hardness than other samples. Therefore, it has better joint characteristics than other samples in terms of intermetallic compounds. The highest value of shear strength was obtained at the temperature of 1050 °C and the time of 90 Min, which is equal to 270 MPa.
M. R. Borhani, M. Rajabi, R. Shoja Razavi, R. Jamaati,
Volume 9, Issue 2 (1-2024)
Abstract
Reconstruction of parts using direct laser deposition can create a combination of high wear resistance properties, good toughness, and corrosion resistance. In this research, the wear properties of Inconel 625 powder cladding on the same substrate have been investigated; For this purpose, room temperature and high temperature wear tests have been used. Mass reduction, friction coefficient, width and depth of wear penetration have been measured. Also, a scanning electron microscope with an energy disspersive spectroscopy system was used to evaluate the cladding surface. The results showed that the mass reduction due to wear at Inconel 625 cladding compared to Inconel 625 substrate has decreased by 7% and 52%, respectively, at temperatures of 25°C and 620°C. Also, the wear mechanism of the room temperature of the cladding is mainly scratchy, and the wear mechanism of high temperature is mainly sticky.
M.r. Hajiha, A. Farzadi, S. A. Samadani Agdam, A. Shabanzadeh, S. Ramezani,
Volume 9, Issue 2 (1-2024)
Abstract
5xxx and 6xxx series alloys are among the most widely used aluminum alloys in various industries, including automobile, shipbuilding and aviation industries. In this research, the joint of two alloys AA6061-T6 and AA5052-H12 was investigated at 4 transmission speeds of 60, 90, 120 and 180 mm/min and 3 rotation speeds of 600, 800 and 1000 rpm. These investigations were carried out in the condition that each of the two alloys was placed in two progressive and regressive sides. The results of these studies showed that the highest tensile strength is when the AA5052 sample is placed on the advancing side and the transfer speed is 90 mm/min and the rotation speed is 600 rpm, and in this case, the final tensile strength value is equal to 197 MPa. In addition, the results showed that, generally, the tensile strength decreases with an increase in the transmission speed at a constant rotational speed, and with an increase in the rotational speed at a constant transmission speed, the tensile strength increases. In addition, microscopic and macroscopic examination of the sections of all samples was performed and various areas and defects were examined. According to the investigations carried out on the microstructure, the grain size in the weld nugget compared to the base metal, HAZ and TMAZ decreases. The grain size in HAZ is the largest in all samples, and this causes a decrease in weld strength in this zone.
R. Mahdizade, S. A.asghar Akbari Mousavi, S. Mehdipour,
Volume 9, Issue 2 (1-2024)
Abstract
In this study, non-homogenous welding of nimonic 75 superalloy to Monel 400 with 1 mm thickness was investigated with pulsed Nd:YAG laser welding. The mechanical properties of the joint were analyzed with optical and scanning electron microscope, X-ray diffraction, micro-hardness test and tensile test. In the case of non-homogeneous welding of Nimoinc 75 superalloy to Monel 400, defects such as liquation cracks and porosity in the welded samples were observed. these defects were removed with increasing the preheating temperature and decreasing the heat input. The results showed the voltage, pulse width, pulse frequency and welding speed should be selected as 500 volts, 9 milliseconds, 3 Hz and 0.9 mm/s respectively to reach the proper penetration depth. Also, the investigations show that the welding structure is composed of austenitic matrix containing columnar dendrites and some cellular areas. The mechanical properties of the weld metal were reduced after joining and segregation causes a change in the amount of elements and the appearance of intermetallic compounds in the spaces between dendrites and cells. All non-homogeneous samples broke during the tensile test from the weld metal area.
M. Bozorgmehr, A. Heidari, K. Amini, M. Loh Mousavi, F. Gharavi,
Volume 9, Issue 2 (1-2024)
Abstract
In the present study, friction stir process (FSP) was used to produce AL/ZrO2/ZrSiO4 surface hybrid composite at a fixed rotation speed of 1400 rpm and traverse speeds of 20, 25, 31.5 and 40 mm/min. Therefore, the purpose of the mentioned study is to investigate the effect of tool traverse speed on the microstructure, hardness and wear behavior of the above-mentioned surface hybrid composite and compare it with base material aluminum 5052. Investigations showed that as a result of FSP operation, a fine-grained structure is created, which improves the hardness and wear resistance of the samples compared to the base sample with the presence of ZrO2 and ZrSiO4 particles. Also, the results showed that among the FSP samples, the sample with a speed of 20 mm/min has the highest hardness and wear resistance. The reason for this is that in this sample, due to the lower traverse speed compared to other samples, more heat has been generated, which has led to more suitable particle distribution and more fine particles. Therefore, in the sample with the traverse speed of 20 mm/min, the hardness and wear resistance increases by 27.3% and 68.9% respectively compared to the base material sample. Also, the examination of the wear surfaces of the samples showed that the wear mechanism in the base sample is strong adhesive wear, and as a result of the FSP operation and surface compositing due to the fineness of the grains and the increase in hardness, the wear mechanism has become weak adhesive, so the wear resistance of the sample is FSPs have been improved.
