Journal of Welding Science and Technology of Iran

The effect of traverse speed in friction stir process on the microstructure, mechanical properties and wear behavior Al5052/ZrO2/ZrSiO4 surface hybrid composite

K. Amini

In the present study, friction stir process (FSP) was used to produce AL/ZrO2/ZrSiO4 surface hybrid composite at a fixed rotation speed of 1400 rpm and traverse speeds of 20, 25, 31.5 and 40 mm/min. Therefore, the purpose of the mentioned study is to investigate the effect of tool traverse speed on the microstructure, hardness and wear behavior of the above-mentioned surface hybrid composite and compare it with base material aluminum 5052. Investigations showed that as a result of FSP operation, a fine-grained structure is created, which improves the hardness and wear resistance of the samples compared to the base sample with the presence of ZrO2 and ZrSiO4 particles. Also, the results showed that among the FSP samples, the sample with a speed of 20 mm/min has the highest hardness and wear resistance. The reason for this is that in this sample, due to the lower traverse speed compared to other samples, more heat has been generated, which has led to more suitable particle distribution and more fine particles. Therefore, in the sample with the traverse speed of 20 mm/min, the hardness and wear resistance increases by 27.3% and 68.9% respectively compared to the base material sample. Also, the examination of the wear surfaces of the samples showed that the wear mechanism in the base sample is strong adhesive wear, and as a result of the FSP operation and surface compositing due to the fineness of the grains and the increase in hardness, the wear mechanism has become weak adhesive, so the wear resistance of the sample is FSPs have been improved.

Evaluation of tribological behaviors of Inconel 625 cladding on same substrate cladded by direct laser deposition process

M. Rajabi

Reconstruction of parts using direct laser deposition can create a combination of high wear resistance properties, good toughness, and corrosion resistance. In this research, the wear properties of Inconel 625 powder cladding on the same substrate have been investigated; For this purpose, room temperature and high temperature wear tests have been used. Mass reduction, friction coefficient, width and depth of wear penetration have been measured. Also, a scanning electron microscope with an energy disspersive spectroscopy system was used to evaluate the cladding surface. The results showed that the mass reduction due to wear at Inconel 625 cladding compared to Inconel 625 substrate has decreased by 7% and 52%, respectively, at temperatures of 25°C and 620°C. Also, the wear mechanism of the room temperature of the cladding is mainly scratchy, and the wear mechanism of high temperature is mainly sticky.

Investigating the microstructure, mechanical properties and corrosion behavior of dissimilar welding of biodegradable magnesium alloy AZ31 to Ti-6Al-4V alloy by friction welding

M. Kasiri-Asgarani

In this research, dissimilar joining of biodegradable AZ31 alloy to Ti-6Al-4V titanium alloy by rotary friction welding method was investigated with aim of preparation of pin or screw for orthopedic applications. optical and scanning electron microscope (sem) were used to investigate the microstructure, x-ray diffraction was conducted for phase analysis, torsion and micro-hardness tests were carried out to investigate mechanical properties, and polarization and electrochemical impedance spectroscopy were employed to evaluate corrosion resistance. in the welding procedure, rotational speed of 1100, 1200 and 1300 rpm and friction time of 2 and 4 seconds were considered as variable parameters, and two parameters of friction pressure and forge pressure were considered as constant parameters at 50 and 40 MPa, respectively. The microstructure of the joint zone showed that there is no deformation in the titanium alloy side. However, in the magnesium side, the greatest amount of deformation occurred with the distance from the joint line, where weld center zone (CZ), dynamic recrystallization zone (DRX), thermomechanical affected zone (TMAZ) and partial deformation zone (PDZ) are detected. The formation of intermetallic phases such as Mg2AlZn, Ti3Al and also the refining the grains size is the main reason for increasing the hardness of the magnesium side near the joint line up to 150 HV. The results of the torsion test showed that the welded sample has the highest shear strength of 81.51 MPa and also the highest corrosion resistance among other samples at a rotation speed of 1200 rpm and a friction time of 4 seconds.

Microstructural and mechanical properties of dissimilar joining of AA5052 and AA6061 by friction stir welding

A. Farzadi

5xxx and 6xxx series alloys are among the most widely used aluminum alloys in various industries, including automobile, shipbuilding and aviation industries. In this research, the joint of two alloys AA6061-T6 and AA5052-H12 was investigated at 4 transmission speeds of 60, 90, 120 and 180 mm/min and 3 rotation speeds of 600, 800 and 1000 rpm. These investigations were carried out in the condition that each of the two alloys was placed in two progressive and regressive sides. The results of these studies showed that the highest tensile strength is when the AA5052 sample is placed on the advancing side and the transfer speed is 90 mm/min and the rotation speed is 600 rpm, and in this case, the final tensile strength value is equal to 197 MPa. In addition, the results showed that, generally, the tensile strength decreases with an increase in the transmission speed at a constant rotational speed, and with an increase in the rotational speed at a constant transmission speed, the tensile strength increases. In addition, microscopic and macroscopic examination of the sections of all samples was performed and various areas and defects were examined. According to the investigations carried out on the microstructure, the grain size in the weld nugget compared to the base metal, HAZ and TMAZ decreases. The grain size in HAZ is the largest in all samples, and this causes a decrease in weld strength in this zone.

