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H.g. Tehrani-Moghadam, H.r. Jafarian, M. Aghazadeh Ghomi, A. Heidarzadeh,
Volume 11, Issue 1 (7-2025)
Abstract

In this study, the effect of friction stir welding on the microstructure and mechanical properties of Fe-24Ni-4Cr austenitic steel was investigated. For this purpose, a sheet with a thickness of 1 mm was subjected to friction stir welding using a WC-5%Co tool at a traverse speed of 100 mm/min and a tool rotational speed of 450 rpm. Electron backscatter diffraction (EBSD) analysis revealed that this process led to grain refinement and an increase in high-angle grain boundaries in the stir zone, attributed to dynamic recrystallization during welding. Phase maps indicated an increase in the BCC phase fraction in the stir zone compared to the base metal. Given the high strain rate and the presence of stabilizing elements, this phase was primarily strain-induced martensite. Mechanical property assessments showed a significant increase in the tensile strength of the stir zone (450 MPa) compared to the base metal (350 MPa). Moreover, the yield strength of the stir zone (388 MPa) was substantially higher than that of the base metal (145 MPa), which can be attributed to grain refinement, an increase in high-angle grain boundaries, a higher dislocation density, and martensite formation. However, the ductility of the stir zone decreased due to higher stress concentration and dislocation density in this region. These findings suggest that friction stir welding can be an effective method for enhancing the strength and hardness of austenitic steels, but process conditions must be carefully controlled to prevent reductions in toughness and ductility.

S. Sajjadi Nikoo, F. Qods, M. Yousefieh,
Volume 11, Issue 1 (7-2025)
Abstract

In this research, the ultrafine-grained (UFG) composite of AA2024 and AA5083 aluminum alloys was made by accumulative roll bonding (ARB) process and butt-welded by friction stir welding. Friction stir welding (FSW) is the best method for the joining of UFG strips. Microstructural investigations were performed by optical microscope and transmission electron microscope in the stir zone (SZ), thermo-mechanically affected zone (TMAZ) and heat affected zone (HAZ). The fine recrystallized structure with a grain size of about 900 nm was determined in the weldment. Due to the strengthening mechanisms of grain boundaries, nano-meter size precipitates and solid solution strengthening, the high strength of about 403 MPa was achieved. The presence of precipitates with homogeneous distribution in FSWed strips caused a high ductility of about 14% compared to the fabricated composite strips (6.9%). The high hardness of the SZ was caused by the formation of new equiaxed grains and fine precipitates, and also the decrease in the hardness of the HAZ was due to the dissolution and coarsening of T-phase precipitates.

F. Bashirzadeh, T. Saeid,
Volume 11, Issue 1 (7-2025)
Abstract

Unlike conventional welding methods, joining titanium alloys to steels using ultrasonic welding does not result in the formation of brittle intermetallic compounds and high torsion, causing a reduction in the mechanical properties of the joint. Ultrasonic welding of the St12-CP.Ti samples was performed at constant parameters of 7 bars, 2 s and 1 kW and variable parameter of interlayer material (Cu, 70B and Zn). The investigation of samples by OM, SEM, shear-tensile and microhardness tests revealed that Zn and Cu samples had the lowest and highest bond densities, with 42.2 and 80.6 percent, respectively. The bond density and the strength of the sample with greater interlayer deformability have higher values. Due to the high plastic deformation capability of copper, the Cu sample has generated more heat and deformation at the joint interface than in the other samples. As a result, the microstructure underwent recrystallization and grain growth after enduring severe plastic deformation. Also, the highest hardness of the steel side equal to
201 HV was for the Cu sample, followed by 70B and Zn, respectively.
A. Rahimi, M. Yazdizadeh, M. Vatan Ara, M. Pouranvari,
Volume 11, Issue 1 (7-2025)
Abstract

Wire-arc additive manufacturing (WAAM) is a prominent technique for producing large metallic components due to its high deposition rate. Utilizing austenitic stainless steels in this process not only reduces production costs but also provides greater design freedom. Among these steels, SS310, known as heat-resistant steel in the industry, offers excellent oxidation resistance and high-temperature performance. However, it is highly susceptible to hot cracking during welding and additive manufacturing processes. In this study, the microstructure and mechanical properties of SS310 fabricated using WAAM with Cold Metal Transfer (CMT) and Gas Metal Arc Welding (GMAW) processes were compared. The results revealed that the CMT process, due to its lower heat input, effectively reduces the susceptibility of SS310 to hot cracking compared to the GMAW process. These findings emphasize the importance of selecting an appropriate process to achieve high-quality components and minimize structural defects.