M. N. Sadraee Far, F. Kolahan,
Volume 9, Issue 2 (1-2024)
Abstract
In this study, we employed the active TIG method with ultrasonic vibration (UV) for welding 316L steel. Throughout the active tungsten inert gas (A-TIG) welding process, a high-frequency ultrasonic generator produced high-intensity acoustic waves at an optimal frequency of 20.3 kHz and a vibration amplitude of 8 micrometers. These waves were directed into the molten weld pool, covered by SiO2 nanoparticles serving as an activating flux. The effect of UV and nanoparticles on weld geometry and weld microstructure was analyzed and compared with conventional TIG welding proces. The results indicated that the use of nanopowder not only increased weld penetration by approximately 17.5% but also reduced the Weld Bead Width (WBW) by 28% compared to Conventional TIG. These values increased by 25% and decreased by 35%, respectively, in the presence of ultrasonic waves. Additionally, the introduction of nanomaterials into the molten pool led to finer grains. The ultrasonic waves played a crucial role in ensuring the uniform distribution of these nanomaterials in the melt, ultimately resulting in an enhanced microstructure of the weld.
Mohammad Reza Borhani, Reza Shoja Razavi, Farid Kermani,
Volume 9, Issue 2 (8-2024)
Abstract
In this study, the effect of friction stir welding (FSW) parameters on the dissimilar joint properties of 5083 aluminum alloys and 316L austenitic stainless steel, with a thickness of 4 mm, has been investigated. The tool speed was considered in the range of 16 to 25 mm/min, and the rotation of tool speed was considered to be equal to a constant speed of 250 rpm. To check the microstructure of different weld areas, optical and scanning electron microscopes were used, to check the mechanical properties, hardness and tensile tests were performed. The results showed the formation of a composite region consisting of steel reinforcement particles in the field of aluminum.
At the steel-aluminum interface, a single layer of discontinuous intermetallic composition with a thickness of about 2 micrometers was observed; Also, by choosing the rotation speed of 250 rpm and the tool speed of 16 mm/min, the tensile strength equal to 298 MPa and ductility of 26% (93% of tensile strength and 50% of ductility of aluminum 5083 alloy) were obtained.
A. Etemadi, M. Kasiri-Asgarani, H. R. Bakhsheshi-Rad, M. Sadeghi Gogheri,
Volume 9, Issue 2 (1-2024)
Abstract
In this research, dissimilar joining of biodegradable AZ31 alloy to Ti-6Al-4V titanium alloy by rotary friction welding method was investigated with aim of preparation of pin or screw for orthopedic applications. optical and scanning electron microscope (sem) were used to investigate the microstructure, x-ray diffraction was conducted for phase analysis, torsion and micro-hardness tests were carried out to investigate mechanical properties, and polarization and electrochemical impedance spectroscopy were employed to evaluate corrosion resistance. in the welding procedure, rotational speed of 1100, 1200 and 1300 rpm and friction time of 2 and 4 seconds were considered as variable parameters, and two parameters of friction pressure and forge pressure were considered as constant parameters at 50 and 40 MPa, respectively. The microstructure of the joint zone showed that there is no deformation in the titanium alloy side. However, in the magnesium side, the greatest amount of deformation occurred with the distance from the joint line, where weld center zone (CZ), dynamic recrystallization zone (DRX), thermomechanical affected zone (TMAZ) and partial deformation zone (PDZ) are detected. The formation of intermetallic phases such as Mg2AlZn, Ti3Al and also the refining the grains size is the main reason for increasing the hardness of the magnesium side near the joint line up to 150 HV. The results of the torsion test showed that the welded sample has the highest shear strength of 81.51 MPa and also the highest corrosion resistance among other samples at a rotation speed of 1200 rpm and a friction time of 4 seconds.
