R. Hedayatnejad, H. Sabet, S. Rahmati, A. Salemi Golezani,
Volume 8, Issue 2 (1-2023)
Abstract
This research examines the microstructure and microhardness in the additive manufacturing process using the laser metal deposition method with the deposition of Inconel 718 powder on the Inconel 738 substrate. For this purpose, deposition with different laser power was performed on different substrates, and the microstructure and hardness of the layers were studied. Three layers of Inconel 718 powder were deposited on the substrates. The results show that the laser power parameter in the deposition process significantly affects the microstructure of the samples. By increasing the laser power by 100 W, the distance between the phases γ' in the substrate and γ'' in the layers decreased significantly. With increasing laser power, an increase in the geometric dimensions and volume percentage of the γ'' phase was also observed. In addition, increasing the laser power decreased the volume percentage of the Laves phase. By measuring the microhardness of the deposition layers, it was found that the hardness of the third layer decreases with increasing laser power.
M.r. Maraki, M. Mahmoodi, M. Yousefieh, H. Tagimalek,
Volume 8, Issue 2 (1-2023)
Abstract
In Wire and arc additive manufacturing (WAAM) based on Gas metal arc welding (GMAW) is one of the methods of manufacturing metal layer by layer. One of this method's basic steps is predicting the welding geometry created in each welding step. In the current research, an experimental study was conducted in this field considering the effective parameters of welding geometry. For this purpose, three parameters of voltage, welding speed, and wire feeding speed were considered as effective parameters on the welding geometry of the process. The width and height of the weld bead was selected as the answer according to the type and application of the research. The least squares support vector machine was used to model the welding geometry in the process. The results obtained from the regression (R2) of train, test, validation, and total were 0.945, 0.793, 0.894, and 0.881 respectively. The comparison between the experimental data and the model data shows the significance of the proposed model.
M. Ahmadi, H.r. Ahmadi, M.r. Khanzadeh, H. Bakhtiari,
Volume 9, Issue 1 (5-2023)
Abstract
In this research, friction stir welding of aluminum 1050 to copper with variable speed was investigated. For friction stir welding, rotational speeds of 900 and 1200 rpm and traverse speeds of 36, 63, and 125 mm/min were used. In order to check the phases and microstructure, scanning electron microscope analysis, X-ray spectrometry, and hardness testing were used. The disturbance zone included Al2Cu3, Al4Cu9, AlCu4, Al2Cu, and AlCu phases. The results showed that the formation of intermetallic phases and severe plastic deformation in the welding area caused an increase in hardness. The highest hardness value in the stirred area was 97.8 Vickers at a rotation speed of 900 rpm and an advance speed of 36 mm/min.
A. Lalpour, M. Mosallaee, A. Ashrafi,
Volume 9, Issue 1 (5-2023)
Abstract
In the present study, friction stir processing (FSP) technique was carried out on the AA2024 sheet at different traverse speed (63 to 250 mm/min) and rotation speed (315 to 800 rpm). The temperature and grain size of stirred zone (SZ) were measured and their relationship was analyzed and effect of FSP parameters on the grain size of SZ was determined. Experiment and analytical investigations revealed that SZ grain size complies the exponential temperature-dependent relationship and can be defined the mathematical equation. Calculations indicate that a change in operational variables (rotation and traverse speeds) makes no variation in strain rate, and it is constant.
M. Safari, A. Ahadi,
Volume 9, Issue 1 (5-2023)
Abstract
In the present research, the coating process of Inconel 718 powder on the H13 steel substrate by direct powder deposition method with the help of 1 KW continuous fiber laser has been investigated. Hence, the effects of process parameters such as laser power, powder feed rate and laser scanning speed on the geometrical characterstics of the clad such as height and width of the clad are examined. In order to perform a comprehensive investigation on the effect of input parameters and their interactions on the height and width of the clad, design of experiment method based on response surface methodology is employed. The results show that the laser scanning speed and powder feed rate are as the important factors affecting the clad height, so that the clad height increases with increasing powder feed rate and decreasing laser scanning rate. Also, it is proved that by increasing the laser power and decreasing the laser scanning speed the width of the clad is increased.