Seyed S. A Hosseini, S. A. A. Akbari Mousavi,
Volume 11, Issue 1 (7-2025)
Abstract

In this study, 1 mm thick austenitic stainless steel 316L sheets were used for experimental testing. The experimental welding process was carried out using a Nd:YAG pulsed laser welding machine, and the welding simulation was performed using the SYSWELD software with a three-dimensional model for thermodynamic and mechanical analysis. The simulation results showed over 90% correlation with the experimental results. Analysis of experimental and numerical data revealed that at a constant voltage of 440 volts, decreasing the welding speed from 2 to 0.5 mm/s increased the overlap rate of pulses from 67% to 93% and the maximum average power density (EPPD) from 5963 to 21831 W/mm². Additionally, increasing the voltage from 440 to 480 volts at a constant speed of 1 mm/s raised the heat input from 114 to 138 J/mm and the weld depth from 0.56 to 0.66 mm. Due to the high cooling rate, the grain size of the weld metal became finer than the base metal (63% reduction in grain size). Two phases, austenite and ferrite, were observed in the weld metal, and the solidification mode was predicted to be FA.With an increase in welding speed from 0.5 mm/s to 2 mm/s at a constant voltage of 440 volts, the maximum tensile residual stress increased from 96 to 260 MPa due to reduced pulse overlap (from 93% to 67%), uneven heat distribution in the part, and the generation of thermal stresses. Furthermore, increasing the welding voltage from 440 to 480 volts at a constant speed of 1 mm/s caused the maximum tensile residual stress to rise from 124 to 152 MPa. The maximum hardness of the weld metal increased from 180 to 215 Vickers as the welding speed rose due to the prevention of carbon diffusion and an increased growth rate. However, with an increase in welding voltage and heat input (from 57 to 69 J/mm), the hardness decreased from 225 to 215 Vickers due to a reduction in thermal gradients and grain growth.

S. Arjmand, Gh. R. Khayati, Z. Rajabi,
Volume 11, Issue 1 (7-2025)
Abstract

In order to improve hardness and wear resistance of St60 steel substrate, NiCrMo welding wire was coated on its surface using gas tungsten arc welding (GTAW) process. Welding characteristics were considered to create a coating with maximum hardness and wear resistance and minimum defects. The results showed that the microstructure of the composite coatings mainly contains of α-Mo, NiMo and blade phases. By increasing in the arc current from 90 to 110 A, porosity and non-uniformity in microstructure of the coatings increased and the sample coated with the arc current of 90 A showed a more uniform microstructure and fewer defects. The average hardness of the coatings was obtained in the range of 218-227 HB (substrate's hardness is approximately equal to 152 HB). The sample prepared with arc current of 90 A showed the least weight loss and the sample prepared with arc current of 110 A showed the greatest weight loss. The wear mechanism of the substrate was mainly abrasive wear and the wear mechanism of the coatings was mainly abrasive and adhesive wear, with the lowest wear products related to the sample prepared with arc current of 90 A and therefore, this sample showed the greatest wear resistance.

A. Bahmani, R. Ashiri,
Volume 11, Issue 1 (7-2025)
Abstract

This research looks at how microstructure and mechanical properties change in resistance spot welds of QP980 advanced high-strength steel. It specifically focuses on the effects of zinc coating and how it influences weld nugget formation, mechanical properties, and fracture behavior. The study involved microscopic examinations, mechanical tests, and finite element simulations to determine the thermal history of different weld zones. A key finding was that rapid cooling during the welding process led to the formation of, metastable phases, such as martensite, in both the weld nugget and the heat-affected zone. A finite element model of the welding process was used to simulate heat distribution and analyze the microstructure in various weld regions. This model showed that reaching the peak temperature during four-pulse resistance spot welding is delayed. This delay, along with proper hold times, helps prevent the formation of voids. The simulated thermal history and the rapid heating/cooling conditions effectively predicted the evolution and transformation of the microstructure in different weld areas. It was found that the presence of a zinc coating, and the resulting reduction in electrical contact resistance, delayed the formation of the weld nugget at lower welding currents. However, at higher currents, the primary source of heat generation shifted from contact resistance to bulk resistance within the steel sheet. This led to larger weld nuggets in coated samples compared to uncoated ones. While uncoated samples showed higher weld nugget hardness (512 Vickers) and greater tensile-shear strength (with a maximum load-bearing capacity of 28.1 kN in uncoated samples versus 24 kN in coated samples), coated samples were able to achieve the critical weld nugget size for a change in fracture mode at lower welding currents (9 kA compared to 9.5 kA).