P. Chamani, H. Sabet, M. Ghanbari Haghighi,
Volume 9, Issue 2 (1-2024)
Abstract
In this study the effect of rotational speed and tool angle parameters on the microstructure and mechanical properties of the AZ91/CP-Ti joint was investigated, for this reason the sheets with 4 x 26 x 100 mm dimensions were prepared and joint by FSW with different rotational speed (800, 1200 and 2500 rpm) and the tool angle (0.5, 1 and 3 degrees). After joining, the samples were cut and prepared for study of microstructural and mechanical properties. OM and SEM examination shows that the structure of AZ91/CP-Ti nugget zone includes alpha grains and the microstructure of the mix zone on the AZ91 side includes α-magnesium coaxial grains with Mg17Al12 intermetallic compounds. The results of the tensile test show that the maximum tensile strength value (160 MPa) related to the rotation speed of 2500 rpm and the tool angle of 1 degree. It was also determined that the rotation speed of 800 rpm was not suitable for joining of AZ91/CP-Ti. On the other hand, it was observed that by increasing the tool angle the work piece, initially leads to an increases the strength from 141 MPa to 160 MPa and then decreases to 132 MPa. the results of the Vickers hardness test show that the average of the nugget zone hardness was to 173, which is higher than the hardness of AZ91 alloy (61 Vickers) and near to the hardness of CP-Ti (167 Vickers).
Mohammad Reza Maraki, H. Tagimalek, Dr Mohammad Yousefieh, , ,
Volume 9, Issue 2 (8-2024)
Abstract
Society's great and growing demand for buildings and structures has created the need to apply new construction methods to shorten construction times, make buildings lighter, extend their useful life, and make them more earthquake-proof. In the long term, the new methods will lead to structural optimization, increased building performance, and the achievement of optimal operating conditions. New technologies are meeting society's increasing need for special structures more than ever. Additive manufacturing is based on gas metal arc welding as one of the fastest and most cost-effective manufacturing methods for primary metal structures. For this purpose, the three parameters voltage, wire feed speed, and welding speed were considered initial parameters affecting the width and height of the welding flux. To investigate the effects of the process, 16 experiments with input parameters were evaluated. The width and height of the sweat pollen were determined by experimental investigations. Subsequently, the resulting welding geometry is modeled using three numerical modeling methods, including intensive learning machines, relevence vector machine, and fuzzy logic. The comparison between the experimental data and the results of the three generated models shows that fuzzy logic comes closest to the experimental data of the welding geometry of the modeling methods. For example, the test data of the generative fuzzy model resulted in an average error for height and width of 0.667 and 0.5477, respectively, and a root mean square error for height and width of 0.0046 and 0.3, respectively, which expresses the generalization ability and reliability compared to other modeling methods in this process. Finally, a metal pattern of a special structure was produced based on arc and wire additive manufacturing based gas metal arc welding.
M. Mosallaee, A.h. Morshedy,
Volume 9, Issue 2 (1-2024)
Abstract
In this research, the optimization of the artificial neural network (ANN) capability for predecting the tensile strength and elongation of friction stir welded Al-5083 (FS-welded Al-5083) was carried out. The effective parameters of ANN, such as the number of layers, number of neurons in hidden layers, transfer function between layers, the learning algorithm and etc. were investigated and the efficient neural network was determined to predict the tensile properties of FS-welded Al-5083. The investigations revealed that the perceptron neural network with two hidden layers and 17 neurons numbers, Lunberg-Marquardt training algorithm and Logsig transfer function for the intermediate layers and Tansig transformation function for the output layer is the most optimized neural network for the prediction. The optimized network has an optimal structure based on the minimum value of the mean square error of 0.05, the maximum total correlation coefficient of 0.93 and the line regression with an angle of 45 degrees between the actual and estimated values. Therefore, this network has a good performance for training, generalizing and estimating of tensile strength and elongation of FS-welded Al-5083.
E. Mansouri, H. Khorsand,
Volume 9, Issue 2 (1-2024)
Abstract
High entropy alloys are especially suitable for use as filler metals in brazing due to their excellent properties. in the present study, three powders with the composition of CoxCrxCuxFexMnxNix (X atomic percentage of the element) were designed using the criteria of these alloys as well as jmatpro software. in the next step, using mechanical alloying, filler nano powder was synthesized and characterized by X-RAY analysis (XRD) test and the effect of filler composition on the thermal behavior of the alloy was studied. then the filler was used in Inconel 600 super alloy brazing, the single-phase solidification behavior and the absence of boron and silicon in the high entropy filler led to the creation of a continuous microstructure without eutectic components or brittle phases in the brazing interface. thus, the shear strength test was performed and 545 MPa was the highest shear strength obtained among the three filler compounds. in brazing conventional filler metal, incomplete isothermal solidification and subsequent thermal solidification of the residual liquid results in large grains of chromium-rich boride phase distributed throughout the microstructure. not using compounds that lower the melting point in the filler for the purpose of joining the nickel-based superalloy is considered an important step in reducing the subsequent brazing processes.