A. Mahdavi Shaker, H. Momeni, A. Khorram, A. Yazdipour,
Volume 9, Issue 1 (5-2023)
Abstract
This study aimed to investigate the effect of electron beam welding parameters on the microstructural characteristics and mechanical properties of the dissimilar joint between 17-4PH stainless steel and Ti6Al4V alloy. For this purpose, the welding of these two alloys was performed with an copper interlayer with a thickness of 1 mm. Two different welding speeds of 0.7 and 0.9 m/min with four levels of beam offset (0, 0.2, 0.4 and 0.6 mm) from the center of the interlayer towards the steel were used to accomplish the experiments. The results show that by using the copper interlayer with thickness of 1 mm, the cracks caused by the formation of intermetallic compounds are removed from the weld pool. At the interface between the titanium and the weld pool, at the beam offset of 0 and 0.2 mm, a solid solution of copper and TiCu2 intermetallic compounds is formed, while at the beam offset of 0.4 and 0.6 mm, a solid solution of copper and TiCu intermetallic compounds is formed. The weld pool, at the beam offset of 0 and 0.2 mm, consists of TiCr2+TiFe2 intermetallic compounds while at the beam offset of 0.4 and 0.6 mm, solid solution of iron (α-Fe), solid solution of copper and TiCu intermetallic compounds are formed. The highest value of hardness is observed at the interface between the weld pool and the titanium alloy, as well as at the interface between the weld pool and the steel, which is due to the presence of intermetallic compounds with high hardness in these regions. By increasing the welding speed and the beam offset, the hardness value decreases, which is due to the reduction of brittle intermetallic compounds in the joint structure. By increasing the beam offset from 0.4 mm to 0.6 mm at the speed of 0.7 m/min, the shear strength increases from 180 MPa to 210 MPa and at the speed of 0.9 m/min, the shear strength raises from 230 MPa to 250 MPa. The welded sample with the welding speed of 0.9 m/min and the beam offset of 0.6 mm has the highest shear strength equal to 250 MPa. The failure in all samples happened at the interface between the weld pool and the titanium alloy, which shows that the weakest region in the joint is this interface.
M. Niazi, A. Afsari, Seyed A. Behgozin, M. R. Nazemosadat,
Volume 9, Issue 1 (5-2023)
Abstract
Optimization of Stir Friction Welding parameters such as linear and rotational speed of the tool can be effective to a large extent in improving welding properties. In this research, welding of two sheets of Aluminum of Al-7075 and Al-6061 were validated based on theoretical relations and numerical simulation. The simulation of the contact characteristics of the workpieces with the tool was done using the contact algorithms available in the Ansys software. From the FEM, rotational and linear speed and diameter of the tool were selected as design variables, and multi object optimization was carried out with genetic algorithm and RSM to reach the lowest tool temperature and residual stress.The parametric analysis of FSW of the threaded and non-threaded tool pins showed that the generated heat has proportional and inverse relation with rotation and linear speed of tool respectively. Tool with a diameter of 20 mm showed minimum residual stress in the workpiece. By increasing welding speed, the temperature curves become more compact and the effect of thread on heat generation was more evident in all cases at lower heat input.
M.r. Borhani, S.r Shoja-Razavi, M. Erfanmanesh, F. Kermani, S.m. Barekat ,
Volume 9, Issue 1 (5-2023)
Abstract
Inconel 713LC super alloy is one of the most widely used high-temperature alloys. Due to the high level of gamma prime phase caused by Ti and Al alloy more than a critical value, this alloy is considered as one of the non-weldable alloys. One of the basic repair methods of this series of superalloys is laser cladding methods. In this research, the IN713LC substrate was reconstructed with Inconel 625 powder by a direct laser deposition system. To characterize, optical and electron microscopy tests, porosity measurement, and XRD were carried out; The results showed that the R (growth rate of the dendrite tip) increases at high speeds of laser cladding; as a result, the G/R (combined solidification point) ratio decreases, and the structure tends towards the coaxial dendritic direction. For this reason, by increasing the speed of laser scanning from 4 to 6 mm/s, the coaxial dendritic structure increases. The hardness measurement results indicate a decrease in the hardness up to the junction area from 430 to 370 Vickers and fluctuations of about 50 Vickers. Due to the high solidification speed, the average distance between the secondary dendritic arm space was 0.8 at the bottom, 1.01 in the middle, and 1.75 micrometers at the top of the sample. Due to the high cooling speed, only carbides and lava phases are formed. Also, the porosity measurement results of the cladding indicate a maximum porosity of 0.1 percent.
