Journal of Welding Science

---

In this research, gas tungsten arc welding of dissimilar joint between 4130 low alloy steel and AISI 201 austenitic stainless steel was investigated. Four filler metals i. e. ERNiCr-3, ER 309L, ER 308L and ER 80SB2 were used. After welding, microstructural features of various areas and also fracture surfaces were examined using optical microscopy and scanning electron microscopy. Tensile test was conducted in order to study the mechanical properties of each joint. It was found that ERNiCr-3 is fractured from fusion zone and the others were fractured from 4130 base metal. Also, some second phase particles such as NbC were seen in the ERNiCr-3 weld joint. SEM observation showed that the fracture behavior of ERNiCr-3 weld joint is semi brittle and the others are ductile. The fusion zone of ERNiCr-3 weld joint was fully austenitic and consisted of equiaxed grains and no crack was seen in this area. The fusion zone of ER 308L and ER 309L were composed from cellular dendrite and finally ER 80S-B2 weld joint was consisted of lath martensite.

---

In the TIG-MIG hybrid welding, higher weld efficiency and better weld quality are obtained with respect to each individual TIG and MIG welding methods. Moreover, in this method, the MIG arc is more stable in pure argon shielding gas. Therefore, in this study, the influence of TIG-MIG hybrid welding parameters on the welds appearance quality and welds depth to width ratio of a 316L austenitic stainless steel was investigated using optimum parameters of Taguchi design of experiments (DOE). Microstructure of the heat affected zone (HAZ) obtained from the hybrid welding was compared with those of each individual MIG and TIG welding techniques under equal heat-input condition. The results indicated that the most important parameter in the hybrid method to obtain the best appearance quality and the highest depth to width ratio is the distance between the two arcs. The MIG and TIG currents are the next influencing parameters. The width of HAZ and the size of constituent grains in hybrid welding with optimum parameter, were smaller than those of each individual TIG and MIG processes due to the higher associated cooling rate in the hybrid welding technique.

---

In the present study, the effect of time and base metal microstructure on the Transient Liquid Phase (TLP) bonding of 304L stainless steel was studied. TLP was performed at 1050 ⁰C for 5 and 60 minutes on the coarse grain austenitic and martensitic microstructure using BNi-2 interlayer. To prepare martensitic microstructure, as-received 304L was rolled at -15 ⁰C up to 80% rolling reduction. TEM analysis was proved that the microstructure of 80% rolled samples consisted of two different morphologies of martensite namely as lath-type and dislocation cell type martensite.  It was observed that the structure of bonded zone after 5 min has consisted of isothermally solidified zone (ISZ) containing γ solid solution and athermally solidified zone (ASZ) containing complex boride phases. Meanwhile, after 60 min of  heating, the structure of bonded zone completely solidifies isothermally. The obtained results also showed that the martensitic microstructure considerably effect on the width of diffusion affected zone (DAZ) which was related to the reversion of martensite to ultrafine grain austenite during heating.

---

In this study the effect of activating fluxes on the penetration depth, microstructure and microhardness of AISI316L austenitic stainless steel were evaluated by three TIG process variations (TIG, A-TIG and FB-TIG) and the results were compared together.. After selecting the optimal flux in the second stage, the effect of that on the penetration depth, microstructure and weld microhardness of  welded 316L austenitic stainless steel by A–TIG and FB-TIG methods, were evaluated and  the results were compared by the sample which was welded by TIG process. At this stage, it was found that the depth and width to depth ratio in FB-TIG method is slightly greater than the other two methods. Also in FB-TIG method, eqiaxed dendritic zone in the center line of weld is slightly greater than in A-TIG method. Study of microhardness of weld in three methods shows that in A-TIG and FB-TIG methods hardness of center line is more than TIG method.

---

Friction stir welding (FSW) was conducted on AISI 304 austenitic stainless steel plate with 2 mm thickness. The FSW was performed at a welding and rotational speeds of 50 mm/min and 400 rpm, respectively. Microstructure observations by the optical microscopy showed that a severe grain refinement occurred in the stir zone (SZ). Electron backscattered diffraction analysis (EBSD) results indicated that high fraction of low angle grain boundaries (LAGBs) developed in the thermo-mechanically affected zone (TMAZ) through the occurrence of the dynamic recovery. Moreover, in the path from the TMAZ towards the SZ, the fraction of high angle grain boundaries (HAGBs) increased with decreasing the fraction of LAGBs through the occurrence of continuous dynamic recrystallization (CDRX). 100 Pole figure showed the formation of shear texture components of A*1 and A*2 in the SZ which implied the occurrence of CDRX mechanism.
 