A. Ardalani, H. Naffakh-Moosavy,
Volume 9, Issue 2 (1-2024)
Abstract
In this research, the effect of temperature and time parameters are investigated on the microstructure and mechanical properties of dissimilar brazing of 17-4 PH stainless steel and Ti-6Al-4V alloy with BNi-2 filler metal. The microstructure of the joint is evaluated with optical and scanning electron microscopes and the mechanical properties of the joint are also evaluated with tensile-shear and microhardness tests. It can be seen that at a constant temperature of 1050°C, increasing the time from 15 to 30 minutes decreases the shear strength from 34.66 to 29.39 MPa. Formation of brittle intermetallic compounds like NiTi2 and FeTi2 increase strength and promote brittle fracture.At a fixed time of 15 minutes, increasing the temperature from 1050 to 1100 °C causes the strength to increase from 34.66 to 38.46 MPa. Also, the increase in temperature and time increases the ISZ thickness formed in the joints on the side of the filler metal - Ti-6Al-4V from 41.40 to 81.48 microns. The increase in temperature and time also causes more diffusion of boron into the SS-filler joint, which forms various boron compounds and widens this region.
Mr E. Ganjeh, Dr Ali Kaflou, Dr Kourosh Shirvani,
Volume 9, Issue 2 (1-2024)
Abstract
In this study, mechanical properties of the transient liquid phase (TLP) bonds between Hastelloy X to Ni3Al IMC at temperature range of 800 - 900 °C were investigated. The microstructure of the joints was examined by optical and scanning electron microscopy. Also, high temperature XRD (HTXRD) analysis was utilized to investigate the phase changes at different temperatures of half-joints. According to microscopic observations, the joint cross-section consisted of three regions including diffusion affected zone (DAZ), isothermal solidification zone (ISZ), and Athermal solidification zone (ASZ), which increasing temperature and time result in ISZ consisting of nickel-rich solid solution developed across the microstructure. The optimum joint bonding strength was achieved for the sample treated at 1100 °C – 180 min equal to 355 ± 4.5 MPa. The ultimate tensile strength reached 36.5 ± 1 and 20.5 ± 1 MPa at temperatures of 800 °C and 900 °C, respectively. Fracture occurred on the side of the IMC substrates at both test temperatures due to the presence of shrinkage porosity during the solidification stage of IMC and crystal lattice parameters mismatch with the matrix.
S. H. Hashemi, R. Vafaei, R. Shoja-Razavi,
Volume 9, Issue 2 (1-2024)
Abstract
316 steel is used in transportation, space, and chemical equipment. This steel is in demand in these industries due to its durability. It is used to increase the lifespan and renovate equipment. The research explores the impact of laser energy density on st6 cladding. It specifically focuses on the microstructure and geometric characteristics of the cladding. The cladding is applied on 316 steel. The experiment was designed with energy density changes from 40 to 116 J/mm and powder rate changes between 12 and 20 g/min. Optical and electron microscopic images were used to evaluate the samples. The results indicated that the dendritic arms grew larger with increased energy density. The dimensions increased from 1.5 to approximately 3. In other words, the speed of cooling is doubled. Increasing energy density from 40 to 75 J/mm reduced cobalt to chromium ratio from 2 to 0.7. It also decreased cobalt to iron ratio from 35 to 3. The changes emphasize how energy density affects microstructure and phase transformations.
Ahmad Reza Nazari, Negar Ghazavi Khorasgani, Aboozar Taherizadeh, Masoud Atapour,
Volume 9, Issue 2 (8-2024)
Abstract
In this study, the microstructure and mechanical properties of dissimilar resistance spot welding of AISI 430 steel and S500 MC steel were investigated. To carry out this research, Taguchi's L9 array was used to determine the number of samples and determine the range of variables of each sample, and after welding the samples and performing the shear tensile test, the sample with the highest tensile shear strength (13740 N) and the highest amount of fracture energy (102160 Joules) ), was considered as the best example; Also, the variables of this sample, i.e., welding current of 12 kW, welding time of 12 cycles, and electrode force of 3 kN, had the highest signal-to-noise values, and these values were chosen among the best range of variables among the proposed variables. Then, a microhardness test was performed on the welded sample with the above variables, and microstructural studies were performed by optical microscope and scanning electron microscope. The hardness of the weld zone was observed to be about 400 Vickers, and the microstructure of the weld metal consisted of ferrite, martensite, and Widmannstatten ferrite.