M. Naseri Alenjagh, T. Saeid,
Volume 9, Issue 1 (5-2023)
Abstract
The purpose of this research is to investigate the change of rotational speed and traverse speed on the microstructure and mechanical properties of the joint in friction stir welding of aluminum 1050 and 316L stainless steel. For this purpose, the microstructure, thickness of intermetallic compounds, hardness and tensile test on the joint were investigated. The proper selection of welding parameters leads to the creation of a joint with suitable metallurgical and mechanical properties. In this research, two rotational speeds of 560 and 900 rpm and four traverse speeds of 60, 80, 100 and 125 mm/min were performed. The microstructure consisted of four areas of the base metal, heat affected zone, thermo-mechanical affected zone and stir zone. In all the samples, the stir zone (SZ) contained a recrystallization microstructure with fine equiaxed grains. According to the Energy dispersive X-ray Spectroscopy results, an IMC layer formed in the joint interface. The hardness of the stir zone in all samples was higher than the aluminum base metal due to the formation of recrystallization fine equiaxed grains and the presence of steel particles. The best sample in terms of mechanical properties, mocrostructure and joint quality was obtained in the conditions of rotation speed of 900 rpm and advance speed of 125 mm/min. The strength was equal to 84 MPa with 77% efficiency.
A. Gandomdoust, M. Sarkari Khorrami, S. F. Kashani-Bozorg, H. Ghorbani,
Volume 9, Issue 1 (5-2023)
Abstract
As one of the important pillars of the fourth industrial revolution, metal additive manufacturing (AM) technologies provide a disruptive approach to digital manufacturing. Laser powder bed fusion (LPBF), as one of these technologies, has great potential in producing geometrically complex and high-performance parts. In recent years, the manufacturing of aluminum alloy parts using this technology has attracted much attention. However, their manufacturing still faces some challenging issues. One of the most serious issues encountered in the manufacturing of aluminum alloys, especially high-strength grades, is solidification cracking. In the present investigation, the formation mechanisms of solidification cracking, and the associated effective factors were reviewed. Controlling the solidification microstructure and grain refinement, using the addition of small quantities (<1 wt.%) of micro- or nano-sized particles to the initial alloying powder, was suggested as the most effective method for reducing solidification cracking. These particles act as nucleation sites, prevent grain growth, pin grain boundaries, and with the help of factors that provide constitutional supercooling can effectively minimize solidification cracking. Eventually, effects of various additives in grain refinement and their associated mechanism in reduction of solidification cracks of high-strength aluminum alloys by LPBF is presented.
N. Abbasian Vardin, T. Saeid, A. R. Akbari ,
Volume 9, Issue 1 (5-2023)
Abstract
In this study, gas-tungsten arc welding was used for the cladding of two high entropy alloys of AlCoCrFeNi (Al1) and Al0.7CoCrFeNi (Al0.7) onto plain carbon steel plates. The welding process was carried out at a welding current of 180 A and a welding speed of 1.4 mm/s. The microstructures, craking behavior, phase composition, and hardness of the clads were characterized using various methods, such as optical microscopy (OM), field emission scanning electron microscopy (FESEM), X-ray diffractometry (XRD) analysis, and microhardness measurements. The results indicated that the Al1 clad had a petal-like structure of the BCC and Cr-rich phases. Both intergranular and transgranular cracks were identified in the Al1 alloy, which were recognized to be solidification cracks. Thermal stress and brittleness of the BCC phase promote cracking of the Al1. On the other hand, in the Al0.7 alloy, in addition to the BCC phase, a new FCC phase was formed with various Widmanstatten and dendritic morphologies in the clad microstructure and the Cr-rich phase was not observed. Furthermore, in this alloy with lower Al content, a crack-free clad was obtained. The crack prevention in the Al0.7 alloy was attributed to a combination of factors, including a decrease in the solidification range, formation of the FCC phase, and reduction in hardness.