---

Dissimilar weld joints between stainless steels and nickel based super alloys are extensively used in petrochemical, gas and oil applications. These joints jave great challenges from metallurgical transformations point of view. In this research, microstructural evolutions and corrosion behavior of laser weld joint between Inconel 625 and AISI 430 ferritic stainless steel were investigated. Ferritic stainless steels are less expensive and have magnetic properties in comparison with austenitic stainless steels. Scanning electron microscope and optical microscope were used in order to study the microstructures of weld metal and heat affected zone. It was found that fine dendritic microstructuresare formed in the weld metal which  isgrown in a competition manner. An epitaxial growth was observed in the interface between AISI base metal and weld metal. No considerable grain growth was observed in the heat affected zone on Inconel 625. Corrosion resistance of weld joint was investigated in 3.5 % wtNaCl solution using potantiodynamic polarization test. It was concluded that corrosion resistance is increased from AISI 430 base metal toward Inconel 625 base metal.
 

---

In this research, dissimilar welding of NiTi shape memory alloy to AISI 304 austenitic stainless steel Archwires was investigated. For this purpose, common straight orthodontic archwire with rectangular cross-section and dimensions of (0.635 × 0.432 mm) were selected and the laser welding technique was used to connect the wires. The microstructure, chemical composition and phasesin the weld zone of the joints werestudied with Optical microscopy (OM), Scanning electron microscopy (SEM) equipped with EDS analysis system, focused X-ray diffraction (Micro-XRD).Also, the mechanical properties of the weld zone were investigated by using Vickers microhardness test. Microstructure investigation showed that the obtained microstructure from the laser weld of these alloys has a dendritic and non-homogeneous structure. According to XRD analysis, brittle intermetallic compounds such as Fe₂Ti, Cr₂Ti, TiNi₃, and Ti₂Ni wereformed during laser welding in the weld zone. Formation of these brittle intermetallics caused increasing the hardness of the weld zoneabout 800 HV. and decreasing the mechanical properties. Also, Fe₂Ti intermetallic particles mainly formed in the weld region near the NiTi fusion zone which results in stress concentration, micro-cracks formation and dropping joints mechanical properties. Therefore, a suitable modification process is required to control the chemical composition of the weld zone and improving the joint properties of dissimilar laser welded archwires of these alloys.

---

Friction stir welding was conducted on AISI 304 austenitic stainless steel sheet with dimensions of
100 mm × 100 mm × 2 mm. The FSW was performed at a welding speed of 150 mm/min and rotational speeds of 400 and 800 rpm. The results showed that high frequency of low angle grain boundaries (LAGBs) were formed through dynamic recovery in the thermo-mechanically affected zone (TMAZ). Higher amount of LAGBs were developed in the TMAZ of welded sample with 800 rpm due to the higher amount of strain and heat generated. High fraction of high angle grain boundaries were formed in the stir zone (SZ) of the welded samples through the occurrence of continuous dynamic recrystallization (CDRX). A very fine microstructure developed in the sampled welded with lower rotational speed. Analysis of texture using {111} Pole figures showed the formation of shear texture components in the SZ of both welded samples. The intensity of the obtained texture for the sample welded with 800 rpm was greater. The formation of shear texture components in the SZ of both samples implied the occurrence of CDRX mechanism

---

In this investigation, the AISI 2205 duplex stainless steel was welded in the form of bead on plate by A-TIG process with different amount of the ZrO2 and TiO2 activated fluxes. The results of the visual inspection showed that the specimen with 50% ZrO2 and 50% TiO2 activated flux, had the lowest face width and the specimen with contains 90% ZrO2 activated flux, had the highest penetration depth. Also, the results showed that the angular distortion of the specimens with mix of the ZrO2 and TiO2 activated flux were 225% less than the specimen without activated flux. The results of macroscopic examination of different samples showed that the maximum length and width of the macroscopic grains were related to the sample with 90% ZrO2 activated flux and the smallest length and width of the macroscopic grains were related to the sample with 90% TiO2 activated flux. The hardness test results showed that the highest hardness of the samples was gained to 90% TiO2 activated flux specimen with 950 HV and the lowest hardness value for the sample with 90% ZrO2 activated flux with 410 HV. The results of all tests showed that surface activated fluxes (ZrO2 and TiO2) affected to the depth of penetration, face width, angular distortion, length and width of macroscopic grains and the hardness of weld metal by changing the longitudinal and transverse melt flow in the weld pool.

