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Showing 152 results for Type of Study: Research

M.r. Hajiha, A. Farzadi, S. A. Samadani Agdam, A. Shabanzadeh, S. Ramezani,
Volume 9, Issue 2 (1-2024)
Abstract

5xxx and 6xxx series alloys are among the most widely used aluminum alloys in various industries, including automobile, shipbuilding and aviation industries. In this research, the joint of two alloys AA6061-T6 and AA5052-H12 was investigated at 4 transmission speeds of 60, 90, 120 and 180 mm/min and 3 rotation speeds of 600, 800 and 1000 rpm. These investigations were carried out in the condition that each of the two alloys was placed in two progressive and regressive sides. The results of these studies showed that the highest tensile strength is when the AA5052 sample is placed on the advancing side and the transfer speed is 90 mm/min and the rotation speed is 600 rpm, and in this case, the final tensile strength value is equal to 197 MPa. In addition, the results showed that, generally, the tensile strength decreases with an increase in the transmission speed at a constant rotational speed, and with an increase in the rotational speed at a constant transmission speed, the tensile strength increases. In addition, microscopic and macroscopic examination of the sections of all samples was performed and various areas and defects were examined. According to the investigations carried out on the microstructure, the grain size in the weld nugget compared to the base metal, HAZ and TMAZ decreases. The grain size in HAZ is the largest in all samples, and this causes a decrease in weld strength in this zone.

R. Mahdizade, S. A.asghar Akbari Mousavi, S. Mehdipour,
Volume 9, Issue 2 (1-2024)
Abstract

In this study, non-homogenous welding of nimonic 75 superalloy to Monel 400 with 1 mm thickness was investigated with pulsed Nd:YAG laser welding. The mechanical properties of the joint were analyzed with optical and scanning electron microscope, X-ray diffraction, micro-hardness test and tensile test. In the case of non-homogeneous welding of Nimoinc 75 superalloy to Monel 400, defects such as liquation cracks and porosity in the welded samples were observed. these defects were removed with increasing the preheating temperature and decreasing the heat input. The results showed the voltage, pulse width, pulse frequency and welding speed should be selected as 500 volts, 9 milliseconds, 3 Hz and 0.9 mm/s respectively to reach the proper penetration depth. Also, the investigations show that the welding structure is composed of austenitic matrix containing columnar dendrites and some cellular areas. The mechanical properties of the weld metal were reduced after joining and segregation causes a change in the amount of elements and the appearance of intermetallic compounds in the spaces between dendrites and cells. All non-homogeneous samples broke during the tensile test from the weld metal area.

M. Bozorgmehr, A. Heidari, K. Amini, M. Loh Mousavi, F. Gharavi,
Volume 9, Issue 2 (1-2024)
Abstract

In the present study, friction stir process (FSP) was used to produce AL/ZrO2/ZrSiO4 surface hybrid composite at a fixed rotation speed of 1400 rpm and traverse speeds of 20, 25, 31.5 and 40 mm/min. Therefore, the purpose of the mentioned study is to investigate the effect of tool traverse speed on the microstructure, hardness and wear behavior of the above-mentioned surface hybrid composite and compare it with base material aluminum 5052. Investigations showed that as a result of FSP operation, a fine-grained structure is created, which improves the hardness and wear resistance of the samples compared to the base sample with the presence of ZrO2 and ZrSiO4 particles. Also, the results showed that among the FSP samples, the sample with a speed of 20 mm/min has the highest hardness and wear resistance. The reason for this is that in this sample, due to the lower traverse speed compared to other samples, more heat has been generated, which has led to more suitable particle distribution and more fine particles. Therefore, in the sample with the traverse speed of 20 mm/min, the hardness and wear resistance increases by 27.3% and 68.9% respectively compared to the base material sample. Also, the examination of the wear surfaces of the samples showed that the wear mechanism in the base sample is strong adhesive wear, and as a result of the FSP operation and surface compositing due to the fineness of the grains and the increase in hardness, the wear mechanism has become weak adhesive, so the wear resistance of the sample is FSPs have been improved.
 