 
M. Farbakhti, S. R. Elmi Hosseini, S. A. Mousavi Mohammadi,
Volume 11, Issue 1 (7-2025)
Abstract

This study investigated the influence of resistance spot welding current intensity on the formation of liquid metal embrittlement (LME) cracks in galvanized advanced QP1180 steel. Galvanized steel sheets with a thickness of 1 mm were welded at currents of 6.5, 7, 7.5, and 8 kA. The results revealed that increasing the current significantly enlarged the weld nugget size, molten volume, electrode indentation, and the likelihood of LME crack formation. Microstructural analysis, elemental distribution, and crack characterization were conducted using optical and electron microscopy. The findings indicated that the weld zone microstructure primarily consisted of martensite, while the non-uniform distribution of zinc along grain boundaries facilitated the initiation and propagation of LME cracks. Cracks were predominantly observed at the periphery of the weld pool indentation and in the electrode-sheet contact area. This study demonstrates that controlling welding current intensity is a key factor in mitigating LME and improving the mechanical properties of joints in galvanized QP1180 steel. Optimizing welding parameters, particularly limiting current intensity, can prevent molten metal-induced cracking and enhance the durability and safety of automotive structures. Hardness profiling revealed peak hardness in the weld zone, followed by a gradual decrease toward the heat-affected zone (HAZ).

S. Pourmorad Kaleybar, H. Khorsand,
Volume 11, Issue 1 (7-2025)
Abstract

This research focuses on the dissimilar joining of Ti6Al4V and Inconel 718 alloys using the Transient Liquid Phase (TLP) bonding process with a BNi2 foil and a copper interlayer. The objective is to analyze the effects of temperature (850, 950, and 1050 °C) and holding time (10, 20, and 30 minutes) on the microstructure, phase composition, and mechanical properties of the bonding region. DSC analysis indicated that melting reactions begin around 950 °C, attributed to the formation of eutectic compounds in the Cu-Ni-B system. SEM and EDS examinations confirmed the formation of intermetallic phases such as Ti₂Ni, NiTi, Cr₂Ti, and ceramic phase Ni₃B in different regions of the joint. Under optimal conditions (950 °C for 20 minutes), a uniform microstructure, controlled boron diffusion, and formation of stable phases were observed. The hardness in the DAZ region was approximately 420–450 HV. In contrast, higher temperatures and extended holding times led to the formation of brittle phases, solidification cracks, and interfacial discontinuities. The diffusion coefficient of titanium under optimal bonding conditions was estimated to be 2.8×10⁻¹¹ m²/s. These findings emphasize the importance of precise control over process parameters to achieve high-quality joints and prevent structural defects.


M. Karimi Dizaj Cheragh, M. Sajed, M. A. Saeimi Sadigh, A. Abyazi, A. Heidarzadeh,
Volume 11, Issue 2 (12-2025)
Abstract

This study experimentally investigates the repair of surface grooves on pure magnesium samples using the surface friction stir processing (SFSP). Grooves with depths of 0.5, 1, and 1.5 mm were created and subsequently repaired under constant parameters of 1400 rpm rotational speed and 40 mm/min travel speed. The results revealed that the stir zone (SZ) exhibited fine equiaxed grains due to complete dynamic recrystallization, leading to significant improvements in tensile strength and hardness compared to the base metal. The highest ultimate tensile strength of 66.1 MPa and hardness of 60 HV were achieved in the 1 mm groove sample. Additionally, partial dynamic recrystallization was observed in the thermo-mechanically affected zone (TMAZ), and complete elimination of grooves was confirmed in all samples. These findings demonstrate that the SFSP is highly effective for localized repair and enhancement of mechanical properties in magnesium components, offering a promising solution to extend the service life of damaged magnesium parts.

