S. Asadi, T. Saeid, A. Valanezhad, J. Khalil Allafi,
Volume 5, Issue 2 (1-2020)
Abstract
In this research, dissimilar welding of NiTi shape memory alloy to AISI 304 austenitic stainless steel Archwires was investigated. For this purpose, common straight orthodontic archwire with rectangular cross-section and dimensions of (0.635 × 0.432 mm) were selected and the laser welding technique was used to connect the wires. The microstructure, chemical composition and phasesin the weld zone of the joints werestudied with Optical microscopy (OM), Scanning electron microscopy (SEM) equipped with EDS analysis system, focused X-ray diffraction (Micro-XRD).Also, the mechanical properties of the weld zone were investigated by using Vickers microhardness test. Microstructure investigation showed that the obtained microstructure from the laser weld of these alloys has a dendritic and non-homogeneous structure. According to XRD analysis, brittle intermetallic compounds such as Fe2Ti, Cr2Ti, TiNi3, and Ti2Ni wereformed during laser welding in the weld zone. Formation of these brittle intermetallics caused increasing the hardness of the weld zoneabout 800 HV. and decreasing the mechanical properties. Also, Fe2Ti intermetallic particles mainly formed in the weld region near the NiTi fusion zone which results in stress concentration, micro-cracks formation and dropping joints mechanical properties. Therefore, a suitable modification process is required to control the chemical composition of the weld zone and improving the joint properties of dissimilar laser welded archwires of these alloys.
S. Azghandirad, M. Movahedi, A. Kokabi, M. Tamizi,
Volume 8, Issue 1 (8-2022)
Abstract
Development of electronic industries, compression of electronic equipment, and removing lead from electronic circuits for environmental issues, resulted in a significant challenge in design and development of tin-based lead-free solders with physical and mechanical properties similar to old tin-lead alloys. In this regard, the set of Sn-Ag-Cu alloys with eutectic and near eutectic compositions have been proposed to replace Sn-Pb solders. As a lead-free solder alloy, low melting point, high reliability, and compatibility with various fluxes are among the properties of this category of alloys. In order to improve the properties of the joint, these solders are sometimes reinforced with different nanoparticles. In this study, Sn0.3Ag0.7Cu compound reinforced with graphene nanosheets with different weight percentages (0, 0.05, 0.1, and 0.2) was studied. Microstructure of the alloys was investigated by scanning electron microscopy(SEM) and optical microscopy. Melting temperature, wetting behavior and electrical resistivity of the solders were evaluated. According to the results, by adding graphene nanosheets, the wetting angle of the solder first decreased and then increased. This parameter showed the optimal amount for sample containing %0.1 graphene nanosheets with a %10 reduction. The melting point and electrical resistance of the solder alloy did not change significantly with compositing. With the addition of graphene nanosheets, the thickness of the intermetallic compounds Cu6Sn5 present at the interface between copper and solder was reduced up to %30.
M. Naseri Alenjagh, T. Saeid,
Volume 9, Issue 1 (5-2023)
Abstract
The purpose of this research is to investigate the change of rotational speed and traverse speed on the microstructure and mechanical properties of the joint in friction stir welding of aluminum 1050 and 316L stainless steel. For this purpose, the microstructure, thickness of intermetallic compounds, hardness and tensile test on the joint were investigated. The proper selection of welding parameters leads to the creation of a joint with suitable metallurgical and mechanical properties. In this research, two rotational speeds of 560 and 900 rpm and four traverse speeds of 60, 80, 100 and 125 mm/min were performed. The microstructure consisted of four areas of the base metal, heat affected zone, thermo-mechanical affected zone and stir zone. In all the samples, the stir zone (SZ) contained a recrystallization microstructure with fine equiaxed grains. According to the Energy dispersive X-ray Spectroscopy results, an IMC layer formed in the joint interface. The hardness of the stir zone in all samples was higher than the aluminum base metal due to the formation of recrystallization fine equiaxed grains and the presence of steel particles. The best sample in terms of mechanical properties, mocrostructure and joint quality was obtained in the conditions of rotation speed of 900 rpm and advance speed of 125 mm/min. The strength was equal to 84 MPa with 77% efficiency.