A. Etemadi, M. Kasiri-Asgarani, H. R. Bakhsheshi-Rad, M. Sadeghi Gogheri,
Volume 9, Issue 2 (1-2024)
Abstract

In this research, dissimilar joining of biodegradable AZ31 alloy to Ti-6Al-4V titanium alloy by rotary friction welding method was investigated with aim of preparation of pin or screw for orthopedic applications. optical and scanning electron microscope (sem) were used to investigate the microstructure, x-ray diffraction was conducted for phase analysis, torsion and micro-hardness tests were carried out to investigate mechanical properties, and polarization and electrochemical impedance spectroscopy were employed to evaluate corrosion resistance. in the welding procedure, rotational speed of 1100, 1200 and 1300 rpm and friction time of 2 and 4 seconds were considered as variable parameters, and two parameters of friction pressure and forge pressure were considered as constant parameters at 50 and 40 MPa, respectively. The microstructure of the joint zone showed that there is no deformation in the titanium alloy side. However, in the magnesium side, the greatest amount of deformation occurred with the distance from the joint line, where weld center zone (CZ), dynamic recrystallization zone (DRX), thermomechanical affected zone (TMAZ) and partial deformation zone (PDZ) are detected. The formation of intermetallic phases such as Mg2AlZn, Ti3Al and also the refining the grains size is the main reason for increasing the hardness of the magnesium side near the joint line up to 150 HV. The results of the torsion test showed that the welded sample has the highest shear strength of 81.51 MPa and also the highest corrosion resistance among other samples at a rotation speed of 1200 rpm and a friction time of 4 seconds.

M. Mosallaee, A.h. Morshedy,
Volume 9, Issue 2 (1-2024)
Abstract

In this research, the optimization of the artificial neural network (ANN) capability for predecting the tensile strength and elongation of friction stir welded Al-5083 (FS-welded Al-5083) was carried out. The effective parameters of ANN, such as the number of layers, number of neurons in hidden layers, transfer function between layers, the learning algorithm and etc. were investigated and the efficient neural network was determined to predict the tensile properties of FS-welded Al-5083. The investigations revealed that the perceptron neural network with two hidden layers and 17 neurons numbers, Lunberg-Marquardt training algorithm and Logsig transfer function for the intermediate layers and Tansig transformation function for the output layer is the most optimized neural network for the prediction. The optimized network has an optimal structure based on the minimum value of the mean square error of 0.05, the maximum total correlation coefficient of 0.93 and the line regression with an angle of 45 degrees between the actual and estimated values. Therefore, this network has a good performance for training, generalizing and estimating of tensile strength and elongation of FS-welded Al-5083.

E. Mansouri, H. Khorsand,
Volume 9, Issue 2 (1-2024)
Abstract

High entropy alloys are especially suitable for use as filler metals in brazing due to their excellent properties. in the present study, three powders with the composition of CoxCrxCuxFexMnxNix (X atomic percentage of the element) were designed using the criteria of these alloys as well as jmatpro software. in the next step, using mechanical alloying, filler nano powder was synthesized and characterized by X-RAY analysis (XRD) test and the effect of filler composition on the thermal behavior of the alloy was studied. then the filler was used in Inconel 600 super alloy brazing, the single-phase solidification behavior and the absence of boron and silicon in the high entropy filler led to the creation of a continuous microstructure without eutectic components or brittle phases in the brazing interface. thus, the shear strength test was performed and 545 MPa  was the highest shear strength obtained among the three filler compounds. in brazing conventional filler metal, incomplete isothermal solidification and subsequent thermal solidification of the residual liquid results in large grains of chromium-rich boride phase distributed throughout the microstructure. not using compounds that lower the melting point in the filler for the purpose of joining the nickel-based superalloy is considered an important step in reducing the subsequent brazing processes.