M. Ilanlou, R. Shoja Razavi, P. Pirali, M.r. Borhani,
Volume 11, Issue 2 (12-2025)
Abstract

In this study, laser direct deposition was employed to fabricate a functionally graded transition between 17‑4PH stainless steel and Stellite 6. Specimens were designed and produced such that the chemical composition varied incrementally from 100% 17‑4PH to 100% Stellite 6, with each step involving a 25% decrease in the 17‑4PH content and a corresponding 25 % increase in Stellite 6. Microstructural evolution and elemental distribution were characterized by scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS), while mechanical properties were assessed via Vickers microhardness testing and uniaxial tensile tests. The microstructural analysis revealed a needle‑like martensitic matrix in the substrate, which transformed into cellular dendrites upon reaching the 25% Stellite 6 layer. As the Stellite 6 fraction increased, along with corresponding rises in Cr and W content, grain boundaries broadened and carbides accumulated within interdendritic regions. At the 50% composition, oriented columnar dendrites became prominent, and at higher Stellite 6 levels the dendritic structure refined further, ultimately evolving into an equiaxed morphology. Microhardness measurements showed a continuous increase from approximately 300 HV in the 17‑4PH substrate to 490 HV in the pure Stellite 6 layer. Tensile testing demonstrated that both yield strength (σᵧ) and ultimate tensile strength (σᵤ) remained within 1102–1159 MPa across all compositions, with no evidence of brittle phases or manufacturing defects. Elongation increased from 7% in pure Stellite 6 to 19% in pure 17‑4PH, with the 50%–50% gradient exhibiting an optimal balance of strength and ductility (14.5% elongation).

A. Adelian, Kh. Ranjbar, M. Reihanian, R. Dehmolaei,
Volume 11, Issue 2 (12-2025)
Abstract

This study investigated the effects of pulsed current and constant current on the microstructure and mechanical properties of Hastelloy X superalloy welds produced by Gas Tungsten Arc Welding (GTAW), using ERNiCrMo-2 filler metal. Key microstructural parameters, such as elemental segregation, dendrite refinement, and weld metal uniformity, along with changes in weld strength and hardness, were examined and compared between the two welding modes. Microstructural evaluations were conducted using optical microscopy, Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive Spectroscopy (EDS), and X-ray Diffraction (XRD) for phase identification. Pulsed current welding resulted in a finer microstructure with more equiaxed dendrites, reduced elemental segregation, and a more uniform distribution of M₆C carbides. Furthermore, this process led to significant improvements in hardness, impact toughness, and tensile strength of the weld metal compared to constant current welding. Fracture analysis confirmed ductile fracture behavior in all specimens, consistent with the microstructural and mechanical findings. The results of this research highlight the importance of using pulsed current in GTAW as an effective method for controlling the microstructure and enhancing the mechanical properties of Hastelloy X alloy joints. 

M. Ansari Lale, M.n. Yoozbashi, M. Zadshakoyan, A. Almasi,
Volume 11, Issue 2 (12-2025)
Abstract

The friction stir spot welding (FSSW) process is a solid-state welding technique recognized as one of the most significant advancements in metal joining over the past decade. In this study, the effects of rotational speed and tool contact time, with a unique design different from previous research, on the microstructure and mechanical properties of 5754 series aluminum alloy were investigated. The workpiece was clamped using a specialized fixture on a radial drilling machine, and welding operations were performed using a FSSW machine at different rotational speeds and various tool contact times. Subsequently, the microstructure, microhardness, and tensile-shear strength of the welded spot region were evaluated. The results showed that increasing the tool rotational speed and prolonging the tool contact time led to an improvement of approximately 105% in the tensile-shear strength. According to statistical analyses, the factors of rotational speed and tool contact time significantly affected the shear strength with a confidence level greater than 95%; however, statistical analyses revealed different results regarding the relationship between rotational speed, contact time, and hardness.