M.h. Nourmohammadi, M. Movahedi, A.h. Kokabi, M. Tamizi,
Volume 9, Issue 1 (5-2023)
Abstract
The miniaturization and compaction trends in electronic equipment and the removal of lead (Pb) element from solder alloys due to environmental considerations have created a great challenge in the field of designing and developing of new solder alloys. Therefore, researchers have recently focused on composite solder alloys using reinforcing particles to improve the reliability of lead-free solders. In this research, SAC0307 solder alloys (99 wt.% Sn, 0.3 wt.% Ag, and 0.7 wt.% Cu) with different percentages of cobalt microparticles were made by the Accumulative Roll Bonding (ARB) method. Then, the effect of the particles on wettability, microstructures and mechanical characteristics of solder alloys was investigated. The lowest contact angle was 23◦in 0.2 wt.% cobalt sample. By adding cobalt to the solder matrix, the size of intermetallic compounds (IMCs), Cu6Sn5 and Ag3Sn, decreased and the percentage of eutectic phases increased. The shape of the interfacial intermetallic compounds changed from scallop to layer shape by adding cobalt, and their average thickness increased about 13-71% in composite samples. The shear strength of solders increased up to 38% by enhancement of cobalt microparticles in the solder alloy containing 0.4 wt.% cobalt; however, shear strength was decreased in the composite solder containing 1 wt.% cobalt due to the agglomeration of microparticles. The shear fracture surfaces showed that the nature of the fracture changed from ductile fracture in the form of elongated dimples to brittle fracture in the form of cleavage with the increase in the percentage of cobalt microparticles. The composite solder alloys containing 0.2-0.4 wt.% Co have the best wettability behavior and tensile shear strength.
Gh. Khalaj, A. Fadaei,
Volume 9, Issue 1 (5-2023)
Abstract
In this research, the effect of post weld heat treatment on the microstructure and mechanical properties of the three-layer explosion welding joint of austenitic steel 321-aluminum 1050-aluminum 5083 was investigated. The welded samples were heat treated at 250 and 350°C for 10000 seconds. The structure and properties were investigated using optical microscope, scanning electron microscope, microhardness measurement and shear-compressive strength. The results showed that in all conditions, the interface of aluminum 5083-aluminum 1050 was smooth and with complete continuity; However, the interface between stainless steel 321 and aluminum 1050 had a reaction layer with variable and discontinuous thickness. During the heat treatment, the thickness of the interface layer increases according to the diffusion kinetics and reaches 18.6 microns in the maximum value. With the increase of heat treatment temperature, the average concentration of aluminum in the reaction layer of the interface increased from 85% to more than 90%, but the concentration of iron decreased from 10% to less than 5%. Also, shear-compressive strength decreases from 94.6 to 56.7 MPa.
L. Gadami Domabi, S. M. Rafiaei, S. Jahanbazi Gojani,
Volume 9, Issue 1 (5-2023)
Abstract
In this paper the production of chitosan and polylactic acid polymer scaffolds containing zinc oxide particles was carried out through the 3D printer method. Zinc oxide particles were processed through combustion synthesis method. According to the XRD results, the produced oxide has a high phase purity, and the evaporation of volatile impurities and the increase of crystallinity happened via performing the calcination process. In the X-ray diffraction pattern of PLA/ZnO/Chitosan, the broad peak in the range of 10-25 degrees indicates the amorphousness of the background polymer, and with the addition of ZnO, sharp and powerful peaks have appeared in the graph. The SEM images of zinc oxide synthesized by combustion method also showed that the size of ZnO nanoparticles is approximately 50 nm, while after the calcination heat treatment, the size of the particles increased greatly and reached an average size of 130-160 nm. Finally, the microscopic images obtained from the surface of scaffolds possessing 10% zinc oxide, 5% chitosan and polylactic acid showed that by optimizing the 3D printer, ZnO particles are uniformly dispersed in PLA/Chitosan polymer field.