A. Ardalani, H. Naffakh-Moosavy,
Volume 9, Issue 2 (1-2024)
Abstract

In this research, the effect of temperature and time parameters are investigated on the microstructure and mechanical properties of  dissimilar brazing of 17-4 PH stainless steel and Ti-6Al-4V alloy with BNi-2 filler metal. The microstructure of the joint is evaluated with optical and scanning electron microscopes and the mechanical properties of the joint are also evaluated with tensile-shear and microhardness tests. It can be seen that at a constant temperature of 1050°C, increasing the time from 15 to 30 minutes decreases the shear strength from 34.66 to 29.39 MPa. Formation of brittle intermetallic compounds like NiTi2 and FeTi2 increase strength and promote brittle fracture.At a fixed time of 15 minutes, increasing the temperature from 1050 to 1100 °C causes the strength to increase from 34.66 to 38.46 MPa. Also, the increase in temperature and time increases the ISZ thickness formed in the joints on the side of the filler metal - Ti-6Al-4V from 41.40 to 81.48 microns. The increase in temperature and time also causes more diffusion of boron into the SS-filler joint, which forms various boron compounds and widens this region.

Mr E. Ganjeh, Dr Ali Kaflou, Dr Kourosh Shirvani,
Volume 9, Issue 2 (1-2024)
Abstract

In this study, mechanical properties of the transient liquid phase (TLP) bonds between Hastelloy X to Ni3Al IMC at temperature range of 800 - 900 °C were investigated. The microstructure of the joints was examined by optical and scanning electron microscopy. Also, high temperature XRD (HTXRD) analysis was utilized to investigate the phase changes at different temperatures of half-joints. According to microscopic observations, the joint cross-section consisted of three regions including diffusion affected zone (DAZ), isothermal solidification zone (ISZ), and Athermal solidification zone (ASZ), which increasing temperature and time result in ISZ consisting of nickel-rich solid solution developed across the microstructure. The optimum joint bonding strength was achieved for the sample treated at 1100 °C – 180 min equal to 355 ± 4.5 MPa. The ultimate tensile strength reached 36.5 ± 1 and 20.5 ± 1 MPa at temperatures of 800 °C and 900 °C, respectively. Fracture occurred on the side of the IMC substrates at both test temperatures due to the presence of shrinkage porosity during the solidification stage of IMC and crystal lattice parameters mismatch with the matrix.

S. H. Hashemi, R. Vafaei, R. Shoja-Razavi,
Volume 9, Issue 2 (1-2024)
Abstract

316 steel is used in transportation, space, and chemical equipment. This steel is in demand in these industries due to its durability. It is used to increase the lifespan and renovate equipment. The research explores the impact of laser energy density on st6 cladding. It specifically focuses on the microstructure and geometric characteristics of the cladding. The cladding is applied on 316 steel. The experiment was designed with energy density changes from 40 to 116 J/mm and powder rate changes between 12 and 20 g/min. Optical and electron microscopic images were used to evaluate the samples. The results indicated that the dendritic arms grew larger with increased energy density. The dimensions increased from 1.5 to approximately 3. In other words, the speed of cooling is doubled. Increasing energy density from 40 to 75 J/mm reduced cobalt to chromium ratio from 2 to 0.7. It also decreased cobalt to iron ratio from 35 to 3. The changes emphasize how energy density affects microstructure and phase transformations.

Dr Mojtaba Movahedi, Dr Amir Hossein Kokabi, Engineer Mohammad Hadi Nourmohammadi,
Volume 9, Issue 2 (8-2024)
Abstract

Soldering plays a crucial role in the electronics industry, driving the need for constant improvements in physical and mechanical properties and the management of intermetallic compound formation. Research in composite materials aims to achieve a uniform distribution of reinforcing particles within solder matrices to enhance their performance. This study investigates the integration of cobalt microparticles into SAC0307 lead-free soft solder alloy using the accumulative roll bonding (ARB) method. Microstructural analysis confirmed a homogeneous dispersion of cobalt particles within the solder after three ARB passes. Moreover, increasing cobalt content led to a reduction in the size of Cu6Sn5 intermetallic compounds, from 9 µm to 5 µm with 1% cobalt by weight. Examination of β-Sn grain morphology revealed the impact of cobalt particles on recovery and recrystallization kinetics in the solder. Mechanical testing indicated a 20% decrease in interlayer strength within composite solder sheets. Tensile tests showed a 28% increase in strength and a 31% decrease in elongation for composite solder alloy containing 1% cobalt. Differential scanning calorimetry (DSC) results revealed minimal change in the melting temperature of composite solder foil
Behnam Heidari-Dehkordi, Mahdi Rafiei, Mahdi Omidi, Mohsen Abbasi-Baharanchi,
Volume 9, Issue 2 (8-2024)
Abstract