The effect of the FSW variables on the microstructure and mechanical properties of the AZ91/CP-Ti joint

H. Sabet

In this study the effect of rotational speed and tool angle parameters on the microstructure and mechanical properties of the AZ91/CP-Ti joint was investigated, for this reason the sheets with 4 x 26 x 100 mm dimensions were prepared and joint by FSW with different rotational speed (800, 1200 and 2500 rpm) and the tool angle (0.5, 1 and 3 degrees). After joining, the samples were cut and prepared for study of microstructural and mechanical properties. OM and SEM examination shows that the structure of AZ91/CP-Ti nugget zone includes alpha grains and the microstructure of the mix zone on the AZ91 side includes α-magnesium coaxial grains with Mg17Al12 intermetallic compounds. The results of the tensile test show that the maximum tensile strength value (160 MPa) related to the rotation speed of 2500 rpm and the tool angle of 1 degree. It was also determined that the rotation speed of 800 rpm was not suitable for joining of AZ91/CP-Ti. On the other hand, it was observed that by increasing the tool angle the work piece, initially leads to an increases the strength from 141 MPa to 160 MPa and then decreases to 132 MPa. the results of the Vickers hardness test show that the average of the nugget zone hardness was to 173, which is higher than the hardness of AZ91 alloy (61 Vickers) and near to the hardness of CP-Ti (167 Vickers).

Investigating the microstructure and mechanical properties of pulsed Nd:YAG laser welding of Monel 400 to Nimonic 75

S. A.Asghar Akbari Mousavi

In this study, non-homogenous welding of nimonic 75 superalloy to Monel 400 with 1 mm thickness was investigated with pulsed Nd:YAG laser welding. The mechanical properties of the joint were analyzed with optical and scanning electron microscope, X-ray diffraction, micro-hardness test and tensile test. In the case of non-homogeneous welding of Nimoinc 75 superalloy to Monel 400, defects such as liquation cracks and porosity in the welded samples were observed. these defects were removed with increasing the preheating temperature and decreasing the heat input. The results showed the voltage, pulse width, pulse frequency and welding speed should be selected as 500 volts, 9 milliseconds, 3 Hz and 0.9 mm/s respectively to reach the proper penetration depth. Also, the investigations show that the welding structure is composed of austenitic matrix containing columnar dendrites and some cellular areas. The mechanical properties of the weld metal were reduced after joining and segregation causes a change in the amount of elements and the appearance of intermetallic compounds in the spaces between dendrites and cells. All non-homogeneous samples broke during the tensile test from the weld metal area.

Similar jointing of Inconel 600 super alloy using nano stracture powder filler with high entropy design

H. Khorsand

High entropy alloys are especially suitable for use as filler metals in brazing due to their excellent properties. in the present study, three powders with the composition of CoxCrxCuxFexMnxNix (X atomic percentage of the element) were designed using the criteria of these alloys as well as jmatpro software. in the next step, using mechanical alloying, filler nano powder was synthesized and characterized by X-RAY analysis (XRD) test and the effect of filler composition on the thermal behavior of the alloy was studied. then the filler was used in Inconel 600 super alloy brazing, the single-phase solidification behavior and the absence of boron and silicon in the high entropy filler led to the creation of a continuous microstructure without eutectic components or brittle phases in the brazing interface. thus, the shear strength test was performed and 545 MPa was the highest shear strength obtained among the three filler compounds. in brazing conventional filler metal, incomplete isothermal solidification and subsequent thermal solidification of the residual liquid results in large grains of chromium-rich boride phase distributed throughout the microstructure. not using compounds that lower the melting point in the filler for the purpose of joining the nickel-based superalloy is considered an important step in reducing the subsequent brazing processes.

Optimization of performance of artificial neural network for predicting the tensile properties of friction stir welded al-5083

M. Mosallaee

In this research, the optimization of the artificial neural network (ANN) capability for predecting the tensile strength and elongation of friction stir welded Al-5083 (FS-welded Al-5083) was carried out. The effective parameters of ANN, such as the number of layers, number of neurons in hidden layers, transfer function between layers, the learning algorithm and etc. were investigated and the efficient neural network was determined to predict the tensile properties of FS-welded Al-5083. The investigations revealed that the perceptron neural network with two hidden layers and 17 neurons numbers, Lunberg-Marquardt training algorithm and Logsig transfer function for the intermediate layers and Tansig transformation function for the output layer is the most optimized neural network for the prediction. The optimized network has an optimal structure based on the minimum value of the mean square error of 0.05, the maximum total correlation coefficient of 0.93 and the line regression with an angle of 45 degrees between the actual and estimated values. Therefore, this network has a good performance for training, generalizing and estimating of tensile strength and elongation of FS-welded Al-5083.

