B. B. Heidari-Dehkordi, M. Rafiei, M. Omidi, M. Abbasi-Baharanchi,
Volume 10, Issue 2 (12-2024)
Abstract
In this study, 316L stainless steel and WC-10Co cermet were bonded by transient liquid phase process with BNi-2 interlayers with different thicknesses of 25 and 50 μm. The bonding process was conducted at 1050 °C for 1, 15, and 30 min. After bonding, the microstructure of the joints was examined using optical microscopy and scanning electron microscopy equipped with energy-dispersive X-ray spectroscopy. Microhardness and tensile-shear tests were also performed to study the mechanical properties of the bonded samples. Microstructural analyses revealed that the formation mechanism of the solidified region in all samples was isothermal solidification, resulting in an isothermal solidification zone upon bonding. Additionally, the only phase present in the isothermal solidification zone was a nickel-based solid solution. In the diffusion-affected zone of the steel base material, complex borides formed regardless of the interlayer thickness. In the diffusion-affected zone of the WC-Co material, a brittle eta phase formed. Microhardness tests indicated that the maximum hardness in all samples was approximately 1100 Vickers, which was attributed to the presence of hard WC particles in the WC-Co base material. Furthermore, the highest tensile-shear strength, approximately 240 MPa, was observed in the bonded sample for 15 min with 50 μm thickness interlayer.
F. Shahin, E. Baharzadeh, M. Rafiei, H. Mostaan,
Volume 10, Issue 2 (12-2024)
Abstract
In this study, formation of Fe3Al and (Fe,Cr)3Al intermetallic compounds and the effect of Cr on microstructural and mechanical properties of Fe-Al cladding system such as hardness and wear resistance, were evaluated. For this purpose, first, iron and aluminum powders were mixed in the first series without chromium powder and in the second series with the addition of chromium powder in high energy planetary ball mill, and Fe3Al and (Fe,Cr)3Al intermetallic compounds were synthesized. The preplaced powders were cladded on the surface of CK45 steel using gas tungsten arc welding process. The microstructure, formed phases and properties of the cladded layers were studied by optical microscope, scanning electron microscope, X-Ray Diffraction, micro and macro hardness, energy dispersive X-ray spectroscopy (EDS) and pin on disk wear test at 25, 250, and 500ᵒC temperatures. It was found that the microstructure of Fe-Al binary cladding contained Fe3Al dendrites with non-epitaxial growth. This non-epitaxial growth results from the difference in the chemical composition of the coating and the substrate at the interface between the coating and the substrate, which has caused the formation of new crystals at the interface. However, the microstructure of Fe-Al-Cr ternary cladding contained martensitic blades within (Fe,Cr)3Al matrix. The results of hardness tests revealed that the hardness of ternary cladding is twice as compared with the binary cladding (30 and 60 HRC for binary and ternary claddings, respectively). Also it was found that the presence of Cr element in Fe-Al cladding improved the wear resistance of deposited layers. The predominant wear mechanism of Fe3Al pin was adhesive, while for (Fe,Cr)3Al pin moreover adhesive wear, micro-plowing abrasive wear was also seen. The mass losses of both pins were maximum at ambient temperature and minimum at temperature of 500 oC.
A. Heidarzadeh, R. Khajeh, M. Sajed,
Volume 10, Issue 2 (12-2024)
Abstract
In this research, the effect of nickel powder as an interlayer and the tool penetration depth on the microstructure and mechanical properties of lap joints between aluminum 1050 (top sheet) and pure copper (bottom sheet), both with a thickness of 2 mm, was investigated. Nickel powder was added through a machined groove with a width and depth of 1 mm at the base of the aluminum sheet. Friction stir lap welding was performed using a hot work steel tool with a shoulder diameter of 16 mm, a pin diameter of 4 mm, a pin height of 2.1 mm, a rotational speed of 950 rpm, a feed rate of 85 mm/min, a tool tilt angle of 2°, and varying tool penetration depths of 0, 0.05, and 0.1 mm. The results revealed that in the sample with a 0 mm penetration depth, due to insufficient heat generation, defects such as tunnel voids were formed. Increasing the penetration depth to 0.05 mm resulted in the formation of uniform and thin intermetallic layers, including Al3Ni2, Al7Cu4Ni, and Cu3.8Ni at the interface, which enhanced joint quality and increased tensile strength to 185.2 MPa with a fracture strain of 8.7%. In the sample with a 0.1 mm penetration depth, thicker and less uniform intermetallic layers were formed, which, despite locally increasing hardness, led to a decrease in tensile strength and fracture strain to 136.6 MPa and 6.7%, respectively. This study demonstrates that under the conditions of this research, a tool penetration depth of 0.05 mm provides the optimal conditions for FSLW of aluminum-copper alloys using nickel powder.