Farzad Shahin, Ehsan Baharzadeh, Mahdi Rafiei, Hossein Mostaan,
Volume 9, Issue 2 (8-2024)
Abstract
In this study, formation of Fe3Al and (Fe,Cr)3Al intermetallic compounds and the effect of Cr on microstructural and mechanical properties of Fe-Al cladding system such as hardness and wear resistance, were evaluated. For this purpose, first, iron and aluminum powders were mixed without chromium powder and in the second stege with the addition of chromium powder in high energy planetary ball mill, and Fe3Al and (Fe,Cr)3Al intermetallic compounds were synthesized. The preplaced powders were cladded on the surface of CK45 steel using gas tungsten arc welding process. The microstructure, formed phases and properties of the cladded layers were studied by optical microscope, scanning electron microscope, X-Ray Diffraction, micro and macro hardness, energy dispersive X-ray spectroscopy (EDS) and pin on disk wear test at temperatures of 25, 250, and 500 ᵒC. It was found that the microstructure of Fe-Al binary cladding contained Fe3Al dendrites with non-epitaxial growth. This non-epitaxial growth resulted from the difference in the chemical composition of the coating and the substrate at the interface between the coating and the substrate, which caused the formation of new crystals at the interface. However, the microstructure of Fe-Al-Cr ternary cladding contained martensitic blades within (Fe,Cr)3Al matrix. The results of hardness tests revealed that the hardness of ternary cladding is twice as compared with the binary cladding (30 and 60 HRC for binary and ternary claddings, respectively). Also it was found that the presence of Cr element in Fe-Al cladding improved the wear resistance of deposited layers. The predominant wear mechanism of Fe3Al pin was adhesive, while for (Fe,Cr)3Al pin moreover adhesive wear, micro-plowing abrasive wear was also seen. The mass losses of both pins were maximum at ambient temperature and minimum at temperature of 500 oC.
Ms Majid Rahimi, Dr. Mahdi Omidi, Dr. Saeid Jabbarzare, Dr Hamid Reza Bakhsheshi-Rad, Dr. Masoud Kasiri-Asgarani, Dr. Hamid Ghayour,
Volume 9, Issue 2 (8-2024)
Abstract
In this research, copper/silver-silicon carbide Cu-Ag-SiC composite was prepared by the friction stir processing (FSP). For this purpose, nanometer and micrometer SiC particles were used as reinforcing particles. In order to evaluate the microstructural properties, X-ray diffraction (XRD) analysis, scanning electron microscope and optical microscope were employed. Evaluation of mechanical properties through microhardness measurement, tensile test and pin on disc test were utilized to evaluate the wear behavior of the composite. The results of X-ray analysis revealed the presence of two phases of CuAg solid solution along with SiC particles, which indicated the formation of Cu-Ag-SiC composite. The addition of nano-particles led to a significant decrease in the intensity of peaks compared to micro-particles. This indicated a decrease in the grain size of the CuAg matrix. Using the FSP in the presence of reinforcing particles and without it led to a decrease in the crystal size and average grain size compared to the sample without FSP. So that the grain size of the sample without FSP and the FSPed sample without reinforcing particles and with nano-reinforcing particles were found to be about 46.3, 19.2 and 3.6 µm, respectively. The wear mechanism in the sample before FSP was adhesive wear due to its soft nature of the matrix, and after FSP in the sample without reinforcing particles, the adhesive wear decreased and due to the addition of silicon carbide micro and nano- particles reinforcement, the wear mechanism in entirely altered to abrasive wear. Overall, it can be stated that the addition of silicon carbide nanoparticles by FSP leads to the fabrication of Cu-Ag-SiC composite with high mechanical properties.
M. R. Borhani, M. Rajabi, R. Shoja Razavi, R. Jamaati,
Volume 9, Issue 2 (1-2024)
Abstract
Reconstruction of parts using direct laser deposition can create a combination of high wear resistance properties, good toughness, and corrosion resistance. In this research, the wear properties of Inconel 625 powder cladding on the same substrate have been investigated; For this purpose, room temperature and high temperature wear tests have been used. Mass reduction, friction coefficient, width and depth of wear penetration have been measured. Also, a scanning electron microscope with an energy disspersive spectroscopy system was used to evaluate the cladding surface. The results showed that the mass reduction due to wear at Inconel 625 cladding compared to Inconel 625 substrate has decreased by 7% and 52%, respectively, at temperatures of 25°C and 620°C. Also, the wear mechanism of the room temperature of the cladding is mainly scratchy, and the wear mechanism of high temperature is mainly sticky.