---

In this study, the temperature in friction stir welding of duplex stainless steel has been investigated. At first, temperature estimation was modeled and estimated at different distances from the center of the stir zone by the multivariate Lagrangian function. Then, the linear extrapolation method and multiple linear regression method were used to estimate the temperature outside the range and center of the stir zone. Temperature estimation is based on three parameters rotational speed, welding speed and distance from the center of stir zone. In the first method, by generalizing the multivariate Lagrangian method, the multivariate Lagrangian temperature function was generalized according to the above parameters. In the second method, in order to investigate the effect of the variables in the regression model, a comparison of two complete models and a reduced model based on the sum of squares errors was used. Then, by analyzing the multiple regression equations governing the output variable, a multiple linear regression function was introduced. Since the temperature of the stir zone is not measurable by the thermocouple, so in general the best fit curve for estimating the function is when the modeling is based on parameters that minimize the error function.To implement the multiple linear regression method, the error function was introduced to minimize the sum of the error squares and the error derivative was calculated in relation to the parameters of tool rotation speed, welding speed and distance from the center of the stir zone. Therefore, multiple linear regression method was considered as the basic method and as a criterion with other methods. According to the results obtained from the prediction in the center of the stir zone, the temperature difference in all three methods is desirable and negligible. The maximum temperature difference of multiple linear regression method with multivariate Lagrangian method in all nodes was 18.8 ^oC and multiple linear regression method with linear extrapolation method was 26.36 ^oC. Therefore, the multivariate Lagrangian interpolation method is less different than the linear extrapolation method in the center of the stir zone and is more accurate.

---

In this study, diffusion bonding between titanium and AISI 304 austenitic stainless steel by Ag interlayer was investigated. In order to carry out this research, samples prepared after surface preparation were placed inside the fixture and placed at the temperatures of 750,800 and 850 °C in the 30,60 and 90 min in the furnace under argon protective gas. The phase transformation and microstructure of diffusion bonding interfaces of the joints were studied using optical microscopy, scanning electron microscopy and x-ray diffraction. Then, the hardness of the samples was measured using a hardness test apparatus. Finally, the samples were tested after being placed in the shear strength test holder using a pressure test device and the shear strength of the samples was measured. Examination of optical microscopic images shows the diffusion of silver in titanium and the partial diffusion of silver in stainless steel. On the other hand, increasing the temperature increases the diffusion region as well as increasing the grain size in the specimens. SEM images from the samples also confirmed the diffusion of silver in titanium and partially diffusion into stainless steel. The results of the XRD test on the samples showed that the temperature rise to 800 °C leads to the formation of TiAg and Ag₃Fe₂ intermetallic compounds, which the existence of TiAg intermetallic compound increases the hardness of the sample. For this reason, the sample at 800 °C showed the highest hardness. The shear strength of the samples showed that the increase in temperature increased the shear strength of the samples and decreased the shear strength by increasing the temperature above 850 ° C due to the formation of brittle intermetallic compounds.

---

---

---

---

---

---

This research studied the effect of two-stage over aging treatmenton the pitting corrosion behavior and microstructure of the weld metals in the 17-4 precipitation hardening stainless steel. For this purpose, this steel was subjected to solution annealing heat treatment at 1035°C for one hour before welding. Then gas tungsten arc welding (GTAW) was performed using ER630 similar filler metal. Subsequently, a section of the weldment was subjected to two-stage over aging treatment. The microstructure and corrosion resistance of the weld zone after the two-stage over aging treatment were investigated and compared with the weld zone behavior in the as-weld condition. Microstructural studies showed that the two-stage over aging treatment of the weld zone led to the tempering of the martensitic, the formation of more reversed austenite, and the formation of α-ferrite. The volume fraction of austenite in the as-weld condition was approximately 7% and increased to about 30% after two-stage over aging treatment, a four-fold increase. The pitting potential (E_Pit) of weld metal was -18.15 mv in the as-weld condition and reached 122.54 mv after two-stage over aging treatment, which also signifies an improvement in pitting resistance. The two-stage over aging treatment also reduced the potential differences between the different parts of welding zones reducing the galvanic corrosion occurrence. The assessment of mechanical properties through impact test revealed that impact resistance after two-stage over aging treatment can be increased by about 66 % compared to as-weld condition.

---

---

---