M. Mizabi Asl, M. Belbasi*,
Volume 10, Issue 2 (12-2024)
Abstract
In this research, the effect of heat input on the microstructure and mechanical properties of the joint of two dissimilar steels D6AC and VCN 200 steel was investigated. For this purpose, the samples were welded with the current intensity of 130, 145 and 160 Ampers by GTAW process and using ER120 SG welding wire with a diameter of 2.4 mm. The metallographic results showed that the microstructure of the weld metal consisted of lath martensite and acicular ferrite phases, which increased the volume fraction of ferrite from 5 to 32% with the increase of heat input, and the morphology of the ferrite changed from acicular to polygonal ferrite due to the decrease in the cooling rate. The HAZ area microstructure consist of bainite, lath martenrite and ferrite. The highest strength value was obtained in the welded sample with low heat input. With the increase of heat input, the tensile strength has decreased from 1154 to 965 MPa. Also, with the increase of heat input, the impact energy has increased in the welding zone due to the increase of stable phases, and in the HAZ zone due to the growth of the primary austenite grains and the reduction of the grain boundary locking effect. The results of the fracture analysis showed that the fracture occurred in the weld zone with low heat input, brittle fracture, and in the HAZ area, combination of ductil and brittle fracture occurred. With the increase in heat input, dutil fracture occurred in the welding zone and brittle fracture occurred in the HAZ zone due to grain growth.
M. Rahimi, M. Omidi, S. Jabbarzare, H. R. Bakhsheshi-Rad, M. Kasiri-Asgarani, H. Ghayour,
Volume 10, Issue 2 (12-2024)
Abstract
In this research, copper/silver-silicon carbide Cu-Ag-SiC composite was prepared by the friction stir processing (FSP). For this purpose, nanometer and micrometer SiC particles were used as reinforcing particles. In order to evaluate the microstructural properties, X-ray diffraction (XRD) analysis, scanning electron microscope and optical microscope were employed. Evaluation of mechanical properties through microhardness measurement, tensile test and pin on disc test were utilized to evaluate the wear behavior of the composite. The results of X-ray analysis revealed the presence of two phases of CuAg solid solution along with SiC particles, which indicated the formation of Cu-Ag-SiC composite. The addition of nano-particles led to a significant decrease in the intensity of peaks compared to micro-particles. This indicated a decrease in the grain size of the CuAg matrix. Using the FSP in the presence of reinforcing particles and without it led to a decrease in the crystal size and average grain size compared to the sample without FSP. So that the grain size of the sample without FSP and the FSPed sample without reinforcing particles and with nano-reinforcing particles were found to be about 46.3, 19.2 and 3.6 µm, respectively. The wear mechanism in the sample before FSP was adhesive wear due to its soft nature of the matrix, and after FSP in the sample without reinforcing particles, the adhesive wear decreased and due to the addition of silicon carbide micro and nano- particles reinforcement, the wear mechanism in entirely altered to abrasive wear. Overall, it can be stated that the addition of silicon carbide nanoparticles by FSP leads to the fabrication of Cu-Ag-SiC composite with high mechanical properties.
H. Abedi Chermahini, M. Piran, A. Esmaeili Chamgordani, M. Atapoor,
Volume 10, Issue 2 (12-2024)
Abstract
In this research, the mechanical and microstructural properties of AISI 316L sheets welded by RSW method using copper interlayer were investigated. In this regard, two types of connections were made, one without the use of an interlayer and the other with the use of a copper interlayer in different currents. In order to choose the optimal current for both types of connections, tensile tests were first performed, and microstructural, microhardness, elemental evaluation and failure mode tests were conducted on the selected samples. According to the obtained results, by increasing the electric current, the heat input in the welding pool is sufficiently high and the microstructural and mechanical properties of the welding zone were improved(Conversion of coarse grain to fine grain). Also, due to the optimality of the electric current in both samples with and without the interface layer, both samples had environmental failure, which indicates the high strength of the interface and their welding point. Changes in the chemical composition in different welding zones were insignificant and the distribution of elements was uniform in all zones. Also, the hardness changes from the base metal to the center of the welding zone were in the order of welding zone > base metal > heat-affected zone, which was consistent with the results obtained from the microstructural investigations. According to the results obtained for both cases with and without the use of an interface layer, the resistance spot welding method showed a successful connection for both types of cases.