R. Sahihi, S. M. A. Boutorabi, R. Ashiri,
Volume 11, Issue 2 (12-2025)
Abstract

The weldability of the superalloy Inconel 738LC is compromised by its susceptibility to heat-affected zone (HAZ) liquation cracking, a consequence of its high gamma-prime (γ') precipitate strength and the formation of low-melting-point eutectic phases. This study investigates the impact of Gas Tungsten Arc Welding (GTAW) current mode—comparing continuous current with pulsed current—on the microstructure, mechanical properties, and overall weldability of IN738LC. Through room-temperature tensile testing, Vickers hardness measurements, and microstructural analysis via optical and electron microscopy, it was demonstrated that pulsed current, particularly at higher frequencies, substantially mitigates liquation cracking and improves joint integrity. The pulsed technique introduces controlled thermal fluctuations that reduce the effective heat input, promoting a transition from columnar to equiaxed dendritic solidification, minimizing interdendritic segregation, and refining the distribution of MC carbides. Consequently, the weld metal exhibits enhanced tensile strength, ductility, and hardness. These findings establish pulsed GTAW as an effective strategy for suppressing cracking and improving the performance of IN738LC welded joints.

M. H. Saebi, A. H. Emami Ghalehghasemi, M. Atapour, A. Saboori,
Volume 11, Issue 2 (12-2025)
Abstract

The Ti-6242 alloy is of particular significance in additive manufacturing due to its high thermal resistance. However, components fabricated from this alloy using the electron beam powder bed fusion (EB-PBF) process often exhibit poor surface quality, primarily resulting from the layer-by-layer fabrication nature and and the presence of partially melted powder particles. In this study, laser polishing was employed to enhance the surface characteristics of EB-PBF fabricated Ti-6242 specimens using three laser powers (195, 260, and 325 W) and two scanning speeds (4.5 and 3 mm/s). The effects of these parameters on surface roughness, microstructure, and mechanical properties were evaluated through surface profilometry, metallography, hardness, and wear tests. The results indicated that the average surface roughness decreased by up to 93%, from 9.36 µm to 0.61 µm. Moreover, the initial α and β phases transformed into a fine, martensitic α′ phase within the polished layer, leading to a 33% increase in hardness—from 380 to 506 HV—and a significant improvement in wear resistance. Consequently, optimal adjustment of laser polishing parameters can simultaneously reduce surface roughness and enhance the mechanical performance of Ti-6242 components.

R. Dadashpour, M. Sajed, M. A. Saeimi Sadigh, A. Abyazi, A. Heidarzadeh,
Volume 11, Issue 2 (12-2025)
Abstract

In this study, the Friction Stir Welding process was employed to repair artificial cracks and grooves in 7075 aluminum alloy. Samples with different groove depths (0.5, 1, 1.5, and 2 mm) were prepared and evaluated through experimental tests, metallographic analysis, tensile testing, and numerical simulation using Abaqus software. The results showed that the Friction Stir Welding successfully repaired the defects without creating voids or surface irregularities. Microstructural observations in the stir zone revealed that dynamic recrystallization led to the formation of fine and homogeneous grains, resulting in improved hardness and tensile strength. The specimen with a 1 mm groove depth exhibited the best mechanical performance, with a maximum hardness of approximately 109 HV and the highest tensile strength among all samples. Conversely, samples with 0.5 and 2 mm groove depths showed void formation and reduced strength due to insufficient or excessive heat input and uneven material flow. Both experimental and simulation results confirmed that a groove depth of 1 mm provides optimal conditions for defect repair in 7075 aluminum alloy.

M. Karbalai-Rashid S. A., H. Abdollah-Pour,
Volume 11, Issue 2 (12-2025)
Abstract

In this study, an AA5083/Al12Mo surface composite containing approximately 10 vol.% of pre-synthesized molybdenum aluminide particles was fabricated using Friction Stir Processing (FSP) under optimized conditions, including six passes, a rotational speed of 1000 rpm, and a traverse speed of 52 mm/min. Multiple FSP passes reduced the particle size from about 20 µm to nearly 1.7 µm and improved their distribution uniformity, while simultaneously refining the matrix grains and enhancing the strain-hardening capability. These microstructural improvements led to a ~16% increase in tensile strength compared to the unreinforced FSPed alloy and ~20% relative to the as-received base metal, along with ~50% and ~63% hardness enhancement in the 4-pass and 6-pass samples, respectively. Quantitative analysis of the strengthening mechanisms revealed that strain hardening contributed the most to the overall strength increment, and the presence of reinforcing particles delayed the onset of the Portevin–Le Chatelier (PLC) serrated flow. Fractography indicated a mixed fracture mode consisting of particle fracture, particle–matrix decohesion, and matrix rupture. Furthermore, corrosion tests demonstrated a decrease in corrosion resistance, mainly due to the discontinuity of the protective aluminum oxide layer and the formation of defects at particle–matrix interfaces caused by severe plastic deformation.