In this study, 316L stainless steel and WC-10Co cermet were bonded by transient liquid phase process with BNi-2 interlayers with different thicknesses of 25 and 50 μm. The bonding process was conducted at 1050 °C for 1, 15, and 30 min. After bonding, the microstructure of the joints was examined using optical microscopy and scanning electron microscopy equipped with energy-dispersive X-ray spectroscopy. Microhardness and tensile-shear tests were also performed to study the mechanical properties of the bonded samples. Microstructural analyses revealed that the formation mechanism of the solidified region in all samples was isothermal solidification, resulting in an isothermal solidification zone upon bonding. Additionally, the only phase present in the isothermal solidification zone was a nickel-based solid solution. In the diffusion-affected zone of the steel base material, complex borides formed regardless of the interlayer thickness. In the diffusion-affected zone of the WC-Co material, a brittle eta phase formed. Microhardness tests indicated that the maximum hardness in all samples was approximately 1100 Vickers, which was attributed to the presence of hard WC particles in the WC-Co base material. Furthermore, the highest tensile-shear strength, approximately 240 MPa, was observed in the bonded sample for 15 min with 50 μm thickness interlayer.
 
M.r Borhani, S.r. Shoja-Razavi, F. Kermani,
Volume 10, Issue 1 (6-2024)
Abstract

In this study, the effects of friction stir welding (FSW) parameters on the properties of dissimilar joints formed between 5083 aluminum alloys and 316L austenitic stainless steel, with a thickness of 4 mm, are investigated. The tool speed is varied in the range of 16 to 25 mm/min, while the tool rotation speed is maintained at a constant value of 250 rpm. To examine the microstructure of different weld regions, both optical and scanning electron microscopes are employed. To assess the mechanical properties, hardness and tensile tests are conducted. The results shows the formation of a composite region characterized by steel reinforcement particles dispersed within an aluminum matrix. At the steel-aluminum interface, a single layer of discontinuous intermetallic composition with a thickness of approximately 2 micrometers is observed. Notably, when the rotation speed is set to 250 rpm and the tool speed is 16 mm/min, a tensile strength of 298 MPa and ductility of 26% (93% of the tensile strength and 50% of the ductility of the 5083 aluminum alloy) are achieved.

M. R. Maraki, H. Tagimalek, Dr M. Yousefieh, A. Aghaeifar, A. Foorginejad,
Volume 10, Issue 1 (6-2024)
Abstract

Society's great and growing demand for buildings and structures has created the need to apply new construction methods to shorten construction times, make buildings lighter, extend their useful life, and make them more earthquake-proof. In the long term, the new methods will lead to structural optimization, increased building performance, and the achievement of optimal operating conditions. New technologies are meeting society's increasing need for special structures more than ever. Additive manufacturing is based on gas metal arc welding as one of the fastest and most cost-effective manufacturing methods for primary metal structures. For this purpose, the three parameters voltage, wire feed speed, and welding speed were considered initial parameters affecting the width and height of the welding flux. To investigate the effects of the process,
16 experiments with input parameters were evaluated. The width and height of the sweat pollen were determined by experimental investigations. Subsequently, the resulting welding geometry is modeled using three numerical modeling methods, including intensive learning machines, relevence vector machine, and fuzzy logic. The comparison between the experimental data and the results of the three generated models shows that fuzzy logic comes closest to the experimental data of the welding geometry of the modeling methods. For example, the test data of the generative fuzzy model resulted in an average error for height and width of 0.667 and 0.5477, respectively, and a root mean square error for height and width of 0.0046 and 0.3, respectively, which expresses the generalization ability and reliability compared to other modeling methods in this process. Finally, a metal pattern of a special structure was produced based on arc and wire additive manufacturing based gas metal arc welding.