H. Abedi Chermahini, M. Atapoor, M. Esmailzadeh,
Volume 10, Issue 2 (12-2024)
Abstract
Nowadays, in order to achieve the combined properties of multiple alloys for important applications such as automotive and marine industries, the use of cladding method is common. Cladding, which is a type of coating through welding, is one of the widely used methods for surface modification of metal parts and sheets in industry. AH36 low-alloy steel is a steel used in shipbuilding, known for its toughness and good corrosion resistance, making it a significant condidcate among other steels used in this industry. In this research, to enhance the corrosion properties of AH36 steel, the cladding process was performed using Gas Tungsten Arc Welding (GTAW) with copper/nickel filler wire. Two samples, one from the coated (weld metal) and one from the uncoated (base metal) sections, were prepared and subjected to microstructural and corrosion investigations. The results indicated an increase in grain size in the heat-affected zone of the weld metal sample, leading to a reduction in mechanical properties. The cyclic polarization test showed that the base metal had higher susceptibility to pitting corrosion compared to the weld metal. Additionally, the weld metal exhibited a higher tendency for repassivation or repairing of the pits. The results of the electrochemical impedance spectroscopy (EIS) test indicated that both the base metal and weld metal samples had a single-loop equivalent circuit. The larger diameter of the Nyquist semicircle for the base metal compared to the weld metal suggests better uniform corrosion behavior of the base metal relative to the weld metal.
M. K. Vojdanpak, B. Niroumand, M. Shamanian,
Volume 10, Issue 2 (12-2024)
Abstract
Despite rapid advancement of additive manufacturing methods in recent years, sufficient research on bonding of additively manufactured materials to conventional alloys has not been conducted. This study evaluates the bonding between austenitic stainless steel L316 and Ti-6242 alloy, fabricated by electron beam melting, using the transient liquid phase (TLP) bonding method. The TLP bonding was achieved using a copper interlayer and processing in a vacuum furnace, examining the effects of process time and surface roughness on bond quality. The samples were characterized by optical and scanning electron microscopy, X-ray diffraction, shear strength testing, and surface roughness measurement. Results showed that reducing the surface roughness increased the shear strength. Additionally, processing time significantly affected the element diffusion, formation of intermetallic compounds like FeTi and TiCu, and the shear strength of the joints. The highest shear strength of 200 MPa was obtained with surface preparation by grinding and polishing and bonding at 980°C for 120 minutes.
Kh. Ranjbar, A. Firoozi, F. Shahriari Nogoorani, S. F. Ziaee,
Volume 10, Issue 2 (12-2024)
Abstract
Plain carbon steels are widely utilized in various industrial applications primarily due to their low cost. However, these steels often fall short in terms of mechanical properties and wear resistance. The deposition of hard and wear-resistant coatings on these steels significantly enhances their performance and extends their range of applications. Colomonoy 6, is a nickel-based superalloy, enhance hardness, erosion resistance, wear resistance, and corrosion resistance on the applied surfaces. The study investigated the application of weld overlay using colomonoy 6 on a plain carbon steel, aimed to create a hard and wear-resistant surface. The overlaying processes were performed using plasma transfer arc welding and gas tungsten arc welding under identical conditions. Microstructural characteristics were examined through optical and electron microscopy, and Phase analysis was performed using X-ray diffraction technique. The wear behavior of the weld overlays was evaluated using pin-on-disc wear testing at three different temperatures: 25 °C, 300 °C, and 600 °C, using an alumina pin. The microstructural investigation revealed the formation of dendritic nickel-rich solid solutions and interdendritic carbide and boride phases within the overlays, contributing to improved hardness and wear properties. Results demonstrated that in both overlaying methods, the wear mechanism at room temperature was mild abrasive, whereas at 600 °C, it was plastic deformation, exhibiting a wear track depth of approximately 33-35 μm, and 50-55 μm, respectively. In both overlayed metals, an approximate Vickers hardness number of 600 was measured a 4-fold increase in hardness of substrate. This finding suggests that factors other than hardness, such as microstructural stability and phase distribution at elevated temperatures, play significant roles in wear performance.
E. Ranjbarnodeh, P. Raissi , A. Kolagar , M. Cheraghzadeh,
Volume 10, Issue 2 (12-2024)
Abstract
Nickel base superalloy IN738LC is widely used in power plant industry and gas turbine blade manufacturing. The main strengthening mechanism of this alloy is the precipitation hardness caused by γ′ precipitates. These precipitates play an important role in determining the mechanical properties of this alloy and their amount and morphology changes under heat treatment. In this research, in order to investigate the evolution of γ' precipitates during heat treatment, a number of solution annealed samples were subjected to arc heat treatment. In this heat treatment, by applying heat caused by a static arc, a temperature ranges from the ambient temperature to above the melting point is created in the sample. Using this process, samples with 100 amp currents were heat treated for 1, 2 and 15 minutes. Electron microscope, image processing and transient heat transfer model with axial symmetry were used for experimental and mathematical investigations. In the following, using the experimental and numerical results simultaneously, a mathematical model for the dissolution kinetics of γ' precipitates in the heat-affected zone of these welds was presented. The results of electron microscopy showed that the dissolution rate and shape of γ′ precipitates are strongly influenced by the distance from the heat source. The activation energy of dissolution of γ′ precipitates increased with increasing time and its value was between 40 and
80 kJ/mol.