S. Ahmadpour, R. Dehmolaei, Kh. Ranjbar, M. Reihanian,
Volume 11, Issue 2 (12-2025)
Abstract

In this study, the effects of diffusion-bonding temperature and time on the microstructure and corrosion behavior of Al₀.₅CoCrFeMnTi₀.₅ high-entropy alloy coatings applied on A283 plain carbon steel were investigated. The coatings were produced by diffusion bonding using the spark plasma sintering method, in which high-entropy alloy powders were bonded to the substrate at temperatures of 850, 950, and 1050°C for holding times of 10, 15, and 20 minutes. Microstructural characterization performed by field-emission scanning electron microscopy (FESEM) revealed that increasing the diffusion-bonding temperature and time led to reduced porosity and enhanced coating densification. Electrochemical impedance spectroscopy (EIS) and potentiodynamic polarization tests conducted in a 3.5 wt.% NaCl solution demonstrated that increasing the bonding temperature and time resulted in higher charge transfer resistance (Rct) and corrosion potential (Ecorr values, along with a decrease in corrosion current density (icorr). The coating produced at 1050°C with a holding time of 20 minutes exhibited the highest corrosion resistance. The improvement in corrosion performance was attributed to the formation of a uniform and adherent oxide film, which effectively inhibited the penetration of corrosive ions into the steel substrate.

A. Amirkhani, B. Beidokhti, K. Shirvani,
Volume 11, Issue 2 (12-2025)
Abstract

In this study, a novel two-step heating strategy was investigated for transient liquid-phase (TLP) bonding of the IN-738LC superalloy. The bonding process consisted of an initial heating at 1150 °C for 5 seconds, followed by holding at 1110–1130 °C for 3 to 40 minutes. The microstructural evolution during the process, as well as the interface morphology, was characterized and compared with conventional TLP joints. This approach significantly reduced the time required to complete isothermal solidification; the width of the central eutectic zone decreased from 45 µm at 3 minutes to 19 µm at 12 minutes, and the eutectic zone was completely eliminated after 40 minutes. Microstructural examinations revealed that the initial step of the two-step heating process produced a cellular–dendritic solidification interface, leading to a non-uniform distribution of porosity along the bond region. Subsequent homogenization removed boride precipitates and resulted in the formation of uniformly distributed γ′ precipitates similar to those in the base metal. These findings provide practical and microstructural insights into the influence of thermal profiles on interfacial evolution and offer a pathway for improving joint quality in nickel-based superalloys.

M. Lotfi, H. Sabet, B. Karbakhsh Ravari, Gh. Faghani,
Volume 11, Issue 2 (12-2025)
Abstract

In the present study, AISI 1030 cast-steel samples were cladded using duplex stainless-steel wire ER2209 by the Gas Tungsten Arc Welding (GTAW) process under different preheating temperatures and varying numbers of passes. The  degrre of dilution of the clad layers,affected by both  of the preheating temperature and the number of passes—was calculated, and was evaluated its influence on the adhesion and bonding integrity of the ER2209 clad layer on the cast-steel substrate. The results showed that by increasing the number of clad layers led to a lower dilution in the samples. Furthermore, a rise in preheating temperature also contributed to an increase in dilution. Among all conditions, the three-pass cladded sample with a preheating temperature of 100 °C exhibited the highest dilution degree. Bending test results demonstrated that the bending angle increased by the number of clad passes. Macroscopic examination confirmed  that complete interfacial continuity between the clad layer and the base metal. Phase analysis and microstructural observations revealed that the base metal consisted of approximately 80% ferrite and 20% pearlite; the heat-affected zone (HAZ) exhibited a ferrite–transformed pearlite structure with similar volume fractions; and the cladded samples in the final pass presented a duplex austenitic–ferritic structure with 10–20 Wt.% ferrite content. Microhardness test indicated that the two-pass cladded sample  that preheated at 200 °C had the highest hardness value, up to 355 HV.


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