Showing 4 results for Isothermal Solidification
S. Ghaderi, F. Karimzadeh, A. Ashrafi,
Volume 5, Issue 2 (1-2020)
Abstract
In the present study, the effect of time and base metal microstructure on the Transient Liquid Phase (TLP) bonding of 304L stainless steel was studied. TLP was performed at 1050 0C for 5 and 60 minutes on the coarse grain austenitic and martensitic microstructure using BNi-2 interlayer. To prepare martensitic microstructure, as-received 304L was rolled at -15 0C up to 80% rolling reduction. TEM analysis was proved that the microstructure of 80% rolled samples consisted of two different morphologies of martensite namely as lath-type and dislocation cell type martensite. It was observed that the structure of bonded zone after 5 min has consisted of isothermally solidified zone (ISZ) containing γ solid solution and athermally solidified zone (ASZ) containing complex boride phases. Meanwhile, after 60 min of heating, the structure of bonded zone completely solidifies isothermally. The obtained results also showed that the martensitic microstructure considerably effect on the width of diffusion affected zone (DAZ) which was related to the reversion of martensite to ultrafine grain austenite during heating.
Dr Behzad Binesh, Dr Sima Mirzaei, Mr Amin Taghi-Ahari,
Volume 7, Issue 2 (1-2022)
Abstract
Transient liquid phase (TLP) bonding of AISI 304L stainless steel was carried out using BNi-2 amorphous interlayer. The microstructure of the joint area was studied by using optical and scanning electron microscopes and energy dispersive spectroscopy. The effect of bonding temperature (1030-1110 °C) was studied on the microstructure and corrosion behavior of the TLP bonded samples. Electrochemical corrosion resistance of the bonded samples was evaluated in 3.5% NaCl solution at room temperature. The mechanism of the microstructure formation and the solidification sequence at the joint area were discussed. Ni- and Cr-rich borides, Ni-Si-B compound and fine Ni3Si particles were identified in the γ-Ni matrix at the joint centerline. The microstructural investigations revealed that the solidification sequence of these phases is: L→ γ + L → γ + Ni boride + Cr boride + L → γ + Ni boride + Cr boride + Ni-Si-B Compound. The highest corrosion resistance was observed in the sample bonded at 1070 °C for 30 min, which is comparable to that of the as-received AISI 304L stainless steel. It was attributed to the bond region microstructure with a negligible amount of eutectic constituents formed in the athermally solidified zone.
M. J. Bagban, M. Mosallaee Pour, H. Hajisafari, A. Babnejad, A. Saboori,
Volume 8, Issue 1 (8-2022)
Abstract
In the present study, the microstructure and mechanical properties of the dissimilar joint of Inconel 625 (IN-625) superalloy to austenitic stainless steel AISI316L (SS-316L) via AWS-BNi3 interface layer and transient liquid phase (TLP) bonding process were evaluated and necessary conditions for creating an efficient joint were determined. TLP bonding was performed in temperature and time range of 1050-1150ºC and 5-20min, respectively, under the protection of argon shielding gas with a purity of 99.9995%. Microstructural (OM and SEM) and phase (XRD) studies revealed that bonding at 1150 ° C for 20 min results in completion of isothermal solidification and develops a uniform gamma (γ) phase at the bonding zone. Cooling the samples before completion of isothermal solidification results in the formation of chromium and molybdenum-rich eutectic compounds at the bonding centerline. The continuous morphology of the eutectic compounds caused a sharp drop in the shear strength of the specimens (~50% reduction of shear strength). The inter-diffusion of alloying elements between the bonding area and the surrounding base metal results in the formation of chromium carbide in the IN-625 and chromium- boron compounds in the SS-316L, which increased the microhardness of these areas compared to the base metals and the bonding zone.
M. M. Taghvaei, M. Shamanian, Behzad Niroumand, H. Mostaan,
Volume 8, Issue 2 (1-2023)
Abstract
Joining of Hastelloy C276 nickel-base superalloy to AISI316 Stainless Steel using BNi-2 interlayer performed by transient liquid phase process (TLP) at 1150°C for 5 and 30 minutes. Bonding microstructure was studied using an Optical microscope and a scanning electron microscope (SEM). Vickers hardness test and shear strength test have been used to evaluate the mechanical properties. Microstructural studies showed that at 5 and 30 minutes of bonding time, isothermal solidification is completely formed, and the Center of the joint is free of any eutectic intermetallic compounds. Also, Findings showed that the DAZ of Hastelloy C276 nickel-base superalloy contains rich borides of Ni, Cr, Mo, and W, and the DAZ of 316 austenitic stainless steel contains borides rich in Fe, Cr, and Ni.