 
A. R. Nazari , A. Taherizadeh, M. Atapour,
Volume 10, Issue 1 (6-2024)
Abstract

In this study, the microstructure and mechanical properties of dissimilar resistance spot welding of AISI 430 steel and S500 MC steel were investigated. To carry out this research, Taguchi's L9 array was used to determine the number of samples and determine the range of variables of each sample, and after welding the samples and performing the shear tensile test, the sample with the highest tensile shear strength (13740 N) and the highest amount of fracture energy (102160 Joules), was considered as the best example; Also, the variables of this sample, i.e., welding current of 12 kW, welding time of 12 cycles, and electrode force of 3 kN, had the highest signal-to-noise values, and these values were chosen among the best range of variables among the proposed variables. Then, a microhardness test was performed on the welded sample with the above variables, and microstructural studies were performed by optical microscope and scanning electron microscope. The hardness of the weld zone was observed to be about 400 Vickers, and the microstructure of the weld metal consisted of ferrite, martensite, and Widmannstatten ferrite.

A. Adelian, Kh. Ranjbar, M.r. Tavakoli Shoushtari,
Volume 10, Issue 1 (6-2024)
Abstract

This research studied the effect of two-stage over aging treatment on the pitting corrosion behavior and microstructure of the weld metals in the 17-4 precipitation hardening stainless steel. For this purpose, this steel was subjected to solution annealing heat treatment at 1035°C for one hour before welding. Then gas tungsten arc welding (GTAW) was performed using ER630 similar filler metal. Subsequently, a section of the weldment was subjected to two-stage over aging treatment. The microstructure and corrosion resistance of the weld zone after the two-stage over aging treatment were investigated and compared with the weld zone behavior in the as-weld condition. Microstructural studies showed that the two-stage over aging treatment of the weld zone led to the tempering of the martensitic, the formation of more reversed austenite, and the formation of α-ferrite. The volume fraction of austenite in the as-weld condition was approximately %7 and increased to about %30 after two-stage over aging treatment, a four-fold increase. The pitting potential (EPit) of weld metal was -18.15 mv in the as-weld condition and reached 122.54 mv after two-stage over aging treatment, which also signifies an improvement in pitting resistance. The two-stage over aging treatment also reduced the potential differences between the different parts of welding zones reducing the galvanic corrosion occurrence. The assessment of mechanical properties through impact test revealed that impact resistance after
two-stage over aging treatment can be increased by about %66 compared to as-weld condition.

 
A. Khorram, H. Habibi, A. Yazdipour ,
Volume 10, Issue 1 (6-2024)
Abstract

This study aimed to investigate the effect of diffusion welding parameters on the microstructural characteristics and mechanical properties of the dissimilar joint between AISI 418 stainless steel and Inconel 738 superalloy using Ni interlayer with a thickness of 50 µm. The experiments were performed in a vacuum furnace at three temperatures of 1000, 1050 and 1150 °C for 45, 60, 75 and 90 min under the pressure of 5 MPa.The results show that voids and non-bonded areas are seen in the samples that were bonded at a lower temperature (1000 °C). By increasing the joining temperature from 1000 °C to 1050 °C, all micro discontinuities have disappeared, which shows that the microplastic deformation of roughness has improved. Then, by increasing the temperature to 1150 °C,non-bonded areas are observed in the joint due to the reduction of pressure on the contact surfaces. When pure nickel is used as an interlayer, intermetallic compounds of
γ' [Ni3(Al, Ti)] are formed in the γ matrix phase on the side of Inconel 738 superalloy while compounds of FeNi3 and γ (γFe, Ni) are formed on the side of AISI 418 stainless steel. According to the results of line scan analysis, the slope and penetration of elements in Inconel 738 superalloy is lower than AISI 418 stainless steel , which indicates less penetration in Inconel 738 superalloy. In the sample welded at the temperature of 1050 °C and the time of  90 Min, the penetration value of the nickel interlayer in AISI 418 stainless steel  and Inconel 738 superalloy was 40 µm and 35 µm, respectively. By comparing the maximum hardness, it can be concluded that the joint at the temperature of 1050 °C and the time of 90 Min has a lower maximum hardness than other samples. Therefore, it has better joint characteristics than other samples in terms of intermetallic compounds. The highest value of shear strength was obtained at the temperature of 1050 °C and the time of 90 Min, which is equal to 270 MPa.