M.r. Hajiha, A. Farzadi, S. A. Samadani Agdam, A. Shabanzadeh, S. Ramezani,
Volume 9, Issue 2 (1-2024)
Abstract
5xxx and 6xxx series alloys are among the most widely used aluminum alloys in various industries, including automobile, shipbuilding and aviation industries. In this research, the joint of two alloys AA6061-T6 and AA5052-H12 was investigated at 4 transmission speeds of 60, 90, 120 and 180 mm/min and 3 rotation speeds of 600, 800 and 1000 rpm. These investigations were carried out in the condition that each of the two alloys was placed in two progressive and regressive sides. The results of these studies showed that the highest tensile strength is when the AA5052 sample is placed on the advancing side and the transfer speed is 90 mm/min and the rotation speed is 600 rpm, and in this case, the final tensile strength value is equal to 197 MPa. In addition, the results showed that, generally, the tensile strength decreases with an increase in the transmission speed at a constant rotational speed, and with an increase in the rotational speed at a constant transmission speed, the tensile strength increases. In addition, microscopic and macroscopic examination of the sections of all samples was performed and various areas and defects were examined. According to the investigations carried out on the microstructure, the grain size in the weld nugget compared to the base metal, HAZ and TMAZ decreases. The grain size in HAZ is the largest in all samples, and this causes a decrease in weld strength in this zone.
R. Mahdizade, S. A.asghar Akbari Mousavi, S. Mehdipour,
Volume 9, Issue 2 (1-2024)
Abstract
In this study, non-homogenous welding of nimonic 75 superalloy to Monel 400 with 1 mm thickness was investigated with pulsed Nd:YAG laser welding. The mechanical properties of the joint were analyzed with optical and scanning electron microscope, X-ray diffraction, micro-hardness test and tensile test. In the case of non-homogeneous welding of Nimoinc 75 superalloy to Monel 400, defects such as liquation cracks and porosity in the welded samples were observed. these defects were removed with increasing the preheating temperature and decreasing the heat input. The results showed the voltage, pulse width, pulse frequency and welding speed should be selected as 500 volts, 9 milliseconds, 3 Hz and 0.9 mm/s respectively to reach the proper penetration depth. Also, the investigations show that the welding structure is composed of austenitic matrix containing columnar dendrites and some cellular areas. The mechanical properties of the weld metal were reduced after joining and segregation causes a change in the amount of elements and the appearance of intermetallic compounds in the spaces between dendrites and cells. All non-homogeneous samples broke during the tensile test from the weld metal area.
M. Bozorgmehr, A. Heidari, K. Amini, M. Loh Mousavi, F. Gharavi,
Volume 9, Issue 2 (1-2024)
Abstract
In the present study, friction stir process (FSP) was used to produce AL/ZrO2/ZrSiO4 surface hybrid composite at a fixed rotation speed of 1400 rpm and traverse speeds of 20, 25, 31.5 and 40 mm/min. Therefore, the purpose of the mentioned study is to investigate the effect of tool traverse speed on the microstructure, hardness and wear behavior of the above-mentioned surface hybrid composite and compare it with base material aluminum 5052. Investigations showed that as a result of FSP operation, a fine-grained structure is created, which improves the hardness and wear resistance of the samples compared to the base sample with the presence of ZrO2 and ZrSiO4 particles. Also, the results showed that among the FSP samples, the sample with a speed of 20 mm/min has the highest hardness and wear resistance. The reason for this is that in this sample, due to the lower traverse speed compared to other samples, more heat has been generated, which has led to more suitable particle distribution and more fine particles. Therefore, in the sample with the traverse speed of 20 mm/min, the hardness and wear resistance increases by 27.3% and 68.9% respectively compared to the base material sample. Also, the examination of the wear surfaces of the samples showed that the wear mechanism in the base sample is strong adhesive wear, and as a result of the FSP operation and surface compositing due to the fineness of the grains and the increase in hardness, the wear mechanism has become weak adhesive, so the wear resistance of the sample is FSPs have been improved.