Brazing of 17-4 PH stainless steel to Ti-6Al-4V alloy using BNi-2 filler metal

H. Naffakh-Moosavy

In this research, the effect of temperature and time parameters are investigated on the microstructure and mechanical properties of dissimilar brazing of 17-4 PH stainless steel and Ti-6Al-4V alloy with BNi-2 filler metal. The microstructure of the joint is evaluated with optical and scanning electron microscopes and the mechanical properties of the joint are also evaluated with tensile-shear and microhardness tests. It can be seen that at a constant temperature of 1050°C, increasing the time from 15 to 30 minutes decreases the shear strength from 34.66 to 29.39 MPa. Formation of brittle intermetallic compounds like NiTi2 and FeTi2 increase strength and promote brittle fracture.At a fixed time of 15 minutes, increasing the temperature from 1050 to 1100 °C causes the strength to increase from 34.66 to 38.46 MPa. Also, the increase in temperature and time increases the ISZ thickness formed in the joints on the side of the filler metal - Ti-6Al-4V from 41.40 to 81.48 microns. The increase in temperature and time also causes more diffusion of boron into the SS-filler joint, which forms various boron compounds and widens this region.

Study of microstructure, phase transformation and high temperature strength of hastelloy X and Ni3Al joint by TLP process

Ali Kaflou

In this study, mechanical properties of the transient liquid phase (TLP) bonds between Hastelloy X to Ni3Al IMC at temperature range of 800 - 900 °C were investigated. The microstructure of the joints was examined by optical and scanning electron microscopy. Also, high temperature XRD (HTXRD) analysis was utilized to investigate the phase changes at different temperatures of half-joints. According to microscopic observations, the joint cross-section consisted of three regions including diffusion affected zone (DAZ), isothermal solidification zone (ISZ), and Athermal solidification zone (ASZ), which increasing temperature and time result in ISZ consisting of nickel-rich solid solution developed across the microstructure. The optimum joint bonding strength was achieved for the sample treated at 1100 °C – 180 min equal to 355 ± 4.5 MPa. The ultimate tensile strength reached 36.5 ± 1 and 20.5 ± 1 MPa at temperatures of 800 °C and 900 °C, respectively. Fracture occurred on the side of the IMC substrates at both test temperatures due to the presence of shrinkage porosity during the solidification stage of IMC and crystal lattice parameters mismatch with the matrix.

Microstructural characterization of the effect of energy density on direct laser deposition of stellite 6 on 316 stainless steel

R. Shoja-Razavi

316 steel is used in transportation, space, and chemical equipment. This steel is in demand in these industries due to its durability. It is used to increase the lifespan and renovate equipment. The research explores the impact of laser energy density on st6 cladding. It specifically focuses on the microstructure and geometric characteristics of the cladding. The cladding is applied on 316 steel. The experiment was designed with energy density changes from 40 to 116 J/mm and powder rate changes between 12 and 20 g/min. Optical and electron microscopic images were used to evaluate the samples. The results indicated that the dendritic arms grew larger with increased energy density. The dimensions increased from 1.5 to approximately 3. In other words, the speed of cooling is doubled. Increasing energy density from 40 to 75 J/mm reduced cobalt to chromium ratio from 2 to 0.7. It also decreased cobalt to iron ratio from 35 to 3. The changes emphasize how energy density affects microstructure and phase transformations.

Investigation of weld bead geometry and microstructures of 316L stainless steel in Activating flux TIG Welding using ultrasonic vibrations

F. Kolahan

In this study, we employed the active TIG method with ultrasonic vibration (UV) for welding 316L steel. Throughout the active tungsten inert gas (A-TIG) welding process, a high-frequency ultrasonic generator produced high-intensity acoustic waves at an optimal frequency of 20.3 kHz and a vibration amplitude of 8 micrometers. These waves were directed into the molten weld pool, covered by SiO2 nanoparticles serving as an activating flux. The effect of UV and nanoparticles on weld geometry and weld microstructure was analyzed and compared with conventional TIG welding proces. The results indicated that the use of nanopowder not only increased weld penetration by approximately 17.5% but also reduced the Weld Bead Width (WBW) by 28% compared to Conventional TIG. These values increased by 25% and decreased by 35%, respectively, in the presence of ultrasonic waves. Additionally, the introduction of nanomaterials into the molten pool led to finer grains. The ultrasonic waves played a crucial role in ensuring the uniform distribution of these nanomaterials in the melt, ultimately resulting in an enhanced microstructure of the weld.