R. Abbasi, S. A.a. Akbari Mousavi, Y. Vahidshad,
Volume 10, Issue 1 (6-2024)
Abstract

The present study focuses on optimizing the mechanical properties and microstructure of laser welding in Haynes 25 (L-605) cobalt-based superalloy. Initially, the influence of laser welding variables such as laser power, pulse frequency, welding speed, and pulse width on the mechanical and metallurgical properties of the weld joints is investigated. By examining the welding variables, the values of G (thermal gradient) and R (cooling rate) are calculated, and their ratio (G/R) and cooling rate (G×R), which predominantly affect the solidification microstructure, are determined. The structural correlation with the mechanical properties resulting from welding is examined.  In this research, it is considered to obtain the welding variables to create a high percentage of the structure in the form of equiaxed dendrite. Microstructural analysis reveals the growth of equiaxed grains and dendritic structures in the weld zone. The high cooling rate in the weld pool leads to dendritic solidification starting from columnar dendrites at the weld walls and ending in equiaxed dendrites at the center of the weld. The microhardness value in the weld zone is HV 328, which is very close to the microhardness of the base material. The tensile strength of the weld samples reaches about 93% to 94% of the base metal tensile strength. Tensile testing of the weld samples indicates a ductile-brittle fracture. Examination of the scanning electron microscope confirms the presence of dimples, intergranular cracks, and microvoids in the fracture zone.

 
Engineer M. H. Nourmohammadi, M. Movahedi, A. H. Kokabi ,
Volume 10, Issue 1 (6-2024)
Abstract

In today's technological landscape, the push for miniaturization in electronic devices is greater than ever, driven by technological advancements.The challenges of electromigration and thermomigration
have arisen due to the need to establish new electronic connections under conditions characterized by creeping temperatures, originating from the low melting point of solders and high current density.  Therefore, recently, alloying and composite materials have been employed to enhance the resistance of electronic connections to electromigration. In this study, efforts to enhance the resistance to electromigration using a composite SAC0307 lead-free solder alloy incorporating cobalt microparticles. The presence of cobalt in the intermetallic composition of the interface causes more stability of the intermetallic composition of the interface and prevents the reduction of the thickness of the intermetallic composition of the interface during the time of the electromigration test; As a result, the stability and electronic connection of the sample soldered with composite solder alloy is more than that of non-composite solder alloy. On the other hand, due to the fine grain structure and the increase in grain boundary density in the composite solder alloy, the lattice diffusion mechanism in the non-composite solder alloy has been changed to the grain boundary diffusion mechanism; As a result, due to the consumption of copper atoms flowed from the cathode side to the anode by the intermetallic compounds present in the grain boundaries, non-uniform microstructural was observed in the composite solder alloy during the time of electromigration test.

H. Zeidabadinejad, M. Rafiei, I. Ebrahimzadeh, M. Omidi, F. Naeimi ,
Volume 10, Issue 1 (6-2024)
Abstract

In this research, the transient liquid phase bonding of St52 carbon steel to WC-Co cermet using a copper interlayer with 50 μm thickness was done. For this purpose, samples were jointed to each other at a constant temperature of 1100 ºC and bonding times of 1, 15, 30, and 45 min. The microstructure of the joints was examined using an optical microscope and scanning electron microscope equipped with energy-dispersive X-ray spectroscopy. XRD analysis was also used to investigate the effect of bonding on the phase changes of the bonding area. Microhardness and tensile shear tests were also conducted to study the mechanical properties of the samples. Microstructural investigations showed the formation of three different zones including isothermal and athermal solidification zones and DAZ in the WC-Co base material side, which determine the characteristics of the samples. The isothermal solidification zone contained a Fe-rich solid solution and the athermal solidification zone contained a Cu-rich solid solution. η phase was not formed in the DAZ of WC-Co cermet at bonding times of 1 and 15 min. This phase was formed in the DAZ of WC-Co cermet by increasing the bonding time to 30 and 45 min. The microhardness studies showed that all samples had the same trend. Maximum microhardness was 1100 HV which was related to WC-Co base cermet and the lowest microhardness was about 220 HV which was related to steel base metal. Also, the maximum tensile-shear strength of the bonded samples was about 180 MPa for a bonded sample at a bonding time of 15 min, which was due to the increase in the volume fraction of iron-rich solid solution, as well as proper microstructural continuity and the presence of an optimal amount of copper-rich phase in the microstructure.


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